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    ODOR SAMPLES OF PEROXIDIC EXPLOSIVES
    5.
    发明申请
    ODOR SAMPLES OF PEROXIDIC EXPLOSIVES 有权
    过氧化物爆炸物的气味样品

    公开(公告)号：US20120090744A1

    公开(公告)日：2012-04-19

    申请号：US13378049

    申请日：2010-06-18

    申请人： Siegfried Waldvogel ,  Carsten Siering ,  Daniel Lubczyk ,  Joerg Loebau ,  Arno Hahma

    发明人： Siegfried Waldvogel ,  Carsten Siering ,  Daniel Lubczyk ,  Joerg Loebau ,  Arno Hahma

    IPC分类号： C06B23/00

    CPC分类号： C06B23/00 ,  C07C407/00 ,  C07C407/006 ,  C07C2601/14 ,  C07C409/20 ,  C07C409/34

    摘要： The present invention provides a method of using a neutral ionic liquid to at least one of stabilize a peroxidic explosive and to produce a stable solution of the peroxidic explosive which includes providing the neutral ionic liquid and using the neutral ionic liquid to at least one of stabilize the peroxidic explosive and to produce the stable solution of the peroxidic explosive. The present invention further provides a stable composition which includes a solution of at least one neutral ionic liquid and a detectable amount of a peroxidic explosive, a method of production thereof, and a method of use thereof as an odor sample.

    摘要翻译： 本发明提供一种使用中性离子液体至少稳定过氧化物爆炸物并产生稳定的过氧化物炸药溶液的方法，其包括提供中性离子液体并使用中性离子液体至少稳定一种 过氧化物炸药并产生稳定的过氧化物炸药溶液。 本发明还提供一种稳定的组合物，其包括至少一种中性离子液体和可检测量的过氧化物炸药的溶液，其制备方法及其作为气味样品的使用方法。

    Method for producing organic peroxides and their use in the radical polymerization of monomers
    8.
    发明申请
    Method for producing organic peroxides and their use in the radical polymerization of monomers 有权
    生产有机过氧化物的方法及其在单体自由基聚合中的应用

    公开(公告)号：US20040249097A1

    公开(公告)日：2004-12-09

    申请号：US10430719

    申请日：2003-05-06

    发明人： Ross J. Cozens ,  Qi Wang ,  M. Frederick V. Glock JR. ,  Daniel A. Zust

    IPC分类号： C08F004/32

    CPC分类号： C08F4/34 ,  C07C407/00 ,  C08F12/04 ,  G01S7/034 ,  H01Q3/24 ,  Y10S526/91 ,  Y10S526/911 ,  Y10S526/932 ,  C07C409/34 ,  C07C409/16 ,  C07C409/38 ,  C07C409/32

    摘要： A process for producing organic peroxide initiators useful in the polymerization of ethylenically unsaturated monomers. The process for making the organic peroxides includes forming an aqueous emulsion of the organic peroxide. The organic peroxide is dispersed as small droplets of from 1 to 10 microns in size in the aqueous emulsion. The organic peroxide may be added to a polymerization reactor containing an ethylenically unsaturated monomer. The organic peroxide functions as a free radical initiator to polymerize the monomer. The organic peroxide may be substantially free of organic solvents and plasticizers. The resulting polymers are of high quality.

    摘要翻译： 一种可用于烯属不饱和单体聚合的有机过氧化物引发剂的方法。 制备有机过氧化物的方法包括形成有机过氧化物的水性乳液。 有机过氧化物在水乳液中分散为1至10微米的小液滴。 可以将有机过氧化物加入到含烯属不饱和单体的聚合反应器中。 有机过氧化物用作自由基引发剂以使单体聚合。 有机过氧化物可以基本上不含有机溶剂和增塑剂。 所得聚合物质量高。

    Peroxide compositions with reactive diluents
    9.
    发明申请
    Peroxide compositions with reactive diluents 失效
    具有活性稀释剂的过氧化物组合物

    公开(公告)号：US20040094744A1

    公开(公告)日：2004-05-20

    申请号：US10451049

    申请日：2003-12-08

    发明人： Jan H Udding ,  Agnes E Wolters ,  Heinz Wilhelm ,  Armin Pfeil ,  Thomas Burgel ,  Lutz Sager

    IPC分类号： C09K003/00

    CPC分类号： C07C407/006 ,  C07C407/00 ,  C08F4/32 ,  C07C409/22 ,  C07C409/38 ,  C07C409/34 ,  C07C409/10

    摘要： The invention relates to peroxide compositions comprising a reactive diluent for the peroxide, wherein the diluent is either a component containing one or more vinyl ether group(s) and having a monomeric structure according to formula 1 (AnullCHnullCHnullO)nnullR, or is a suitable resinous compound comprising, in a covalently built-in manner, a component containing one or more vinyl ether group(s). In the formula A represents hydrogen or an alkyl group with 1-3 C atoms, and individual A groups may be different R either represents an aliphatic group, optionally branched, with 1-20 C atoms, etc. or represents a polyethylene or polypropylene glycol with 2 to 120 glycol units, etc. and n is 1, 2, 3 or 4. The resinous compounds comprising, in a covalently built-in manner, a component containing one or more vinyl ether group(s)are obtained by reaction of: a) a first compound (the HVE-compound) containing at least one hydroxyl group and at least one vinyl ether group, and b) a second compound (the D/HIC-compound), being an isocyanate, reacting with formation of one or more urethane group(s), and c) a third compound (the G/P/HP-compound) chosen from the groups of (1) C2-6 glycols, (2) C5-20 polyols having 2-5 hydroxyl groups and (3) hydroxyl terminated polyester compounds, not being alkyd resins, having 1-5 free hydroxyl groups and from 2-50 monomeric ester units (the G/P/HP-compound), or mixtures thereof. The invention also relates to the preparation of such compositions and to the use of such reactive diluents for peroxides in radically curing of unsaturated polyester resins for structural applications.

    摘要翻译： 本发明涉及包含用于过氧化物的反应性稀释剂的过氧化物组合物，其中稀释剂是含有一个或多个乙烯基醚基团且具有根据式1的单体结构（A-CH = CH-O）nR 或者是合适的树脂化合物，其以共价内置的方式包含含有一个或多个乙烯基醚基团的组分。 式A表示氢或具有1-3个C原子的烷基，各个A基团可以不同，R表示任选支链的1-20个C原子的脂族基团等，或代表聚乙烯或聚丙二醇 2〜120个二醇单元等，n为1,2,3或4.含有一个或多个乙烯基醚基的成分以共价内置的方式包含的树脂化合物是通过 ：a）含有至少一个羟基和至少一个乙烯基醚基团的第一化合物（HVE-化合物），和b）作为异氰酸酯的第二化合物（D / HIC-化合物）与形成一个 或更多的氨基甲酸酯基团，和c）选自（1）C 2-6二元醇，（2）具有2-5个羟基的C5-20多元醇的第三化合物（G / P / HP-化合物） 和（3）羟基封端的聚酯化合物，不是醇酸树脂，具有1-5个游离羟基和2-50个单体酯单元（G / P / HP-化合物），o r混合物。 本发明还涉及这种组合物的制备以及这种反应性稀释剂在不饱和聚酯树脂的自由基固化中用于结构应用的过氧化物的用途。

    Process for preparing peroxides using mixed anhydrides
    10.
    发明申请
    Process for preparing peroxides using mixed anhydrides 审中-公开
    使用混合酸酐制备过氧化物的方法

    公开(公告)号：US20040049070A1

    公开(公告)日：2004-03-11

    申请号：US10616007

    申请日：2003-07-09

    发明人： Johannes Willibrordus A. Overkamp ,  Marinus Catharinus Tammer ,  Bernard De Vries ,  Anna Gerdine Van de Bovenkamp-Bouwman

    IPC分类号： C07C409/24

    CPC分类号： C07C69/96 ,  C07C409/24 ,  C07C409/34 ,  C07C409/38 ,  C07C2601/14

    摘要： The invention relates to a process for the preparation of a peracid, perester or diacylperoxide and is characterized in that a mixed anhydride of formula R1nullC(O)OC(O)OR2nulln or nullR3C(O)OC(O)OnullpR4 is contacted with a hydroperoxide of formula R5nullOOHnullm in the presence of a base, wherein R1 represents a mono-, di-, tri- or tetravalent C1-C19 hydrocarbon group, optionally containing one or more hetero atoms, n is 1-4, R2 represents a C1-C20 hydrocarbon group, optionally containing one or more hetero atoms, R3 represents a C1-C19 hydrocarbon group, optionally containing one or more hetero atoms, R4 represents a di-, tri- or tetravalent C1-C20 hydrocarbon group, optionally containing one or more hetero atoms, p is 2-4, R5 represents hydrogen or a mono- or divalent C3-C18 tertiary alkyl or C2-C20 acyl group, in which the tertiary alkyl or acyl group may optionally contain one or more hetero atoms, m is 1 or 2, and if R5 represents hydrogen, m is 1, provided that if the hydroperoxide is an null,nullnull-dihydroperoxyperoxide, the reaction is not carried out in an inert two-phase solvent system comprising a polar solvent and an apolar solvent. The invention also relates to a hydroxyperacid, hydroxyperester, and hydroxydiacylperoxide obtainable by said process and the use of said hydroxyperoxides.

    摘要翻译： 本发明涉及一种制备过酸，过氧化物或二酰基过氧化物的方法，其特征在于式R 1 [C（O）OC（O）OR 2] n或[R 3 在碱的存在下，将C（O）OC（O）O] p R 4与式R 5 [OOH] m的氢过氧化物接触，其中R 1表示单 - ，二 - 任选含有一个或多个杂原子的三价或四价C 1 -C 19烃基，n为1-4，R 2表示任选含有一个或多个杂原子的C 1 -C 20烃基，R 3表示 任选含有一个或多个杂原子的C 1 -C 19烃基，R 4表示任选含有一个或多个杂原子的二价，三价或四价C 1 -C 20烃基，p是2-4，R 5 >表示氢或一价或二价C 3 -C 18叔烷基或C 2 -C 20酰基，其中叔烷基或酰基可任选地含有一个或多个杂原子，m为1或2，如果R 5为 代表氢，m是1，条件是如果是氢 过氧化物是α，α'-二氢过氧化氢，该反应不能在包含极性溶剂和非极性溶剂的惰性两相溶剂体系中进行。 本发明还涉及通过所述方法和所述羟基过氧化物的使用可获得的羟基过酸，羟基过氧化物和羟基过氧化氢。