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1.发明授权Adducts of epoxy resins and amino-substituted aromatic sulfonic acid amides 失效环氧树脂和氨基取代的芳香族磺酸酰胺的加合物
公开(公告)号：US4528359A
公开(公告)日：1985-07-09
申请号：US610896
申请日：1984-05-16
IPC分类号： C08L63/00 , C08G59/00 , C08G59/10 , C08G59/14 , C08G59/18 , C08G59/44 , C08G59/50 , C08G59/54
CPC分类号： C08G59/10 , C08G59/184 , C08G59/444 , C08G59/54
摘要： Resin compositions are prepared by reacting an epoxy resin with an amine-substituted aromatic sulfonic acid amide at a temperature up to about 130.degree. C. The resultant product can be cured by heating to a temperature of at least about 150.degree. C. in the presence of suitable curing agents and in some instances in the absence of any curing agent.
摘要翻译： 通过使环氧树脂与胺取代的芳族磺酸酰胺在高达约130℃的温度下反应来制备树脂组合物。所得产物可以在存在下加热至至少约150℃的温度来固化 的合适的固化剂，在某些情况下，在没有任何固化剂的情况下。
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公开(公告)号：US4370465A
公开(公告)日：1983-01-25
申请号：US330047
申请日：1981-12-14
CPC分类号： C08J5/24 , C08G59/066 , C08G59/688 , C08J2363/00 , Y10T428/31515 , Y10T428/31518
摘要： Epoxy resins having improved properties are prepared by reacting an epoxy resin with a dihydric phenol in the presence of a sufficient quantity of a phosphonium catalyst such that the product resulting from reacting a mixture of the catalyst, epoxy resin and dihydric phenol has a % epoxide difference from the theoretical percent epoxide of from about 0.5 to about 4.0.
摘要翻译： 具有改进性能的环氧树脂通过使环氧树脂与二元酚在足够量的鏻催化剂存在下反应制备，使得由催化剂，环氧树脂和二元酚的混合物反应得到的产物具有％的环氧化物差异 从约0.5至约4.0的理论环氧化物含量。
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3.发明授权Process for preparing epoxy resins having improved physical properties when cured using quaternary phosphonium catalysts 失效使用季鏻催化剂固化时具有改善的物理性能的环氧树脂的制备方法
公开(公告)号：US4352918A
公开(公告)日：1982-10-05
申请号：US212959
申请日：1980-12-04
IPC分类号： C08G20060101 , C08G59/00 , C08G59/06 , C08G59/14 , C08G59/18 , C08G59/62 , C08G59/68 , C08J5/24 , C08L63/00 , C08L63/02
CPC分类号： C08J5/24 , C08G59/066 , C08G59/688 , C08J2363/00
摘要： Epoxy resins having improved properties are prepared by reacting an epoxy resin with a dihydric phenol in the presence of a sufficient quantity of a phosphonium catalyst such that the product resulting from reacting a mixture of the catalyst, epoxy resin and dihydric phenol has a % epoxide difference from the theoretical percent epoxide of from about 0.5 to about 4.0.
摘要翻译： 具有改进性能的环氧树脂通过使环氧树脂与二元酚在足够量的鏻催化剂存在下反应制备，使得由催化剂，环氧树脂和二元酚的混合物反应得到的产物具有％的环氧化物差异 从约0.5至约4.0的理论环氧化物含量。
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4.发明授权Process for preparing resin impregnated substrates for use in preparing electrical laminates 失效制备用于制备电性层压板的树脂浸渍基材的方法
公开(公告)号：US4251594A
公开(公告)日：1981-02-17
申请号：US79282
申请日：1979-09-27
IPC分类号： B32B15/04 , B32B15/08 , B32B15/092 , B32B27/38 , C08G59/06 , C08J5/04 , C08J5/24 , H01B3/08 , H01B3/40 , H05K1/03
CPC分类号： C08J5/24 , C08G59/066 , H01B3/084 , H01B3/40 , C08J2363/00 , H05K1/0326 , Y10T428/31511
摘要： The preparation of substrates impregnated with epoxy resins and curing agents therefor is improved by employing as the epoxy resin one which has been prepared by reacting a low equivalent weight epoxy resin having an aliphatic halide content of at least about 500 ppm such as a diglycidyl ether of bisphenol A with a dihydric phenolic compound such as tetrabromo bisphenol A in the presence of an alkali metal hydroxide such as potassium hydroxide.
摘要翻译： 通过使用通过使用具有至少约500ppm的脂肪族卤化物含量的低当量环氧树脂使其制备的环氧树脂，例如二环氧基醚的二缩水甘油醚 双酚A与二羟基酚类化合物如四溴双酚A在碱金属氢氧化物如氢氧化钾的存在下反应。
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5.发明授权
公开(公告)号：US5276071A
公开(公告)日：1994-01-04
申请号：US15505
申请日：1993-02-09
CPC分类号： C08G59/14 , C08G59/066 , C08G59/226 , C09D5/4434
摘要： Cationic advanced resins are obtained by (I) reacting a composition comprising (A) an advanced epoxy resin composition comprising the product resulting from reacting a composition comprising (1) an aromatic hydroxyl-containing product resulting from reacting a composition comprising (a) at least one diglycidyl ether of (i) an oxyalkylated aromatic diol, or ii) at least one compound having two hydroxyl groups per molecule in which the hydroxyl groups are attached to an aliphatic or cycloaliphatic carbon atom and which compound is free of aromatic rings; or (iii) a combination of (i) and (ii); and (iv) optionally a diglycidyl ether compound different from (i) and (ii); and (b) at least one compound containing two aromatic hydroxyl groups per molecule; (2) at least one diglycidyl ether of a compound containing two aromatic groups per molecule; (3) optionally, one or more compounds containing two aromatic hydroxyl groups per molecule; and (4) optionally, a monofunctional capping agent; with (B) a nucleophilic compound; and (II) adding an organic acid and water at at least one point during the preparation of the cationic resin. The cationic advanced resins are useful in coating compositions.
摘要翻译： 阳离子高级树脂是通过以下方法获得的：（I）包含（A）包含由下述组分组成的高级环氧树脂组合物的高级环氧树脂组合物的组合物，所述组合物是使包含（1）含芳族羟基的产物与 （i）烷氧基化芳族二醇的一种二缩水甘油醚，或ii）至少一种每分子具有两个羟基的化合物，其中羟基连接到脂族或脂环族碳原子上，该化合物不含芳环; 或（iii）（i）和（ii）的组合; 和（iv）任选的不同于（i）和（ii）的二缩水甘油醚化合物; 和（b）至少一种每分子含有两个芳族羟基的化合物; （2）每分子含有两个芳族基团的化合物的至少一种二缩水甘油醚; （3）任选地，每个分子含有一个或多个含有两个芳族羟基的化合物; 和（4）任选的单官能封端剂; 与（B）亲核化合物; 和（II）在制备阳离子树脂期间至少一点加入有机酸和水。 阳离子高级树脂可用于涂料组合物。
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6.发明授权Epoxy resin advanced with polyphenol/oxyalkylated aromatic or cycloyaliphatic diglycidyl ether product 失效环氧树脂与多酚/烷氧基化芳族或环脂族二缩水甘油醚产品一起推进
公开(公告)号：US5334676A
公开(公告)日：1994-08-02
申请号：US121398
申请日：1993-09-14
CPC分类号： C08G59/14 , C08G59/066 , C08G59/226 , C09D5/4434
摘要： Advanced epoxy resin compositions are prepared by reacting a composition comprising (1) an aromatic hydroxyl-containing product resulting from reacting a composition comprising (a) at least one diglycidyl ether of (i) an oxyalkylated aromatic diol, or (ii) at least one compound having two hydroxyl groups per molecule in which the hydroxyl groups are attached to an aliphatic or cycloaliphatic carbon atom and which compound is free of aromatic rings; or (iii) a combination of (i) and (ii); and (iv) optionally a diglycidyl ether compound different from (i) and (ii); and (b) at least one compound containing two aromatic hydroxyl groups per molecule; (2) at least one diglycidyl ether of a compound containing two aromatic groups per molecule; (3) optionally, one or more compounds containing two aromatic hydroxyl groups per molecule; and (4) optionally, a monofunctional capping agent. The advanced resins are useful in coating compositions.
摘要翻译： 先进的环氧树脂组合物是通过使包含（1）含芳族羟基的产物的组合物反应来制备的，所述组合物是使包含（a）至少一种（i）烷氧基化芳族二醇的二缩水甘油醚，或（ii）至少一种 每分子具有两个羟基的化合物，其中羟基连接到脂族或脂环族碳原子上，该化合物不含芳环; 或（iii）（i）和（ii）的组合; 和（iv）任选的不同于（i）和（ii）的二缩水甘油醚化合物; 和（b）至少一种每分子含有两个芳族羟基的化合物; （2）每分子含有两个芳族基团的化合物的至少一种二缩水甘油醚; （3）任选地，每个分子含有一个或多个含有两个芳族羟基的化合物; 和（4）任选的单官能封端剂。 先进的树脂可用于涂料组合物中。
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7.再颁专利Process for preparing epoxy resins having improved physical properties when cured using quaternary phosphonium catalysts 失效使用季鏻催化剂固化时具有改善的物理性能的环氧树脂的制备方法
公开(公告)号：USRE32951E
公开(公告)日：1989-06-13
申请号：US509479
申请日：1983-06-30
CPC分类号： C08G59/066 , C08G59/688
摘要： Epoxy resins having improved properties are prepared by reacting an epoxy resin with a dihydric phenol in the presence of a sufficient quantity of a phosphonium catalyst such that the product resulting from reacting a mixture of the catalyst, epoxy resin and dihydric phenol has a % epoxide difference from the theoretical percent epoxide of from about 0.5 to about 4.0.
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8.发明授权Process for preparing epoxy resins having improved physical properties when cured 失效制备固化后具有改善的物理性能的环氧树脂的方法
公开(公告)号：US4410596A
公开(公告)日：1983-10-18
申请号：US330046
申请日：1981-12-14
CPC分类号： C08J5/24 , B32B27/04 , C08G59/066 , C08G59/688 , C08J2363/00 , Y10T428/31511 , Y10T428/31525
摘要： Epoxy resins having improved properties are prepared by reacting an epoxy resin with a dihydric phenol in the presence of a sufficient quantity of a phosphonium catalyst such that the product resulting from reacting a mixture of the catalyst, epoxy resin and dihydric phenol has a % epoxide difference from the theoretical percent epoxide of from about 0.5 to about 4.0.
摘要翻译： 具有改进性能的环氧树脂通过使环氧树脂与二元酚在足够量的鏻催化剂存在下反应制备，使得由催化剂，环氧树脂和二元酚的混合物反应得到的产物具有％的环氧化物差异 从约0.5至约4.0的理论环氧化物含量。
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公开(公告)号：US5212262A
公开(公告)日：1993-05-18
申请号：US516018
申请日：1990-04-27
CPC分类号： C08G59/14 , C08G59/066 , C08G59/226 , C09D5/4434
摘要： A composition useful as an electrodepositable coating comprises a curing agent and an advanced epoxy resin prepared by advancing a diglycidyl ether of a dihydric phenol with an aromatic hydroxyl-containing reaction product of a diglycidyl ether of an oxyalkylated dihydric phenol and/or a diglycidyl ether of a (cyclo) aliphatic diol, optionally with a dihydric phenol and/or a monofunctional capping agent, combined with a diglycidyl ether of a dihydric phenol.
摘要翻译： 可用作电可沉积涂料的组合物包括固化剂和通过使二元酚的二缩水甘油醚与含烷氧基化的二元酚的二缩水甘油醚和/或二环氧基醚的二缩水甘油醚的芳族羟基反应产物 任选具有二元酚和/或单官能封端剂的（环）脂族二醇，与二元酚的二缩水甘油醚组合。
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公开(公告)号：US4614788A
公开(公告)日：1986-09-30
申请号：US770138
申请日：1985-08-28
CPC分类号： C08G59/4071 , C08G59/504 , C08G59/72
摘要： Disclosed are thermosettable compositions comprising (A) an epoxy resin such as the diglycidyl ether of bisphenol A; (B) boron trifluoride complexed with a primary, secondary or tertiary amine such as monoethanolamine and (C) at least one cyclic or acyclic phosphazene having at least one pendant ##STR1## group wherein Z is an alkyl or an aryl group such as hexa(n-propylamino)cyclotriphosphazene.When cured, these compositions have an increased glass transition temperature (Tg) value as compared to a similar composition without the phosphazene compound.These compositions are useful in potting compositions, wet lay-up and pre-impregnated laminate, adhesive, molding, coating, casting, encapsulation, filament winding and transfer molding applications.
摘要翻译： 公开了可热固组合物，其包含（A）环氧树脂，例如双酚A的二缩水甘油醚; （B）与伯胺，仲胺或叔胺如单乙醇胺络合的三氟化硼和（C）至少一种具有至少一个侧基的基团的环状或无环磷腈，其中Z是烷基或芳基如六（ 正丙基氨基）环三磷腈。 当固化时，与没有磷腈化合物的类似组合物相比，这些组合物具有增加的玻璃化转变温度（Tg）值。 这些组合物可用于灌封组合物，湿铺层和预浸层压板，粘合剂，模塑，涂布，浇铸，封装，长丝缠绕和传递模塑应用。
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