公开(公告)号：US5714013A

公开(公告)日：1998-02-03

申请号：US681704

申请日：1996-07-29

申请人： Kazuchika Ohta ,  Tsuyoshi Komatsu

发明人： Kazuchika Ohta ,  Tsuyoshi Komatsu

IPC分类号： B23K35/363 ,  B23K1/00 ,  B23K31/12 ,  B23K35/02 ,  B23K35/14 ,  B23K35/26 ,  H05K1/02 ,  H05K3/34 ,  B23K35/362

CPC分类号： B23K31/12 ,  B23K35/025 ,  B23K35/26 ,  H05K1/0266 ,  H05K3/3457 ,  H05K3/3484

摘要： The present invention relates to a method of infusing coloration in solder to facilitate inspection of soldered portions in the production of electronic machinery, equipment and apparatus, and further, a method of forming a colored membrane on the surface of the soldered portions by employing colored solder materials. Physically and chemically stable colored powders composed of rare earth compounds or metallic fluoride compounds, having properties of specific gravity lighter than that of solder and further being indecomposable even at a temperature higher than that of the melting points of solders, are mixed into flux. After soldering by employing solder cream containing the mixture, a colored membrane or layer may be formed on the surface of soldered portions by deposition of the colored powder compounds.

摘要翻译： 本发明涉及一种在焊料中浸渍着色的方法，便于在电子机器，设备和设备的生产中对焊接部分进行检查，另外，通过使用着色焊料在焊接部分的表面上形成着色膜的方法 材料 由稀土化合物或金属氟化物组成的物理化学稳定的着色粉末，比具有比焊料重的比重的特性，甚至在比焊料的熔点高的温度下也是不可分解的。 在使用含有混合物的焊膏进行焊接之后，可以通过沉积着色的粉末化合物在焊接部分的表面上形成有色的膜或层。

公开(公告)号：US5110916A

公开(公告)日：1992-05-05

申请号：US633248

申请日：1990-12-21

申请人： Iwao Yamamoto ,  Kazuchika Ohta ,  Tsuyoshi Komatsu

发明人： Iwao Yamamoto ,  Kazuchika Ohta ,  Tsuyoshi Komatsu

IPC分类号： C07D487/22 ,  C07F5/00 ,  C09B47/06 ,  C09B47/08 ,  C09K9/02 ,  C09K19/40

CPC分类号： C07D487/22 ,  C09B47/062 ,  C09B47/08 ,  C09K19/40 ,  C09K9/02

摘要： The present invention discloses lanthanide series bisphthalocyanine complex compounds, wherein chemically and thermally stable side chains effective for the development of a functional film due to generation of solubility and liquid crystallization in a solvent.The compounds according to the present invention having no reacting positions at side chains thereof possess electrochromic properties and further possess excellent electrochemical characteristics. Moreover, these compounds are soluble in a solvent and show discotic liquid crystal phase. Therefore, these compounds are very effective for the development of a functional film.

摘要翻译： 本发明公开了镧系系列双酞菁络合物，其中化学和热稳定的侧链由于在溶剂中产生溶解度和液晶而有效地发挥功能性膜。 在侧链上没有反应位置的根据本发明的化合物具有电致变色性质，并且还具有优异的电化学特性。 此外，这些化合物可溶于溶剂并显示盘状液晶相。 因此，这些化合物对功能膜的开发非常有效。

公开(公告)号：US20100196248A1

公开(公告)日：2010-08-05

申请号：US12534268

申请日：2009-08-03

申请人： Kazuchika OHTA ,  Ick-Soo KIM ,  Byoung-Suhk KIM ,  Jongchul PARK

发明人： Kazuchika OHTA ,  Ick-Soo KIM ,  Byoung-Suhk KIM ,  Jongchul PARK

IPC分类号： D01F9/12

CPC分类号： B82Y40/00 ,  B01J31/04 ,  B01J2531/847 ,  B82Y30/00 ,  C01B32/162 ,  Y10S977/842 ,  Y10S977/844

摘要： A method for manufacturing carbon nanotubes of the present invention includes the steps of: preparing a metal complex which contains at least one metal selected from a group consisting of iron, cobalt and nickel and an organic compound: and forming carbon nanotubes which contain metal therein by using the organic compound as a carbon source, wherein the carbon nanotubes are formed by putting the metal complex into a heating vessel which has a substance capable of converting electromagnetic energy into heat, and by heating the metal complex using heat which is generated by the heating vessel when electromagnetic energy is applied to the heating vessel. As the metal complex used in a method for manufacturing carbon nanotubes of the present invention, nickel stearate or nickel benzoate can be named, for example. According to the method for manufacturing carbon nanotubes of the present invention, it is possible to manufacture carbon nanotubes using an inexpensive heating device within a short time.

摘要翻译： 本发明的制造碳纳米管的方法包括以下步骤：制备含有选自铁，钴和镍中的至少一种金属和有机化合物的金属络合物，并通过以下方法形成含有金属的碳纳米管： 使用有机化合物作为碳源，其中通过将金属络合物放入具有能够将电磁能转化成热的物质的加热容器中，并且通过加热产生的加热金属络合物来形成碳纳米管 当电磁能被施加到加热容器时的容器。 作为本发明的碳纳米管制造方法中使用的金属络合物，例如可以列举硬脂酸镍或苯甲酸镍。 根据本发明的碳纳米管的制造方法，可以在短时间内使用便宜的加热装置制造碳纳米管。

公开(公告)号：US08192714B2

公开(公告)日：2012-06-05

申请号：US12534262

申请日：2009-08-03

申请人： Kazuchika Ohta ,  Ick-Soo Kim ,  Byoung-Suhk Kim ,  Jongchul Park

发明人： Kazuchika Ohta ,  Ick-Soo Kim ,  Byoung-Suhk Kim ,  Jongchul Park

IPC分类号： D01F9/12 ,  B01J19/08

CPC分类号： B82Y40/00 ,  B82Y30/00 ,  C01B32/162 ,  Y10S977/842 ,  Y10S977/844

摘要： A method for manufacturing carbon nanotubes of the present invention includes the steps of: preparing at least one metal selected from a group consisting of iron, cobalt and nickel and an organic compound: and forming carbon nanotubes by using the organic compound as a carbon source, wherein the metal and the organic compound are put into a heating vessel having a substance capable of converting electromagnetic energy into heat, and the organic compound is brought into contact with the metal in a state where the inside of the heating vessel is heated at a temperature of 600° C. to 900° C. by applying the electromagnetic energy to the heating vessel so as to form the carbon nanotubes.

摘要翻译： 本发明的制造碳纳米管的方法包括以下步骤：制备选自铁，钴和镍中的至少一种金属和有机化合物，并通过使用有机化合物作为碳源形成碳纳米管， 其中将金属和有机化合物放入具有能够将电磁能转换成热的物质的加热容器中，并且在加热容器的内部被加热的状态下使有机化合物与金属接触 通过将电磁能施加到加热容器以形成碳纳米管，其温度为600℃至900℃。

公开(公告)号：US5650020A

公开(公告)日：1997-07-22

申请号：US340735

申请日：1994-11-16

申请人： Kazuchika Ohta ,  Tsuyoshi Komatsu

发明人： Kazuchika Ohta ,  Tsuyoshi Komatsu

IPC分类号： B23K35/363 ,  B23K1/00 ,  B23K31/12 ,  B23K35/02 ,  B23K35/14 ,  B23K35/26 ,  H05K1/02 ,  H05K3/34 ,  B23K35/34

CPC分类号： B23K31/12 ,  B23K35/025 ,  B23K35/26 ,  H05K1/0266 ,  H05K3/3457 ,  H05K3/3484

摘要： The present invention relates to a method of infusing coloration in solder to facilitate inspection of soldered portions in the production of electronic machinery, equipment and apparatus, and further, a method of forming a colored membrane on the surface of the soldered portions by employing colored solder materials.Physically and chemically stable colored powders composed of rare earth compounds or metallic fluoride compounds, having properties of specific gravity lighter than that of solder and further being indecomposable even at a temperature higher than that of the melting points of solders, are mixed into flux. After soldering by employing solder cream containing the mixture, a colored membrane or layer may be formed on the surface of soldered portions by deposition of the colored powder compounds.

摘要翻译： 本发明涉及一种在焊料中浸渍着色的方法，便于在电子机器，设备和设备的生产中对焊接部分进行检查，另外，通过使用着色焊料在焊接部分的表面上形成着色膜的方法 材料 由稀土化合物或金属氟化物组成的物理化学稳定的着色粉末，比具有比焊料重的比重的特性，甚至在比焊料的熔点高的温度下也是不可分解的。 在使用含有混合物的焊膏进行焊接之后，可以通过沉积着色的粉末化合物在焊接部分的表面上形成有色的膜或层。

公开(公告)号：US08333947B2

公开(公告)日：2012-12-18

申请号：US12534252

申请日：2009-08-03

申请人： Kazuchika Ohta ,  Ick-Soo Kim ,  Byoung-Suhk Kim ,  Jongchul Park

发明人： Kazuchika Ohta ,  Ick-Soo Kim ,  Byoung-Suhk Kim ,  Jongchul Park

IPC分类号： D01F9/12 ,  B01J19/08

CPC分类号： B82Y40/00 ,  B82Y30/00 ,  C01B32/15

摘要： A method for manufacturing carbon nanotubes includes the steps of: preparing metal-containing-nanofibers which include nanofibers made of organic polymer and metal which possesses a catalytic function in forming carbon nanotubes; and forming carbon nanotubes which contain metal therein by using the nanofibers as a carbon source, wherein the carbon nanotubes are formed by putting the metal-containing-nanofibers into a heating vessel which has a substance capable of converting electromagnetic energy into heat, and by heating the metal-containing-nanofibers using heat which is generated by the heating vessel when electromagnetic energy is applied to the heating vessel.

摘要翻译： 制造碳纳米管的方法包括以下步骤：制备含有纳米纤维的纳米纤维，所述纳米纤维包括由有机聚合物制成的纳米纤维和在形成碳纳米管时具有催化功能的金属; 并且通过使用纳米纤维作为碳源形成含有金属的碳纳米管，其中，通过将含金属的纳米纤维放入具有能够将电磁能转化为热的物质的加热容器中，并且通过加热形成碳纳米管 含有电子的纳米纤维，当电磁能被施加到加热容器时，使用由加热容器产生的热量。

公开(公告)号：US20100296996A1

公开(公告)日：2010-11-25

申请号：US12534252

申请日：2009-08-03

申请人： Kazuchika OHTA ,  Ick-Soo KIM ,  Byoung-Suhk KIM ,  Jongchul PARK

发明人： Kazuchika OHTA ,  Ick-Soo KIM ,  Byoung-Suhk KIM ,  Jongchul PARK

IPC分类号： D01F9/12

CPC分类号： B82Y40/00 ,  B82Y30/00 ,  C01B32/15

摘要： A method for manufacturing carbon nanotubes includes the steps of: preparing metal-containing-nanofibers which include nanofibers made of organic polymer and metal which possesses a catalytic function in forming carbon nanotubes; and forming carbon nanotubes which contain metal therein by using the nanofibers as a carbon source, wherein the carbon nanotubes are formed by putting the metal-containing-nanofibers into a heating vessel which has a substance capable of converting electromagnetic energy into heat, and by heating the metal-containing-nanofibers using heat which is generated by the heating vessel when electromagnetic energy is applied to the heating vessel.

摘要翻译： 制造碳纳米管的方法包括以下步骤：制备含有纳米纤维的纳米纤维，所述纳米纤维包括由有机聚合物制成的纳米纤维和在形成碳纳米管时具有催化功能的金属; 并且通过使用纳米纤维作为碳源形成含有金属的碳纳米管，其中，通过将含金属的纳米纤维放入具有能够将电磁能转化为热的物质的加热容器中，并且通过加热形成碳纳米管 含有电子的纳米纤维，当电磁能被施加到加热容器时，使用由加热容器产生的热量。

公开(公告)号：US08202504B2

公开(公告)日：2012-06-19

申请号：US12534268

申请日：2009-08-03

申请人： Kazuchika Ohta ,  Ick-Soo Kim ,  Byoung-Suhk Kim ,  Jongchul Park

发明人： Kazuchika Ohta ,  Ick-Soo Kim ,  Byoung-Suhk Kim ,  Jongchul Park

IPC分类号： D01F9/12 ,  B01J19/08

CPC分类号： B82Y40/00 ,  B01J31/04 ,  B01J2531/847 ,  B82Y30/00 ,  C01B32/162 ,  Y10S977/842 ,  Y10S977/844

摘要： A method for manufacturing carbon nanotubes of the present invention includes the steps of: preparing a metal complex which contains at least one metal selected from a group consisting of iron, cobalt and nickel and an organic compound: and forming carbon nanotubes which contain metal therein by using the organic compound as a carbon source, wherein the carbon nanotubes are formed by putting the metal complex into a heating vessel which has a substance capable of converting electromagnetic energy into heat, and by heating the metal complex using heat which is generated by the heating vessel when electromagnetic energy is applied to the heating vessel. As the metal complex used in a method for manufacturing carbon nanotubes of the present invention, nickel stearate or nickel benzoate can be named, for example. According to the method for manufacturing carbon nanotubes of the present invention, it is possible to manufacture carbon nanotubes using an inexpensive heating device within a short time.

摘要翻译： 本发明的制造碳纳米管的方法包括以下步骤：制备含有选自铁，钴和镍中的至少一种金属和有机化合物的金属络合物，并通过以下方法形成含有金属的碳纳米管： 使用有机化合物作为碳源，其中通过将金属络合物放入具有能够将电磁能转化成热的物质的加热容器中，并且通过加热产生的加热金属络合物来形成碳纳米管 当电磁能被施加到加热容器时的容器。 作为本发明的碳纳米管制造方法中使用的金属络合物，例如可以列举硬脂酸镍或苯甲酸镍。 根据本发明的碳纳米管的制造方法，可以在短时间内使用便宜的加热装置制造碳纳米管。

公开(公告)号：US20100196247A1

公开(公告)日：2010-08-05

申请号：US12534262

申请日：2009-08-03

申请人： Kazuchika OHTA ,  Ick-Soo KIM ,  Byoung-Suhk KIM ,  Jongchul PARK

发明人： Kazuchika OHTA ,  Ick-Soo KIM ,  Byoung-Suhk KIM ,  Jongchul PARK

IPC分类号： D01F9/12

CPC分类号： B82Y40/00 ,  B82Y30/00 ,  C01B32/162 ,  Y10S977/842 ,  Y10S977/844

摘要： A method for manufacturing carbon nanotubes of the present invention includes the steps of: preparing at least one metal selected from a group consisting of iron, cobalt and nickel and an organic compound: and forming carbon nanotubes by using the organic compound as a carbon source, wherein the metal and the organic compound are put into a heating vessel having a substance capable of converting electromagnetic energy into heat, and the organic compound is brought into contact with the metal in a state where the inside of the heating vessel is heated at a temperature of 600° C. to 900° C. by applying the electromagnetic energy to the heating vessel so as to form the carbon nanotubes.

摘要翻译： 本发明的制造碳纳米管的方法包括以下步骤：制备选自铁，钴和镍中的至少一种金属和有机化合物，并通过使用有机化合物作为碳源形成碳纳米管， 其中将金属和有机化合物放入具有能够将电磁能转换成热的物质的加热容器中，并且在加热容器的内部被加热的状态下使有机化合物与金属接触 通过将电磁能施加到加热容器以形成碳纳米管，其温度为600℃至900℃。

公开(公告)号：US5062990A

公开(公告)日：1991-11-05

申请号：US457397

申请日：1989-12-27

申请人： Iwawo Yamamoto ,  Kazuchika Ohta

发明人： Iwawo Yamamoto ,  Kazuchika Ohta

IPC分类号： G02F1/13 ,  C07D487/22 ,  C09K19/34 ,  C09K19/40 ,  H01B1/12

CPC分类号： C07D487/22 ,  C09K19/3488 ,  C09K19/40 ,  H01B1/12 ,  C09K2019/0429

摘要： Octasubstituted tetraphyrazinotetraazaporphrazine and compositions forming an electron acceptable discotic liquid crystal phase are disclosed. Said compounds and the metal complexes are easily soluble in an organic solvent such as chloroform or dichloromethane etc and are insoluble in acetone and alcohols; and therefore a columnar phase by silica gel/dichloromethane, recrystallization from tetra-hydrofuran or refining through solid liquid extraction by acetone is possible. Furthermore, stability in a giant molecular can be expected and a functional membrane can be formed by a solution cast method etc., thereby employing as an electon or photoelectron material or an indication element.

摘要翻译： 公开了八取代的四联氮杂四氮杂菲和形成电子可接受的盘状液晶相的组合物。 所述化合物和金属络合物易溶于有机溶剂如氯仿或二氯甲烷等，并且不溶于丙酮和醇; 因此通过硅胶/二氯甲烷进行柱状相，由四氢呋喃重结晶或通过丙酮固液萃取进行精制。 此外，可以预期在巨分子中的稳定性，并且可以通过溶液流延法等形成功能膜，由此使用电子或光电子材料或指示元件。