摘要:
An instrument and method for high pressure microwave assisted chemistry are disclosed. The method includes the steps of applying microwave radiation to a sample in a sealed vessel while measuring the temperature of the sample and measuring the pressure generated inside the vessel and until the measured pressure reaches a designated set point, opening the vessel to release gases until the pressure inside the vessel reaches a lower designated set point, closing the vessel, and repeating the steps of opening the vessel at designated pressure set points and closing the vessel at designated pressure set points to the sample until the sample reaction reaches a designated high temperature. The designated set points can controllably differ from one another as the reaction proceeds. Microwave energy can be applied continuously or intermittently during the opening and closing steps. The apparatus includes a microwave cavity, a microwave transparent pressure resistant reaction vessel in the cavity, a cap on the reaction vessel, a pressure sensor for measuring pressure in the vessel, a temperature sensor, and means for opening and closing the cap at predetermined pressure set points measured by the pressure sensor to release pressure from the vessel.
摘要:
A processor complex architecture facilitates accurate passing of transient data among processor complex stages of a pipelined processing engine. The processor complex comprises a central processing unit (CPU) coupled to an instruction memory and a pair of context data memory structures via a memory manager circuit. The context memories store transient “context” data for processing by the CPU in accordance with instructions stored in the instruction memory. The architecture further comprises data mover circuitry that cooperates with the context memories and memory manager to provide a technique for efficiently passing data among the stages in a manner that maintains data coherency in the processing engine. An aspect of the architecture is the ability of the CPU to operate on the transient data substantially simultaneously with the passing of that data by the data mover.
摘要:
An instrument and method for high pressure microwave assisted chemistry are disclosed. The method includes the steps of applying microwave radiation to a sample in a sealed vessel while measuring the temperature and pressure generated inside the vessel and until the measured pressure reaches a designated set point, opening the vessel to release gases until the pressure inside the vessel reaches a lower set point, closing the vessel, and repeating the steps of opening the vessel at designated pressure set points and closing the vessel at designated pressure set points to the sample until the sample reaction reaches a designated high temperature. Microwave energy can be applied continuously or intermittently during the opening and closing steps. Among other items, the instrument includes pressure and temperature sensors and means for opening and closing the vessel at the set points.
摘要:
A programmable processing engine processes transient data within an intermediate network station of a computer network. The engine comprises an array of processing elements symmetrically arrayed as rows and columns, and embedded between input and output buffer units with a plurality of interfaces from the array to an external memory. The external memory stores non-transient data organized within data structures, such as forwarding and routing tables, for use in processing the transient data. Each processing element contains an instruction memory that allows programming of the array to process the transient data as processing element stages of baseline or extended pipelines operating in parallel.
摘要:
A processor complex architecture facilitates accurate passing of transient data among processor complex stages of a pipelined processing engine. The processor complex comprises a central processing unit (CPU) coupled to an instruction memory and a pair of context data memory structures via a memory manager circuit. The context memories store transient “context” data for processing by the CPU in accordance with instructions stored in the instruction memory. The architecture further comprises data mover circuitry that cooperates with the context memories and memory manager to provide a technique for efficiently passing data among the stages in a manner that maintains data coherency in the processing engine. An aspect of the architecture is the ability of the CPU to operate on the transient data substantially simultaneously with the passing of that data by the data mover.
摘要:
A synchronization and control system for an arrayed processing engine of an intermediate network station comprises sequencing circuitry that controls the processing engine. The processing engine generally includes a plurality of processing element stages arrayed as parallel pipelines. The control system further includes an input header buffer (IHB) and an output header buffer (OHB), the latter comprising circuitry for receiving current transient data processed by the pipelines and for decoding control signals to determine a destination for the processed data. One destination is a feedback path that couples the OHB to the IHB and returns the processed data to the IHB for immediate loading into an available pipeline.
摘要:
A system and method are provided that permit an accurate checksum to be generated of a block of data being transmitted via a prefetched bus, despite repeated transmissions of identical portions of the block and presentation of those identical to checksum logic simultaneously with their transmission by the bus, by ensuring that only those portions of the data block that have yet to be checksummed are checksummed.
摘要:
A parallel processor is provided that includes integrated debugging capabilities. The processor includes a pipelined processing engine, having an array of processing element complex stages, and input and output header buffers. A debug system is provided that, when triggered, may put some or all of the processing element complexes into a debug mode of operation. When a complex is in debug mode, examination of internal stages of the component circuits of the complex may occur, in order to facilitate debugging of software and hardware errors that may occur during operation of the processor.
摘要:
A processor complex architecture facilitates accurate passing of transient data among processor complex stages of a pipelined processing engine. The processor complex comprises a central processing unit (CPU) coupled to an instruction memory and a pair of context data memory structures via a memory manager circuit. The context memories store transient “context” data for processing by the CPU in accordance with instructions stored in the instruction memory. The architecture further comprises data mover circuitry that cooperates with the context memories and memory manager to provide a technique for efficiently passing data among the stages in a manner that maintains data coherency in the processing engine. An aspect of the architecture is the ability of the CPU to operate on the transient data substantially simultaneously with the passing of that data by the data mover.
摘要:
An instrument is disclosed for microwave-assisted chemical processes that avoids tuning discrepancies that otherwise result based upon the materials being heated. The instrument includes a source of microwave radiation, a waveguide in communication with the source, with at least a portion of the waveguide forming a cylindrical arc, a cylindrical cavity immediately surrounded by the cylindrical arc portions of the waveguide, and at least three slotted openings in the circumference of the circular waveguide that provide microwave communication between the waveguide and the cavity.