Processes for preparing certain hexaazaisowurtzitanes and their use in preparing hexanitrohexaazaisowurtzitane
    1.
    发明授权
    Processes for preparing certain hexaazaisowurtzitanes and their use in preparing hexanitrohexaazaisowurtzitane 有权
    制备某些六氮杂异纤锌矿型结构烷烃的方法及其在制备六硝基六氮杂异纤锌矿型结构烷烃

    公开(公告)号:US08268993B1

    公开(公告)日:2012-09-18

    申请号:US12976605

    申请日:2010-12-22

    申请人: Robert D. Chapman

    发明人: Robert D. Chapman

    IPC分类号: C07D255/00

    CPC分类号: C07D487/22

    摘要: A heavy-metal-free sequence leading to a superior, more economical, and scalable process for the high efficiency conversion of hexaallylhexaazaisowurtzitane (HAllylIW) to hexanitrohexaazaisowurtzitane (CL-20).

    摘要翻译: 一种无重金属的顺序,导致六烯丙基六氮杂异纤锌矿型结构烷烃(HAllylIW)高效转化为六硝基六氮杂异纤锌矿型结构烷烃(CL-20)的优越,更经济和可扩展的工艺。

    Method and apparatus for treating freshly metallized substrates
    2.
    发明授权
    Method and apparatus for treating freshly metallized substrates 失效
    用于处理新鲜金属化基材的方法和设备

    公开(公告)号:US5451429A

    公开(公告)日:1995-09-19

    申请号:US292865

    申请日:1994-08-19

    申请人: Robert D. Chapman

    发明人: Robert D. Chapman

    CPC分类号: C23C2/26 C23C2/22

    摘要: A method and apparatus for treating a freshly metallized substrate in which a metal substrate is passed through a bath of molten metal for the purpose of applying a coating thereto while a treating gas containing a reducing gas, a non-oxidizing gas or combination thereof is provided at the region where the metallized substrate exits the molten metal bath to thereby at least reduce oxidation of the metallized substrate and the surface of the molten metal bath.

    摘要翻译: 提供一种用于处理新金属化基板的方法和装置,其中金属基板通过熔融金属浴以便施加涂层,同时提供含有还原气体,非氧化性气体或其组合的处理气体 在金属化衬底离开熔融金属浴的区域,从而至少减少金属化衬底和熔融金属浴表面的氧化。

    3,3,7,7-tetrakis(difluoramino)octahydro-1,5-diazocinium salts
    3.
    发明授权
    3,3,7,7-tetrakis(difluoramino)octahydro-1,5-diazocinium salts 有权
    3,3,7,7-四(二氟氨基)八氢-1,5-二氮杂鎓盐

    公开(公告)号:US08444783B1

    公开(公告)日:2013-05-21

    申请号:US12479278

    申请日:2009-06-05

    IPC分类号: C06B45/00 D03D23/00 D03D43/00

    CPC分类号: C07D245/02

    摘要: 3,3,7,7-Tetrakis(difluoramino)octahydro-1,5-diazocinium intermediate salts through difluoramination followed by N-denosylation or N-deprotection, which are valuable for use as precursor(s) to HNFX as well as to other members of the rare class of 3,3,7,7-tetrakis(difluoramino)octahydro-1,5-diazocines.

    摘要翻译: 3,3,7,7-四(二氟氨基)八氢-1,5-二氮杂鎓中间体盐,通过二氟化,然后进行N-去甲硅烷基化或N-去保护,这对HNFX以及其他 稀有类3,3,7,7-四(二氟氨基)八氢-1,5-二氮杂辛的成员。

    Processes for preparing certain hexaazaisowurtzitanes and their use in preparing hexanitrohexaazaisowurtzitane
    4.
    发明授权
    Processes for preparing certain hexaazaisowurtzitanes and their use in preparing hexanitrohexaazaisowurtzitane 有权
    制备某些六氮杂异纤锌矿型结构烷烃的方法及其在制备六硝基六氮杂异纤锌矿型结构烷烃

    公开(公告)号:US08268991B1

    公开(公告)日:2012-09-18

    申请号:US12022930

    申请日:2008-01-30

    IPC分类号: C07D487/00

    CPC分类号: C07D487/22

    摘要: The present invention describes a novel heavy-metal-free sequence leading to a superior, more economical, and scalable process for the high efficiency conversion of hexaallylhexaazaisowurtzitane (HAllylIW) to hexa(1-propenyl)hexaazaisowurtzitane (HPIW) and hence via reaction with singlet oxygen and subsequent nitrolysis to hexanitrohexaazaisowurtzitane (CL-20).

    摘要翻译: 本发明描述了一种新的无重金属顺序,导致六烯丙基六氮杂异纤锌矿型结构烷烃(HAllylIW)与六(1-丙烯基)六氮杂异纤锌矿型结构烷烃(HPIW)的高效转化并因此通过与单线态反应的优异,更经济和可扩展的方法 氧和随后的硝基分解到六硝基六氮杂异纤锌矿型结构烷烃(CL-20)。

    Process for employing HNFX as a biocidal explosive
    5.
    发明授权
    Process for employing HNFX as a biocidal explosive 有权
    使用HNFX作为杀生物剂的方法

    公开(公告)号:US08221566B1

    公开(公告)日:2012-07-17

    申请号:US12615918

    申请日:2009-11-10

    申请人: Robert D. Chapman

    发明人: Robert D. Chapman

    IPC分类号: D03D23/00 D03D43/00

    CPC分类号: A01N25/20 A01N59/00 A01N59/10

    摘要: A process of making detonation products having an effect on biological agents, providing an effective amount of HNFX; combining HNFX with an additive; detonating the combination with a detonation device; creating detonation products from the combination; contacting the detonation products with the harmful agents; exposing the detonation products for about at least 2 seconds to harmful agents; and destroying the harmful agents.

    摘要翻译: 制造对生物制剂有影响的爆炸产物,提供有效量的HNFX的方法; 结合HNFX与添加剂; 用爆震装置引爆组合; 从组合中产生爆炸产物; 将爆炸产物与有害物质接触; 将爆炸产物暴露于有害物质中至少2秒钟; 并破坏有害物质。

    Octafluoropentaerythrityltetramine (octafluoro-peta) and process for its preparation
    6.
    发明授权
    Octafluoropentaerythrityltetramine (octafluoro-peta) and process for its preparation 有权
    八氟五季戊四醇(八氟 - peta)及其制备方法

    公开(公告)号:US08008527B1

    公开(公告)日:2011-08-30

    申请号:US12496962

    申请日:2009-07-02

    IPC分类号: C07C291/00

    CPC分类号: C07C239/04

    摘要: A composition and method of manufacturing the same. Embodiments of an aspect of the invention relate to the formula C(CH2NF2)4 having the name octafluoropentaerythrityltetramine (octafluoro-PETA). In embodiments of another aspect generally relate to a method for manufacturing octafluoropentaerythrityltetramine (octafluoro-PETA) including, basifying pentaerythrityltetramine tetrahydrochloride in an aqueous solution with an aqueous alkali and treating with alkyl chloroformate for producing a tetraalkyl pentaerythrityltetra carbamate, extracting the compound into a nonaqueous solvent suitable for extraction from water and removing the solvent for providing a pure form of tetraethyl pentaerythrityltetracarbamate, bubbling elemental fluorine and/or mixtures of fluorine with an inert gas through tetraalkyl pentaerythrityltetracarbamate in a solvent suitable for direct fluorinations of protected amines until excess fluorine appears, and purifying the resultant octafluoropentaerythrityltetramine.

    摘要翻译: 一种组合物及其制造方法。 本发明的一个方面的实施方案涉及具有名称八氟五甲基四胺(octadecluoro-PETA)的式C(CH 2 NF 2)4。 在另一方面的实施方案中,一般涉及制备八氟季戊四醇四胺(八氟-PETA)的方法,其包括在含水碱的水溶液中碱化季戊四醇四胺盐酸盐,并用氯甲酸烷基酯处理以制备四烷基季戊四醇四氨基甲酸酯,将该化合物萃取到非水溶剂 适用于从水中萃取并除去溶剂以提供纯形式的四乙基季戊四醇四氨基甲酸盐,在适用于直接氟化被保护的胺直到氟出现的溶剂中,将元素氟和/或氟与惰性气体的混合物通过四烷基季戊四醇四氨基甲酸四烷基季铵式四氨基甲酸铵鼓泡, 纯化所得的八氟季戊四醇四胺。

    Poster supporting frame
    7.
    发明授权
    Poster supporting frame 失效
    海报支持框架

    公开(公告)号:US4176480A

    公开(公告)日:1979-12-04

    申请号:US867834

    申请日:1978-01-09

    摘要: A device for use in maintaining a poster or like sheet decorative material in a flat configuration by removably engaging narrow marginal edge portions thereof, and as a result no portion of the decorative insignia on the poster being concealed from view when supported by the device. The device when not in use may be dismantled and the components thereof stored side-by-side in a compact configuration until again needed.

    摘要翻译: 一种用于通过可移除地接合其窄边缘部分而将平板结构中的海报或类似的装饰材料维持在其中的装置,并且因此当由装置支撑时,海报上的装饰徽章的部分不被隐藏。 不使用时的装置可以被拆卸,其组件以紧凑的配置并排存储,直到再次需要。