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公开(公告)号：US08748511B2
公开(公告)日：2014-06-10
申请号：US13267295
申请日：2011-10-06
CPC分类号： C09J171/02 , C08G65/336
摘要： Curable compositions comprising a) an alkoxysilane and/or acyloxysilane terminated polymer having at least one end group of the general formula (I) -An-R—SiXYZ (I) and b) hollow microspheres made of a copolymer obtained by the polymerization of methacrylonitrile and at least one monomer M2 selected from the group consisting of acrylic acid, methacrylic acid, acrylic acid alkyl esters and methacrylic acid alkyl esters, wherein the copolymer comprises at maximum 5 wt. % units that are due to the installation of additional monomers and is free of units containing chlorine, to a method for the production thereof and to the use thereof as silane cross-linking adhesive, sealing or coating substances.
摘要翻译： 可固化组合物，其包含a）具有至少一个具有通式（I）-n-R-SiXYZ（I）的端基的烷氧基硅烷和/或酰氧基硅烷封端的聚合物，和b）由通过甲基丙烯腈的聚合获得的共聚物制成的中空微球 和选自丙烯酸，甲基丙烯酸，丙烯酸烷基酯和甲基丙烯酸烷基酯的至少一种单体M2，其中所述共聚物包含最多5wt。 由于安装另外的单体而且不含有氯的单元，其制备方法以及作为硅烷交联粘合剂，密封或涂覆物质的用途的单位为％。
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公开(公告)号：US20120123016A1
公开(公告)日：2012-05-17
申请号：US13267295
申请日：2011-10-06
IPC分类号： C09D175/04 , C08K5/10 , C08K5/11 , C08K5/06 , C08K5/12 , C08K5/521 , C08K5/42 , C09J175/04 , C08K5/1515
CPC分类号： C09J171/02 , C08G65/336
摘要： Curable compositions comprising a) an alkoxysilane and/or acyloxysilane terminated polymer having at least one end group of the general formula (I) -An-R-SiXYZ (I) and b) hollow microspheres made of a copolymer obtained by the polymerization of methacrylonitrile and at least one monomer M2 selected from the group consisting of acrylic acid, methacrylic acid, acrylic acid alkyl esters and methacrylic acid alkyl esters, wherein the copolymer comprises at maximum 5 wt. % units that are due to the installation of additional monomers and is free of units containing chlorine, to a method for the production thereof and to the use thereof as silane cross-linking adhesive, sealing or coating substances.
摘要翻译： 可固化组合物，其包含a）具有至少一个具有通式（I）-n-R-SiXYZ（I）的端基的烷氧基硅烷和/或酰氧基硅烷封端的聚合物，和b）由通过甲基丙烯腈的聚合获得的共聚物制成的中空微球 和选自丙烯酸，甲基丙烯酸，丙烯酸烷基酯和甲基丙烯酸烷基酯的至少一种单体M2，其中所述共聚物包含最多5wt。 由于安装另外的单体而且不含有氯的单元，其制备方法以及作为硅烷交联粘合剂，密封或涂覆物质的用途的单位为％。
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公开(公告)号：US08609800B2
公开(公告)日：2013-12-17
申请号：US12906397
申请日：2010-10-18
申请人： Helene Boudet , Andreas Bolte , Thomas Bachon , Lars Zander , Christiane Kunze , Johann Klein , Nicole Ditges
发明人： Helene Boudet , Andreas Bolte , Thomas Bachon , Lars Zander , Christiane Kunze , Johann Klein , Nicole Ditges
IPC分类号： C08G18/83
CPC分类号： C09J175/04 , C08G18/10 , C08G18/765 , C08G2190/00 , C08G18/289
摘要： Silylated polyurethanes can be manufactured by reacting at least one polyol compound, having a molecular weight from 4000 to 20,000 dalton, with a diisocyanate, with a stoichiometric excess of the diisocyanate compound with respect to the polyol compound or compounds, with the result that a polyurethane prepolymer that is isocyanate-terminated is formed; and by subsequently reacting the polyurethane prepolymer with one or more OH-terminated silanes of formula (1) to yield a polyurethane having predominantly terminal alkoxysilyl groups. In formula (1), m is equal to 0, 1, or 2, R1 is an alkyl residue having 1 to 4 carbon atoms, R2 is an alkyl residue having 1 to 4 carbon atoms, R3 is a divalent organic residue having 1 to 12 atoms, selected from C, N, S, and/or O, in the chain, but by preference exclusively carbon atoms, R4 is a hydrogen atom or an alkyl residue having 1 to 10 carbon atoms, and R is a difunctional organic group, preferably a linear or branched alkyl group having 1 to 6 carbon atoms. The silylated polyurethanes are suitable for use in a preparation as an adhesive, sealant, or coating agent.
摘要翻译： 甲硅烷基化聚氨酯可以通过使至少一种分子量为4000至20,000道尔顿的多元醇化合物与二异氰酸酯相对于多元醇化合物或化合物与化学计量过量的二异氰酸酯化合物反应而制备，结果是聚氨酯 形成异氰酸酯封端的预聚物; 并随后使聚氨酯预聚物与一种或多种式（1）的OH封端的硅烷反应，得到主要具有末端烷氧基甲硅烷基的聚氨酯。 在式（1）中，m等于0,1或2，R 1是具有1至4个碳原子的烷基，R 2是具有1至4个碳原子的烷基，R 3是具有1至 在链中选自C，N，S和/或O的12个原子，但仅仅是碳原子，R4是氢原子或具有1-10个碳原子的烷基，R是双官能有机基团 优选具有1-6个碳原子的直链或支链烷基。 甲硅烷基化聚氨酯适用于作为粘合剂，密封剂或涂层剂的制剂。
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公开(公告)号：US08431675B2
公开(公告)日：2013-04-30
申请号：US12791974
申请日：2010-06-02
申请人： Daniela Braun , Johann Klein , Christiane Kunze , Sara Gonzalez , Lars Zander , Andreas Bolte , Helene Boudet , Sarah Schulz
发明人： Daniela Braun , Johann Klein , Christiane Kunze , Sara Gonzalez , Lars Zander , Andreas Bolte , Helene Boudet , Sarah Schulz
IPC分类号： C08G77/04
CPC分类号： C09J175/04 , C08G18/12 , C08G18/282 , C08G18/4825 , C08G18/765 , C08G2190/00 , C08G18/718 , C08G18/289
摘要： A method for producing a silylated polyurethane including the steps: (A) converting (i) at least polyol compound having a molecular weight of 4,000-30,000 g/mol and at least one monofunctional compound relative to isocyanates and (ii) at least one diisocyanate at a stoichiometric excess of the sum of the polyol compound(s) and monofunctional compound relative to the diisocyanate compound(s), whereby a hydroxyl-terminated polyurethane prepolymer is formed; and (B) converting the polyurethane prepolymer and one or more isocyanate silane(s) of the formula (I): OCN—R—Si—(R1)m(-OR2)3-m, where m is 0, 1 or 2, each R2 is an alkyl radical having 1 to 4 carbon atoms, each R1 is an alkyl radical having 1 to 4 carbon atoms, and R is a difunctional organic group. Also compounds comprising the silylated polyurethane that can be so produced, and the use thereof as an adhesive and sealant or coating composition.
摘要翻译： 一种甲硅烷基化聚氨酯的制造方法，包括以下步骤：（A）至少将（i）至少相对于异氰酸酯转化分子量为4,000〜30,000g / mol的多元醇化合物和至少一种单官能化合物，和（ii）至少一种二异氰酸酯 多元醇化合物和单官能化合物相对于二异氰酸酯化合物的总和的化学计量过量，由此形成羟基封端的聚氨酯预聚物; 和（B）将聚氨酯预聚物和一种或多种式（I）的异氰酸酯硅烷转化为：OCN-R-Si-（R1）m（-OR2）3-m，其中m为0,1或2 每个R 2是具有1至4个碳原子的烷基，每个R 1是具有1至4个碳原子的烷基，R 2是双官能的有机基团。 还包括可以如此制备的包含甲硅烷基化聚氨酯的化合物，以及其作为粘合剂和密封剂或涂料组合物的用途。
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公开(公告)号：US20100280209A1
公开(公告)日：2010-11-04
申请号：US12791974
申请日：2010-06-02
申请人： Daniela Braun , Johann Klein , Christiane Kunze , Sara Gonzalez , Lars Zander , Andreas Bolte , Helene Boudet , Sarah Schulz
发明人： Daniela Braun , Johann Klein , Christiane Kunze , Sara Gonzalez , Lars Zander , Andreas Bolte , Helene Boudet , Sarah Schulz
IPC分类号： C08G71/04
CPC分类号： C09J175/04 , C08G18/12 , C08G18/282 , C08G18/4825 , C08G18/765 , C08G2190/00 , C08G18/718 , C08G18/289
摘要： A method for producing a silylated polyurethane including the steps: (A) converting (i) at least polyol compound having a molecular weight of 4,000-30,000 g/mol and at least one monofunctional compound relative to isocyanates and (ii) at least one diisocyanate at a stoichiometric excess of the sum of the polyol compound(s) and monofunctional compound relative to the diisocyanate compound(s), whereby a hydroxyl-terminated polyurethane prepolymer is formed; and (B) converting the polyurethane prepolymer and one or more isocyanate silane(s) of the formula (I): OCN—R—Si—(R1)m(-OR2)3-m, where m is 0, 1 or 2, each R2 is an alkyl radical having 1 to 4 carbon atoms, each R1 is an alkyl radical having 1 to 4 carbon atoms, and R is a difunctional organic group. Also compounds comprising the silylated polyurethane that can be so produced, and the use thereof as an adhesive and sealant or coating composition.
摘要翻译： 一种甲硅烷基化聚氨酯的制造方法，包括以下步骤：（A）至少将（i）至少相对于异氰酸酯转化分子量为4,000〜30,000g / mol的多元醇化合物和至少一种单官能化合物，和（ii）至少一种二异氰酸酯 多元醇化合物和单官能化合物相对于二异氰酸酯化合物的总和的化学计量过量，由此形成羟基封端的聚氨酯预聚物; 和（B）将聚氨酯预聚物和一种或多种式（I）的异氰酸酯硅烷转化为OCN-R-Si-（R1）m（-OR2）3-m，其中m为0,1或2 每个R 2是具有1至4个碳原子的烷基，每个R 1是具有1至4个碳原子的烷基，R 2是双官能的有机基团。 还包括可以如此制备的包含甲硅烷基化聚氨酯的化合物，以及其作为粘合剂和密封剂或涂料组合物的用途。
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6.发明申请公开(公告)号：US20100331480A1
公开(公告)日：2010-12-30
申请号：US12832356
申请日：2010-07-08
申请人： Noelle Wrubbel , Helene Boudet , Andrea Krlejova , Andreas Bolte , Lars Zander , Johann Klein , Christiane Kunze
发明人： Noelle Wrubbel , Helene Boudet , Andrea Krlejova , Andreas Bolte , Lars Zander , Johann Klein , Christiane Kunze
CPC分类号： C08G18/4866 , C08G18/10 , C08G18/4879 , C08G18/718 , C08G65/30 , C08G65/33351 , C08G65/336 , C08G65/337 , C08G2190/00
摘要： Silyated polyurethanes can be manufactured by (A) converting (i) at least one polyol compound A with a molecular weight of 500-20,000 Dalton, in particular 4000-10,000 Dalton, (ii) with a dihalogenide to a polyol compound B with a molecular weight of 4000-40,000 Dalton, in particular 8000-20,000 Dalton, and subsequent (B) conversion of this polyol B with one or more isocyanatosilanes of formula (1): OCN—R—Si—(R1)m(-OR2)3-m where m is 0.1 or 2, each R2 is an alkyl radical with 1 to 4 carbon atoms, each R1 is an alkyl radical with 1 to 4 carbon atoms and R is a difunctional organic pump. These silylated polyurethanes are suited to use as adhesives, sealant or coating agent in preparations containing one or more such silylated polyurethane.
摘要翻译： 可以通过（A）将（i）至少一种分子量为500-20,000道尔顿，特别是4000-10,000道尔顿的多元醇化合物A，（ii）与二卤化物转化成多元醇化合物B的分子式 重量为4000-40,000道尔顿，特别是8000-20,000道尔顿，随后（B）将该多元醇B与一种或多种式（1）的异氰酸基硅烷转化：OCN-R-Si-（R1）m（-OR2）3 -m其中m为0.1或2，每个R 2为具有1至4个碳原子的烷基，每个R 1为具有1至4个碳原子的烷基，R为双官能有机泵。 这些甲硅烷基化聚氨酯适于在含有一种或多种这种甲硅烷基化聚氨酯的制剂中用作粘合剂，密封剂或包衣剂。
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公开(公告)号：US20110034627A1
公开(公告)日：2011-02-10
申请号：US12906397
申请日：2010-10-18
申请人： Helene Boudet , Andreas Bolte , Thomas Bachon , Lars Zander , Christiane Kunze , Johann Klein , Nicole Ditges
发明人： Helene Boudet , Andreas Bolte , Thomas Bachon , Lars Zander , Christiane Kunze , Johann Klein , Nicole Ditges
CPC分类号： C09J175/04 , C08G18/10 , C08G18/765 , C08G2190/00 , C08G18/289
摘要： Silylated polyurethanes can be manufactured by reacting at least one polyol compound, having a molecular weight from 4000 to 20,000 dalton, with a diisocyanate, with a stoichiometric excess of the diisocyanate compound with respect to the polyol compound or compounds, with the result that a polyurethane prepolymer that is isocyanate-terminated is formed; and by subsequently reacting the polyurethane prepolymer with one or more OH-terminated silanes of formula (1) to yield a polyurethane having predominantly terminal alkoxysilyl groups. In formula (1), m is equal to 0, 1, or 2, R1 is an alkyl residue having 1 to 4 carbon atoms, R2 is an alkyl residue having 1 to 4 carbon atoms, R3 is a divalent organic residue having 1 to 12 atoms, selected from C, N, S, and/or O, in the chain, but by preference exclusively carbon atoms, R4 is a hydrogen atom or an alkyl residue having 1 to 10 carbon atoms, and R is a difunctional organic group, preferably a linear or branched alkyl group having 1 to 6 carbon atoms. The silylated polyurethanes are suitable for use in a preparation as an adhesive, sealant, or coating agent.
摘要翻译： 甲硅烷基化聚氨酯可以通过使至少一种分子量为4000至20,000道尔顿的多元醇化合物与二异氰酸酯相对于多元醇化合物或化合物与化学计量过量的二异氰酸酯化合物反应而制备，结果是聚氨酯 形成异氰酸酯封端的预聚物; 并随后使聚氨酯预聚物与一种或多种式（1）的OH封端的硅烷反应，得到主要具有末端烷氧基甲硅烷基的聚氨酯。 在式（1）中，m等于0,1或2，R 1是具有1至4个碳原子的烷基，R 2是具有1至4个碳原子的烷基，R 3是具有1至 在链中选自C，N，S和/或O的12个原子，但仅仅是碳原子，R4是氢原子或具有1-10个碳原子的烷基，R是双官能有机基团 优选具有1-6个碳原子的直链或支链烷基。 甲硅烷基化聚氨酯适用于作为粘合剂，密封剂或涂层剂的制剂。
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