Process for the preparation of organic dithiol polysulfides
    4.
    发明授权
    Process for the preparation of organic dithiol polysulfides 失效
    制备有机二硫醇多硫化物的方法

    公开(公告)号:US3862922A

    公开(公告)日:1975-01-28

    申请号:US39644473

    申请日:1973-09-12

    Abstract: A process for the preparation of organic dithiol polysulfides with a molecular weight of between 500 and 10,000, characterized by the fact that these products are obtained when a dihalogenated organic derivative and hydrogen sulfide react simultaneously with an alkaline polysulfide solution. New products are obtained by this process, using dichlorodiethyl formal and dichlorodibutyl formal. These dithiol polysulfides react with sulfur to form either plasticized sulfur, with many possible applications in the coating field, or polysulfide polymers, one of the applications of which is the modification of bitumens.

    Abstract translation: 一种制备分子量在500至10,000之间的有机二硫醇多硫化物的方法,其特征在于当二卤代有机衍生物和硫化氢与碱性多硫化物溶液同时反应时获得这些产物。 通过该方法获得新产物,使用二氯二乙基甲缩醛和二氯正丁基甲醛。 这些二硫醇多硫化物与硫反应以形成增塑硫,在涂层领域有许多可能的应用,或多硫化物聚合物,其应用之一是改性沥青。

    New and useful sulphur compositions and their preparation
    5.
    发明授权
    New and useful sulphur compositions and their preparation 失效
    新的和有用的硫化物组合物及其制备

    公开(公告)号:US3631158A

    公开(公告)日:1971-12-28

    申请号:US3631158D

    申请日:1970-01-29

    CPC classification number: C04B28/36 C01B17/0243 C04B24/16

    Abstract: IN WHICH R IS 2 OR 3, Z IS 0 OR 1, N AND M ARE EACH FROM 1 TO 8, R AND R'', WHICH MAY BE THE SAME OR DIFFERENT, ARE EACH HYDROGEN, A MONOVALENT HYDROCARBON RADICAL CONTAINING 1 TO 12 CARBON ATOMS, WHICH RADICALS CAN BE SATURATED OR UNSATURATED ALIPHATIC RADICALS, SATURATED OR UNSATURATED CYCLOALKYL RADICALS, OR AROMATIC RADICALS, AND X IS ANY OF THE FOLLOWING: -NH,-O-,-S-

    -CH(-R")-

    (IN WHICH R" CAN BE H, CH3 OR OH)

    -O-(CH2)P-O-

    AND -S-(CH2)P-S-(P BEING FROM 1 TO 6).
    NEW PLASTIC SULPHUR COMPOSITIONS ARE PREPARED BY CAUSING MOLTEN SULPHUR TO REACT WITH ONE OR MORE CYCLIC POLYSULPHIDES OF THE FORMULA:

    (-(CH(-R))N-(X)Z-(CH(-R''))M-)>(S)R

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