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    N-cycloalkyl-3-alkenybenzoyl-pyrazole derivatives
    4.
    发明授权
    N-cycloalkyl-3-alkenybenzoyl-pyrazole derivatives 失效
    N-环烷基-3-烯基苯甲酰基 - 吡唑衍生物

    公开(公告)号：US06475957B1

    公开(公告)日：2002-11-05

    申请号：US10019047

    申请日：2001-12-27

    申请人： Ulf Neidlein ,  Norbert Götz ,  Ernst Baumann ,  Wolfgang von Deyn ,  Steffen Kudis ,  Roland Götz ,  Klaus Langemann ,  Guido Mayer ,  Ulf Misslitz ,  Matthias Witschel ,  Martina Otten ,  Karl-Otto Westphalen ,  Helmut Walter

    发明人： Ulf Neidlein ,  Norbert Götz ,  Ernst Baumann ,  Wolfgang von Deyn ,  Steffen Kudis ,  Roland Götz ,  Klaus Langemann ,  Guido Mayer ,  Ulf Misslitz ,  Matthias Witschel ,  Martina Otten ,  Karl-Otto Westphalen ,  Helmut Walter

    IPC分类号： A01N4356

    CPC分类号： A01N43/56 ,  C07D231/20

    摘要： Cycloalkyl-substituted benzoylpyrazoles of the formula I where the variables have, for example, the following meanings: R1 is hydrogen, nitro, halogen, cyano, thiocyanato, or an unsubstituted or substituted aliphatic radical; R2 is an unsubstituted or substituted aliphatic radical, halogen, nitro, or substituted sulfonyl or amino groups, R3 is hydrogen, halogen, C1-C6-alkyl, C1-C6-haloalkyl, C1-C6-alkoxy, C2-C6-alkenyl or C2-C6-alkynyl; R4, R5 are hydrogen, nitro, halogen, cyano, thiocyanato, an unsubstituted or substituted aliphatic radical or substituted sulfonyl or amino groups; R6 is hydrogen, halogen, C1-C6-alkyl, C1-C6-alkoxy, C3-C8-cycloalkyl; R7 is a cyclic ring system having 3-14 ring atoms; R16 is hydroxyl or a substituted hydroxyl group; and their tautomers or agriculturally useful salts are described. Moreover, the invention describes processes for preparing compounds of the formula I, compositions comprising them, and the use of the compounds of the formula I and of the compositions comprising them for controlling harmful plants.

    摘要翻译： 式I的环烷基取代的苯甲酰基吡唑，其中变量具有例如以下含义：R 1是氢，硝基，卤素，氰基，氰硫基或未取代或取代的脂族基; R 2是未取代或取代的脂族基，卤素， 硝基或取代的磺酰基或氨基，R 3是氢，卤素，C 1 -C 6烷基，C 1 -C 6卤代烷基，C 1 -C 6 - 烷氧基，C 2 -C 6 - 烯基或C 2 -C 6 - 炔基; R 4，R 5是氢 硝基，卤素，氰基，氰硫基，未取代或取代的脂族基团或取代的磺酰基或氨基; R 6是氢，卤素，C 1 -C 6烷基，C 1 -C 6 - 烷氧基，C 3 -C 8环烷基; 具有3-14个环原子的环系; R 16是羟基或取代的羟基;并且描述了它们的互变异构体或农业上有用的盐。此外，本发明描述了制备式I化合物的方法，包含它们的组合物，以及使用 式I化合物和组合物的化合物 包括它们用于控制有害植物。

    TRICYCLIC BENZOYLPYRAZOLE DERIVATIVES
    5.
    发明申请
    TRICYCLIC BENZOYLPYRAZOLE DERIVATIVES 审中-公开
    三苯甲酰基吡唑衍生物

    公开(公告)号：US20070197393A1

    公开(公告)日：2007-08-23

    申请号：US11461491

    申请日：2006-08-01

    申请人： Matthias Witschel ,  Steffen Kudis ,  Klaus Langemann ,  Ernst Baumann ,  Wolfgang von Deyn ,  Guido Mayer ,  Ulf Misslitz ,  Ulf Neidlein ,  Martina Otten ,  Karl-Otto Westphalen ,  Helmut Walter

    发明人： Matthias Witschel ,  Steffen Kudis ,  Klaus Langemann ,  Ernst Baumann ,  Wolfgang von Deyn ,  Guido Mayer ,  Ulf Misslitz ,  Ulf Neidlein ,  Martina Otten ,  Karl-Otto Westphalen ,  Helmut Walter

    IPC分类号： A01N43/02 ,  A01N43/08 ,  A01N43/16 ,  A01N43/18 ,  A01N43/58

    CPC分类号： C07D413/06 ,  A01N43/80 ,  A01N43/90 ,  C07D491/04 ,  C07D495/04

    摘要： Tricyclic benzoylpyrazole derivatives of the formula I where: X is oxygen, sulfur, S═O, S(═O)2, CR6R7, NR8 or a bond; Y together with the two carbons to which it is attached forms a saturated, partially saturated or unsaturated 5- or 6-membered heterocycle; R1, R2, R6, R7 are hydrogen, alkyl, haloalkyl, alkoxy or haloalkoxy; R3 is halogen, alkyl, haloalkyl, alkoxy or haloalkoxy; R4 is hydrogen, nitro, halogen, cyano, alkyl, haloalkyl, alkoxy, haloalkoxy, alkylthio, haloalkylthio, alkylsulfinyl, haloalkylsulfinyl, alkylsulfonyl, haloalkylsulfonyl, unsubstituted or substituted aminosulfonyl or unsubstituted or substituted sulfonylamino; R5 is hydrogen, alkyl or halogen; l is 0, 1 or 2; R8 is hydrogen, alkyl, haloalkyl, alkylcarbonyl, formyl, alkoxycarbonyl, haloalkoxycarbonyl, alkylsulfonyl or haloalkylsulfonyl; R9 is substituted pyrazol-4-ylcarbonyl or substituted 5-oxopyrazolin-4-ylmethylidene; and their agriculturally useful salts; processes and intermediates for preparing the tricyclic benzoylpyrazole derivatives; compositions comprising them and the use of these derivatives or of the compositions comprising them for controlling undesirable plants are described.

    摘要翻译： 式I的三环苯甲酰基吡唑衍生物其中：X是氧，硫，SO，S（-O）2，CR 6，R 7， NR 8或键; Y与连接的两个碳一起形成饱和的，部分饱和的或不饱和的5-或6-元杂环; R 1，R 2，R 6，R 7是氢，烷​​基，卤代烷基，烷氧基或卤代烷氧基; R 3是卤素，烷基，卤代烷基，烷氧基或卤代烷氧基; R 4是氢，硝基，卤素，氰基，烷基，卤代烷基，烷氧基，卤代烷氧基，烷硫基，卤代烷硫基，烷基亚磺酰基，卤代烷基亚磺酰基，烷基磺酰基，卤代烷基磺酰基，未取代或取代的氨基磺酰基或未取代或取代的磺酰基氨基; R 5是氢，烷基或卤素; l为0,1或2; R 8是氢，烷基，卤代烷基，烷基羰基，甲酰基，烷氧基羰基，卤代烷氧基羰基，烷基磺酰基或卤代烷基磺酰基; R 9是取代的吡唑-4-基羰基或取代的5-氧代吡唑啉-4-基亚甲基; 及其农业用盐; 制备三环苯甲酰基吡唑衍生物的方法和中间体; 描述了包含它们的组合物以及这些衍生物或包含它们的组合物用于防治不期望的植物的用途。

    Synthesis of functionalized macrocycles by ring closing metathesis
    9.
    发明授权
    Synthesis of functionalized macrocycles by ring closing metathesis 失效
    通过闭环复分解合成官能化大环

    公开(公告)号：US5936100A

    公开(公告)日：1999-08-10

    申请号：US767561

    申请日：1996-12-16

    申请人： Alois Furstner ,  Klaus Langemann ,  Nicole Kindler

    发明人： Alois Furstner ,  Klaus Langemann ,  Nicole Kindler

    IPC分类号： C07C45/67 ,  C07C45/69 ,  C07C49/587 ,  C07D225/02 ,  C07D273/00 ,  C07D313/00 ,  C07D321/00 ,  C07D339/08 ,  C07C45/65 ,  C07D49/587

    CPC分类号： C07D339/08 ,  C07C45/673 ,  C07C45/69 ,  C07C49/587 ,  C07D225/02 ,  C07D273/00 ,  C07D313/00 ,  C07D321/00

    摘要： The invention concerns an improved process for the preparation of macrocyclic products with 12 or more ring atoms containing one or more polar functional groups on the ring and/or one or more heteroatoms within the ring by ring closing metathesis (RCM) of suitably substituted diene precursors even if the substrates are devoid of any kind of conformational preorganization. Metal carbene complexes of Ru, Mo, W, Re, Os, which are tolerant towards the respective functional group and can either be isolated or prepared in situ are used as catalysts or catalyst precursors. Preferred catalysts or catalyst precursors are ruthenium complexes of the general type XX.sub.1 LL.sub.1 Ru.dbd.CRR.sub.1, wherein X, X.sub.1 =halogen, L, L.sub.1 =trialkylphosphine, R, R1=H, Ph, CH.dbd.CPh.sub.2 denote the most preferred embodiment. The process can be applied to the synthesis of olfactory compounds, perfumary ingredients, pheromones, crown ethers, antibiotics and pharmaceuticals for human and veterinary medicine.

    摘要翻译： 本发明涉及一种用于制备具有12个或更多个环原子的大环产物的改进方法，该环原子在环中具有一个或多个极性官能团和/或环内的一个或多个杂原子，通过闭环复分解（RCM）适当取代的二烯前体 即使基材没有任何种类的构象预组织。 用作催化剂或催化剂前体的Ru，Mo，W，Re，Os的金属碳烯配合物可以各自的官能团耐受并且可以原位分离或制备。 优选的催化剂或催化剂前体是通式XX1LL1Ru = CRR1的钌络合物，其中X，X1 =卤素，L，L1 =三烷基膦，R，R1 = H，Ph，CH = CPh2表示最优选的实施方案。 该方法可应用于嗅觉化合物，香料成分，信息素，冠醚，抗生素和人兽药等药物的合成。