摘要:
An instrument and method for high pressure microwave assisted chemistry are disclosed. The method includes the steps of applying microwave radiation to a sample in a sealed vessel while measuring the temperature of the sample and measuring the pressure generated inside the vessel and until the measured pressure reaches a designated set point, opening the vessel to release gases until the pressure inside the vessel reaches a lower designated set point, closing the vessel, and repeating the steps of opening the vessel at designated pressure set points and closing the vessel at designated pressure set points to the sample until the sample reaction reaches a designated high temperature. The designated set points can controllably differ from one another as the reaction proceeds. Microwave energy can be applied continuously or intermittently during the opening and closing steps. The apparatus includes a microwave cavity, a microwave transparent pressure resistant reaction vessel in the cavity, a cap on the reaction vessel, a pressure sensor for measuring pressure in the vessel, a temperature sensor, and means for opening and closing the cap at predetermined pressure set points measured by the pressure sensor to release pressure from the vessel.
摘要:
A processor complex architecture facilitates accurate passing of transient data among processor complex stages of a pipelined processing engine. The processor complex comprises a central processing unit (CPU) coupled to an instruction memory and a pair of context data memory structures via a memory manager circuit. The context memories store transient “context” data for processing by the CPU in accordance with instructions stored in the instruction memory. The architecture further comprises data mover circuitry that cooperates with the context memories and memory manager to provide a technique for efficiently passing data among the stages in a manner that maintains data coherency in the processing engine. An aspect of the architecture is the ability of the CPU to operate on the transient data substantially simultaneously with the passing of that data by the data mover.
摘要:
An instrument and method for high pressure microwave assisted chemistry are disclosed. The method includes the steps of applying microwave radiation to a sample in a sealed vessel while measuring the temperature of the sample and measuring the pressure generated inside the vessel and until the measured pressure reaches a designated set point, opening the vessel to release gases until the pressure inside the vessel reaches a lower designated set point, closing the vessel, and repeating the steps of opening the vessel at designated pressure set points and closing the vessel at designated pressure set points to the sample until the sample reaction reaches a designated high temperature. The designated set points can controllably differ from one another as the reaction proceeds. Microwave energy can be applied continuously or intermittently during the opening and closing steps. The apparatus includes a microwave cavity, a microwave transparent pressure resistant reaction vessel in the cavity, a cap on the reaction vessel, a pressure sensor for measuring pressure in the vessel, a temperature sensor, and means for opening and closing the cap at predetermined pressure set points measured by the pressure sensor to release pressure from the vessel.
摘要:
A system and technique facilitate fast context switching among processor complex stages of a pipelined processing engine. Each processor complex comprises a central processing unit (CPU) core having a plurality of internal context switchable registers that are connected to respective registers within CPU cores of the pipelined stages by a processor bus. The technique enables fast context switching by sharing the context switchable registers between upstream and downstream CPUs to, inter alia, force program counters into the downstream registers. In one aspect of the inventive technique, the system automatically reflects (shadows) the contents of an upstream CPU's context switchable registers at respective registers of a downstream CPU over the processor bus. In another aspect of the invention, the system redirects instruction execution by the downstream CPU to an appropriate routine based on processing performed by the upstream CPU.
摘要:
An internetworking system for exchanging packets of information between networks, the system comprising a network interface module for connecting a network to the system, receiving packets from the network in a native packet format used by the network and converting each received native packet to a packet having a generic format common to all networks connected to the system, and converting each of the generic packets to the native packet format for transmission to the network; a communication channel for carrying the generic packets to and from the network interface module, the channel having bandwidth; a first processing module for controlling dynamic allocation and deallocation of the channel bandwidth to the network connected to the system via the network interface module; and a second processing module for receiving all of the generic packets put on the channel by the network interface module, determining a destination network interface module for each of the generic packets on the channel, determining whether each of the generic packet needs to be bridged to the destination network interface module, and transmitting each of the generic packets determined to need bridging to the destination network interface module via the channel.
摘要:
A pressure-sealing, pressure-monitoring closure for non-invasively sealing a reaction vessel to a defined release pressure in microwave-assisted chemistry is disclosed. The closure includes a pressure-resistant, microwave-transparent reaction vessel, one portion of which defines a mouth, a flexible pressure-transmitting releasable cover assembly on the mouth of the vessel, a pressure transducer on the cover and external to the vessel for monitoring the pressure in the vessel as exerted against the flexible cover, and a clamp for urging the vessel, the cover and the transducer together under a defined force so that when the pressure in the vessel exceeds the defined force, the cover can flex and release the pressure from the vessel.
摘要:
A processor complex architecture facilitates accurate passing of transient data among processor complex stages of a pipelined processing engine. The processor complex comprises a central processing unit (CPU) coupled to an instruction memory and a pair of context data memory structures via a memory manager circuit. The context memories store transient “context” data for processing by the CPU in accordance with instructions stored in the instruction memory. The architecture further comprises data mover circuitry that cooperates with the context memories and memory manager to provide a technique for efficiently passing data among the stages in a manner that maintains data coherency in the processing engine. An aspect of the architecture is the ability of the CPU to operate on the transient data substantially simultaneously with the passing of that data by the data mover.
摘要:
A processor complex architecture facilitates accurate passing of transient data among processor complex stages of a pipelined processing engine. The processor complex comprises a central processing unit (CPU) coupled to an instruction memory and a pair of context data memory structures via a memory manager circuit. The context memories store transient “context” data for processing by the CPU in accordance with instructions stored in the instruction memory. The architecture further comprises data mover circuitry that cooperates with the context memories and memory manager to provide a technique for efficiently passing data among the stages in a manner that maintains data coherency in the processing engine. An aspect of the architecture is the ability of the CPU to operate on the transient data substantially simultaneously with the passing of that data by the data mover.
摘要:
An instrument is disclosed for microwave-assisted chemical processes that avoids tuning discrepancies that otherwise result based upon the materials being heated. The instrument includes a source of microwave radiation, a waveguide in communication with the source, with at least a portion of the waveguide forming a cylindrical arc, a cylindrical cavity immediately surrounded by the cylindrical arc portions of the waveguide, and at least three slotted openings in the circumference of the circular waveguide that provide microwave communication between the waveguide and the cavity.
摘要:
A programmable processing engine processes transient data within an intermediate network station of a computer network. The engine comprises an array of processing elements symmetrically arrayed as rows and columns, and embedded between input and output buffer units with a plurality of interfaces from the array to an external memory. The external memory stores non-transient data organized within data structures, such as forwarding and routing tables, for use in processing the transient data. Each processing element contains an instruction memory that allows programming of the array to process the transient data as processing element stages of baseline or extended pipelines operating in parallel.