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公开(公告)号：US11034584B1
公开(公告)日：2021-06-15
申请号：US17015235
申请日：2020-09-09
摘要： Single-step, inexpensive, scalable, and eco-friendly methods and systems for exfoliation and deposition of 2D reduced phosphorene nanosheets are provided, as well as deposited phosphorene nanosheets with high specific capacitance. The exfoliation and deposition can be in situ and can include exfoliation from bulk black phosphorus (BP) into a solvent and deposition onto a negative feeding electrode. The positive feeding electrode can be a noble metal, such as a platinum wire.
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公开(公告)号：US11605507B1
公开(公告)日：2023-03-14
申请号：US17839984
申请日：2022-06-14
摘要： Microsupercapacitors (MSCs), as well as methods of fabricating the same and methods of using the same, are provided. An MSC can include interdigitated microelectrodes having reduced graphene oxide (rGO) (e.g., vertically aligned nanosheets thereof) disposed on upper surfaces of the microelectrodes. The MSC can be fabricated by preparing a micro-current collector (MCC) comprising the interdigitated microelectrodes using photolithography and then performing a bipolar electrochemistry process on the MCC to deposit rGO on the upper surfaces of the interdigitated microelectrodes (e.g., in a single-step in situ exfoliation, reduction, and deposition).
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公开(公告)号：US11352703B2
公开(公告)日：2022-06-07
申请号：US17234114
申请日：2021-04-19
IPC分类号： C25B1/135 , C25B11/036 , C25B15/02 , C25B11/046 , C25B9/17 , C25B11/043
摘要： Bipolar electrochemistry (BPE) concepts are used to provide a single-step and controllable process for simultaneously exfoliating a graphite source and depositing both graphene oxide and reduced graphene oxide layers on conductive substrates. A bipolar electrochemical cell can be used for a three-in-one deposition and can include two wired pieces of graphite to monitor the amount of current that passes through the bipolar electrode.
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公开(公告)号：US20210388513A1
公开(公告)日：2021-12-16
申请号：US17234114
申请日：2021-04-19
IPC分类号： C25B11/036 , C25B9/17 , C25B15/02 , C25B1/135 , C25B11/043 , C25B11/046
摘要： Bipolar electrochemistry (BPE) concepts are used to provide a single-step and controllable process for simultaneously exfoliating a graphite source and depositing both graphene oxide and reduced graphene oxide layers on conductive substrates. A bipolar electrochemical cell can be used for a three-in-one deposition and can include two wired pieces of graphite to monitor the amount of current that passes through the bipolar electrode.
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公开(公告)号：US10676357B1
公开(公告)日：2020-06-09
申请号：US16361332
申请日：2019-03-22
摘要： A single-step, in situ bipolar exfoliation system, and methods for exfoliations of multi-layer bulk black phosphorous into single-layer (two-dimensional), few-layer, or even nano-platelets phosphorene are provided. The bipolar exfoliation system can include: a first driving electrode; a second driving electrode electrically connected to the first driving electrode through an external power supply; at least one bipolar electrode comprising multi-layer bulk black phosphorous; and a solvent in physical contact with the first driving electrode, the second driving electrode, and the at least one bipolar electrode. The system can be configured such that the electric conditions between the first and second driving electrodes can be used to turn one end of the at least one bipolar electrode into an anodic pole and the other end of the at least one bipolar electrode into a cathodic pole such that the multi-layer black phosphorous is exfoliated into the single-layer, few-layer, or nano-platelets phosphorene.
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