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    Method for producing thin film electrodes
    3.
    发明授权
    Method for producing thin film electrodes 有权
    薄膜电极的制造方法

    公开(公告)号：US09359223B2

    公开(公告)日：2016-06-07

    申请号：US13237487

    申请日：2011-09-20

    申请人： Manoj Narayanan ,  Beihai Ma ,  Uthamalingam Balachandran ,  Stephen Dorris

    发明人： Manoj Narayanan ,  Beihai Ma ,  Uthamalingam Balachandran ,  Stephen Dorris

    IPC分类号： B05D5/12 ,  C01G55/00 ,  H01L49/02

    CPC分类号： H05K3/068 ,  C01G55/00 ,  C01G55/002 ,  C01P2004/03 ,  C01P2006/32 ,  C01P2006/40 ,  H01B1/08 ,  H01L28/65 ,  H05K1/092 ,  Y10T428/31678

    摘要： The invention provides for A method for producing pure phase strontium ruthenium oxide films, the method comprising solubilizing ruthenium-containing and strontium-containing compounds to create a mixture; subjecting the mixture to a first temperature above that necessary for forming RuO2 while simultaneously preventing formation of RuO2; maintaining the first temperature for a time to remove organic compounds from the mixture, thereby forming a substantially dry film; and subjecting the film to a second temperature for time sufficient to crystallize the film. Also provided is pure phase material comprising strontium ruthenium oxide wherein the material contains no RuO2.

    摘要翻译： 本发明提供了一种生产纯相锶氧化钌薄膜的方法，该方法包括使含钌和含锶化合物溶解以产生混合物; 使混合物经受高于形成RuO 2所必需的第一温度，同时防止形成RuO 2; 保持第一温度一段时间以从混合物中除去有机化合物，从而形成基本干燥的膜; 并将膜处于第二温度足以使膜结晶的时间。 还提供了包含氧化钌的纯相材料，其中该材料不含RuO 2。

    Method for preparing solid ruthenium nitrosyl nitrate
    5.
    发明授权
    Method for preparing solid ruthenium nitrosyl nitrate 有权
    固体硝基硝酸硝基钌的制备方法

    公开(公告)号：US09005555B2

    公开(公告)日：2015-04-14

    申请号：US14475547

    申请日：2014-09-02

    申请人： Sunshine Kaidi New Energy Group Co., Ltd.

    发明人： Li Xu ,  Bo Lai ,  Dechen Song ,  Qianqian Liu ,  Yiming Han

    IPC分类号： C01G55/00 ,  C22B3/00

    CPC分类号： C22B11/048 ,  C01G55/00 ,  C01P2006/80 ,  C22B1/005 ,  C22B7/009 ,  Y02P10/214 ,  Y02P10/234

    摘要： A method for preparing solid ruthenium nitrosyl nitrate, including: 1) drying a ruthenium-containing spent catalyst, and calcining the spent catalyst, and cooling to room temperature, whereby yielding a ruthenium-containing solid; 2) grinding the ruthenium-containing solid to yield a powder, introducing the powder to a fluidized bed reactor, aerating the fluidized bed reactor with nitrogen or an inert gas, charging hydrogen, whereby yielding ruthenium metal; 3) contacting a mixed gas of ozone and air with the ruthenium metal, whereby yielding gaseous ruthenium tetroxide; 4) introducing the gaseous ruthenium tetroxide into a three-stage absorption plant, whereby yielding an acid solution including ruthenium nitrate; 5) adding a solid of sodium nitrite to the acid solution, stirring, and heating a resulting solution, whereby yielding a solution of ruthenium nitrosyl nitrate; and 6) extracting the solution of ruthenium nitrosyl nitrate with anhydrous ether.

    摘要翻译： 一种制备固体硝酸亚硝基硝酸盐的方法，包括：1）干燥含钌废废催化剂，煅烧废催化剂，冷却至室温，由此得到含钌固体; 2）研磨含钌固体产生粉末，将粉末引入流化床反应器，用氮气或惰性气体充气流化床反应器，加入氢气，从而产生钌金属; 3）将臭氧和空气的混合气体与钌金属接触，从而产生四氧化四钌; 4）将气态四氧化钌引入三级吸收装置，从而产生包含硝酸钌的酸溶液; 5）向酸溶液中加入亚硝酸钠固体，搅拌并加热所得溶液，由此得到硝酸亚硝基硝酸钌溶液; 和6）用无水乙醚萃取硝酸亚硝基硝酸钌溶液。