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公开(公告)号：US4271279A
公开(公告)日：1981-06-02
申请号：US688874
申请日：1976-05-21
Applicant: Ronald L. Pastorino , Roger N. Lewis , Charles B. Abma
Inventor： Ronald L. Pastorino , Roger N. Lewis , Charles B. Abma
IPC: C07D323/00 , C08K5/159 , C08F8/06
CPC classification number: C07D323/00 , C08K5/159
Abstract: High density polyethylene is cross-linked with certain cyclic perketals including a group of novel cyclic perketals. Typical of the novel molecules is 3,6,6,9,9-pentamethyl-3-ethylacetate-1,2,4,5-tetraoxy cyclononane.
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2.发明授权Novel method of crosslinking/foaming of low density polyethylene using linear peroxyketals 失效使用线性过氧化缩酮的低密度聚乙烯的交联/发泡的新方法
公开(公告)号：US4330495A
公开(公告)日：1982-05-18
申请号：US237200
申请日：1981-02-23
Applicant: Reidar Halle , Roger N. Lewis , John R. Muenchow
Inventor： Reidar Halle , Roger N. Lewis , John R. Muenchow
CPC classification number: C08J9/08 , C08J9/10 , C08J2323/04 , Y10S264/05 , Y10S264/18
Abstract: A novel method of making foamed, crosslinked low density polyethylene utilizing as dual crosslinking/blowing agents, organic peroxides of the formula: ##STR1## where each R is a t-alkyl group bonded through its tertiary carbon atom and having 4-8 carbon atoms; and R' is an alkyl group of 1-6 carbon atoms.
Abstract translation: 一种利用双交联/发泡剂制备泡沫交联的低密度聚乙烯的新方法，下式的有机过氧化物：其中每个R是通过其叔碳原子键合并具有4-8个碳原子的叔烷基 ; 并且R'是1-6个碳原子的烷基。
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3.发明授权2-Chloro-2-alkyl substituted asymmetrical diacyl peroxides and polymerization process using same 失效2-氯-2-烷基取代的不对称二酰基过氧化物和使用其的聚合方法
公开(公告)号：US4307217A
公开(公告)日：1981-12-22
申请号：US241161
申请日：1981-03-06
Applicant: Reidar Halle , David Peterson , Roger N. Lewis
Inventor： Reidar Halle , David Peterson , Roger N. Lewis
Abstract: Dialkyl diacyl peroxides in which the alpha carbon atom of one of the alkyl groups is secondary and substituted by chloro and alkyl. The compounds are useful as polymerization initiators of ethylenically unsaturated monomers such as vinyl chloride.
Abstract translation: 二烷基二酰基过氧化物，其中一个烷基的α碳原子是仲的并被氯和烷基取代。 该化合物可用作烯属不饱和单体如氯乙烯的聚合引发剂。
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4.发明授权
公开(公告)号：US4267109A
公开(公告)日：1981-05-12
申请号：US929160
申请日：1978-07-31
Applicant: Pastorino, Ronald L. , Roger N. Lewis
Inventor： Pastorino, Ronald L. , Roger N. Lewis
IPC: C07D323/00
CPC classification number: C07D323/00 , C08K5/159
Abstract: High density polyethylene is cross-linked with certain cyclic perketals including a group of novel cyclic perketals. Typical of the novel molecules is 3,6,6,9,9-pentamethyl-3-ethylacetate-1,2,4,5-tetraoxy cyclononane.
Abstract translation: 高密度聚乙烯与某些包括一组新型环状胃肠缩酮的环状胃肠素交联。 典型的新型分子是3,6,6,9,9-五甲基-3-乙基乙酸酯-1,2,4,5-四氧基环壬烷。
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5.发明授权Thermally stable high molecular weight acyl peroxycarbonic esters in polyester curing 失效聚酯固化中热稳定的高分子量酰基过氧碳酸酯
公开(公告)号：US4129613A
公开(公告)日：1978-12-12
申请号：US817634
申请日：1977-07-21
Applicant: Roger N. Lewis , Ronald L. Pastorino , James F. Wilts
Inventor： Roger N. Lewis , Ronald L. Pastorino , James F. Wilts
IPC: C08F4/00 , C07C67/00 , C07C407/00 , C07C409/32 , C07C409/34 , C08F2/00 , C08F2/50 , C08F4/28 , C08F4/34 , C08F299/04 , C08K5/14 , C08L67/06
CPC classification number: C08K5/14 , C08F299/045 , C08F4/34
Abstract: Acyl peroxycarbonic esters of the formula ##STR1## in which R is methyl or ethyl, R' is alkyl, and R and R' together have 17 or more carbon atoms. The compounds have unusual thermal stability, together with improved polymerization initiating efficiency. Particularly outstanding efficiency is found in connection with the curing of polyester resins.
Abstract translation: 式“IMAGE”的酰基过氧碳酸酯，其中R是甲基或乙基，R'是烷基，R和R'共有17个或更多个碳原子。 这些化合物具有不寻常的热稳定性，同时提高了聚合引发效率。 与聚酯树脂的固化有关的特别突出的效率。
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Patent Agency Ranking6.发明授权T-Alkyl peresters of t-hydroperoxides catalysts for polymerization of unsaturated monomers 失效用于不饱和单体聚合的叔丁基过氧化氢催化剂的T型烷基酯
公开(公告)号：US4063013A
公开(公告)日：1977-12-13
申请号：US791819
申请日：1977-04-28
Applicant: Ronald L. Friedman , Roger N. Lewis
Inventor： Ronald L. Friedman , Roger N. Lewis
IPC: C08F2/00 , C08F4/34 , C08F4/28 , C08F14/06 , C08F110/02
CPC classification number: C08F4/34
Abstract: Novel tertiary alkyl peresters of tertiary hydroperoxides are used as polymerization initiators wherein the peresters are characterized by the tertiary alkyl group of the acid moiety having at least two alkyl groups of two or more carbon atoms and the tertiary alkyl group of the hydroperoxide has at least five carbon atoms. Typical is the polymerization of certain vinyl monomers such as vinyl chloride.
Abstract translation: 使用叔氢过氧化物的新型叔烷基过酸酯作为聚合引发剂，其中过酸酯的特征在于酸部分的叔烷基具有至少两个具有两个或更多个碳原子的烷基，并且氢过氧化物的叔烷基具有至少五个 碳原子。 典型的是某些乙烯基单体如氯乙烯的聚合。
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公开(公告)号：US4051310A
公开(公告)日：1977-09-27
申请号：US696463
申请日：1976-06-16
Applicant: Roger N. Lewis , Ronald L. Pastorino , James F. Wilts
Inventor： Roger N. Lewis , Ronald L. Pastorino , James F. Wilts
IPC: C08F4/00 , C07C67/00 , C07C407/00 , C07C409/32 , C07C409/34 , C08F2/00 , C08F2/50 , C08F4/28 , C08F4/34 , C08F299/04 , C08K5/14 , C08F20/10 , C08G63/12 , C08G77/04
CPC classification number: C08K5/14 , C08F299/045 , C08F4/34
Abstract: Acyl peroxycarbonic esters of the formula ##STR1## in which R is methyl or ethyl, R' is alkyl, and R and R' together have 17 or more carbon atoms. The compounds have unusual thermal stability, together with improved polymerization initiating efficiency. Particularly outstanding efficiency is found in connection with the polymerization of methyl methacrylate.
Abstract translation: 式“IMAGE”的酰基过氧碳酸酯，其中R是甲基或乙基，R'是烷基，R和R'一起具有17个或更多个碳原子。 这些化合物具有不寻常的热稳定性，同时提高了聚合引发效率。 与甲基丙烯酸甲酯的聚合有关的特别突出的效率。
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8.发明授权Alpha halo substituted peroxyesters and their use as polymerization initiators 失效α卤代取代的过氧酯和它们作为聚合引发剂的用途
公开(公告)号：US4051167A
公开(公告)日：1977-09-27
申请号：US642432
申请日：1975-12-19
Applicant: Roger N. Lewis
Inventor： Roger N. Lewis
IPC: C07C409/38 , C08F4/34 , C08F299/04 , C07C179/18 , C08L67/06
CPC classification number: C08F4/34 , C07C409/38 , C08F299/045
Abstract: Aliphatic peroxyester polymerization initiators whose thermal stability is controlled by a bromine or chlorine substituent on the carbon atom in the alpha position relative to the carbonyl group in the acid moity of the perester. The initiators show increased efficiency for the polymerization of methyl methacrylate, styrene, ethylene, and in curing unsaturated polyester resins. Typical is 1,1,3,3-tetramethyl butyl peroxy 2-chlorolaurate.
Abstract translation: 脂肪族过氧酯聚合引发剂，其热稳定性通过在过酸酯的酸性中相对于羰基的α位置上的碳原子上的溴或氯取代基来控制。 引发剂显示提高甲基丙烯酸甲酯，苯乙烯，乙烯和固化不饱和聚酯树脂的聚合效率。 典型的是1,1,3,3-四甲基丁基过氧化2-氯代牛油酸酯。
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9.发明授权Process for crosslinking thermoplastic polymers and crosslinking system used therein 失效用于交联热塑性聚合物和交联体系的方法
公开(公告)号：US5856412A
公开(公告)日：1999-01-05
申请号：US850334
申请日：1997-05-02
Applicant: Lawrence A. Bock , Roger N. Lewis
Inventor： Lawrence A. Bock , Roger N. Lewis
IPC: C08J3/24 , C07C409/00 , C08F8/00 , C08L23/30 , C08F8/06
CPC classification number: C08F8/00
Abstract: A crosslinking system which includes a 1,2,4-trioxacycloheptane and a crosslink-promoting polyfunctional ethylenically unsaturated compound. This system is employed in a process of crosslinking a thermoplastic polymer. Preferred polymers, useful in this process, include ethylene homopolymers and copolymers.
Abstract translation: 交联体系，其包括1,2,4-三氧杂环庚烷和交联促进多官能烯属不饱和化合物。 该系统用于交联热塑性聚合物的方法。 在该方法中有用的优选聚合物包括乙烯均聚物和共聚物。
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公开(公告)号：US4279831A
公开(公告)日：1981-07-21
申请号：US65410
申请日：1979-08-10
Applicant: Reidar Halle , David Peterson , Roger N. Lewis
Inventor： Reidar Halle , David Peterson , Roger N. Lewis
IPC: C07C409/34 , C08F4/34 , C07C179/14
CPC classification number: C08F4/34 , C07C409/34
Abstract: Dialkyl diacyl peroxides in which the alpha carbon atom of one of the alkyl groups is secondary and substituted by chloro and alkyl. The compounds are useful as polymerization initiators of ethylenically unsaturated monomers such as vinyl chloride.
Abstract translation: 二烷基二酰基过氧化物，其中一个烷基的α碳原子是仲的并被氯和烷基取代。 该化合物可用作烯属不饱和单体如氯乙烯的聚合引发剂。
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