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公开(公告)号：US20050277770A1
公开(公告)日：2005-12-15
申请号：US10867512
申请日：2004-06-14
IPC分类号： C07D487/22 , C07D43/14
CPC分类号： C07D487/22
摘要： A method of making a 5-formylporphyrin, comprises the steps of: condensing a 5-acetaldipyrromethane with a dipyrromethane-1,9-dicarbinol to produce a porphyrin having an acetal group substituted thereon at the 5 position; and then hydrolyzing said porphyrin to produce said 5-formylporphyrin. Products and intermediates useful in such methods, along with methods of making such intermediates, are also described.
摘要翻译： 制备5-甲酰卟啉的方法包括以下步骤：使5-乙醛二吡咯甲烷与二吡咯烷-1,9-二甲醇缩合以产生在5位上具有取代在其上的缩醛基团的卟啉; 然后水解所述卟啉以产生所述5-甲酰卟啉。 还描述了在这些方法中有用的产物和中间体以及制备此类中间体的方法。
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公开(公告)号：US20110152515A1
公开(公告)日：2011-06-23
申请号：US13035235
申请日：2011-02-25
IPC分类号： C07D487/22
CPC分类号： C07D487/22
摘要： A method of making a 5-formylporphyrin, comprises the steps of: condensing a 5-acetaldipyrromethane with a dipyrromethane-1,9-dicarbinol to produce a porphyrin having an acetal group substituted thereon at the 5 position; and then hydrolyzing said porphyrin to produce said 5-formylporphyrin. Products and intetinediates useful in such methods, along with methods of making such intermediates, are also described.
摘要翻译： 制备5-甲酰卟啉的方法包括以下步骤：使5-乙醛二吡咯甲烷与二吡咯烷-1,9-二甲醇缩合以产生在5位上具有取代在其上的缩醛基团的卟啉; 然后水解所述卟啉以产生所述5-甲酰卟啉。 还描述了可用于这些方法的产品和内联物，以及制备此类中间体的方法。
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公开(公告)号：US08420804B2
公开(公告)日：2013-04-16
申请号：US13035235
申请日：2011-02-25
IPC分类号： C07D487/22
CPC分类号： C07D487/22
摘要： A method of making a 5-formylporphyrin, comprises the steps of: condensing a 5-acetaldipyrromethane with a dipyrromethane-1,9-dicarbinol to produce a porphyrin having an acetal group substituted thereon at the 5 position; and then hydrolyzing said porphyrin to produce said 5-formylporphyrin. Products and intermediates useful in such methods, along with methods of making such intermediates, are also described.
摘要翻译： 制备5-甲酰卟啉的方法包括以下步骤：使5-乙醛二吡咯甲烷与二吡咯烷-1,9-二甲醇缩合以产生在5位上具有取代在其上的缩醛基团的卟啉; 然后水解所述卟啉以产生所述5-甲酰卟啉。 还描述了在这些方法中有用的产物和中间体以及制备此类中间体的方法。
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公开(公告)号：US07919615B2
公开(公告)日：2011-04-05
申请号：US12362714
申请日：2009-01-30
IPC分类号： C07D487/22 , C07D405/14 , C07D213/70
CPC分类号： C07D487/22
摘要： A method of making a 5-formylporphyrin, comprises the steps of: condensing a 5-acetaldipyrromethane with a dipyrromethane-1,9-dicarbinol to produce a porphyrin having an acetal group substituted thereon at the 5 position; and then hydrolyzing said porphyrin to produce said 5-formylporphyrin. Products and intermediates useful in such methods, along with methods of making such intermediates, are also described.
摘要翻译： 制备5-甲酰卟啉的方法包括以下步骤：使5-乙醛二吡咯甲烷与二吡咯烷-1,9-二甲醇缩合以产生在5位上具有取代在其上的缩醛基团的卟啉; 然后水解所述卟啉以产生所述5-甲酰卟啉。 还描述了在这些方法中有用的产物和中间体以及制备此类中间体的方法。
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公开(公告)号：US07501507B2
公开(公告)日：2009-03-10
申请号：US10867512
申请日：2004-06-14
IPC分类号： C07D487/22 , C07B43/00
CPC分类号： C07D487/22
摘要： A method of making a 5-formylporphyrin, comprises the steps of: condensing a 5-acetaldipyrromethane with a dipyrromethane-1,9-dicarbinol to produce a porphyrin having an acetal group substituted thereon at the 5 position; and then hydrolyzing said porphyrin to produce said 5-formylporphyrin. Products and intermediates useful in such methods, along with methods of making such intermediates, are also described.
摘要翻译： 制备5-甲酰卟啉的方法包括以下步骤：使5-乙醛二吡咯甲烷与二吡咯烷-1,9-二甲醇缩合以产生在5位上具有取代在其上的缩醛基团的卟啉; 然后水解所述卟啉以产生所述5-甲酰卟啉。 还描述了在这些方法中有用的产物和中间体以及制备此类中间体的方法。
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公开(公告)号：US20090137795A1
公开(公告)日：2009-05-28
申请号：US12362714
申请日：2009-01-30
IPC分类号： C07D487/22 , C07D405/14 , C07D213/70
CPC分类号： C07D487/22
摘要： A method of making a 5-formylporphyrin, comprises the steps of: condensing a 5-acetaldipyrromethane with a dipyrromethane-1,9-dicarbinol to produce a porphyrin having an acetal group substituted thereon at the 5 position; and then hydrolyzing said porphyrin to produce said 5-formylporphyrin. Products and intermediates useful in such methods, along with methods of making such intermediates, are also described.
摘要翻译： 制备5-甲酰卟啉的方法包括以下步骤：使5-乙醛二吡咯甲烷与二吡咯烷-1,9-二甲醇缩合以产生在5位上具有取代在其上的缩醛基团的卟啉; 然后水解所述卟啉以产生所述5-甲酰卟啉。 还描述了在这些方法中有用的产物和中间体以及制备此类中间体的方法。
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7.发明申请METHODS AND INTERMEDIATES FOR THE SYNTHESIS OF DIPYRRIN-SUBSTITUTED PORPHYRINIC MACROCYCLES 失效二吡啶取代的磷杂环化合物的合成方法及其中间体公开(公告)号：US20070191600A1
公开(公告)日：2007-08-16
申请号：US11737979
申请日：2007-04-20
IPC分类号： C09B47/04
CPC分类号： H01L51/0077 , C07D403/06 , C07D403/14 , C07D487/22 , Y02E10/549 , Y02P70/521
摘要： The present invention provides dipyrrin substituted porphyrinic macrocycles, intermediates useful for making the same, and methods of making the same. Such compounds may be used for purposes including the making of molecular memory devices, solar cells and light harvesting arrays.
摘要翻译： 本发明提供二吡咯取代的卟啉大环化合物，可用于制备其的中间体及其制备方法。 这些化合物可用于包括制备分子记忆装置，太阳能电池和光收集阵列的目的。
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公开(公告)号：US20050282779A1
公开(公告)日：2005-12-22
申请号：US10956781
申请日：2004-10-01
IPC分类号： A61K31/69 , C07D487/22 , C07F5/02
CPC分类号： C07D207/335 , C07D487/22 , C07F5/02 , C07F5/022
摘要： A method of making a metal complex comprises combining a 1-monoacyldipyrromethane with a compound of the formula R1R2MX, wherein M is boron, R1 and R2 are each independently organic substituents; and X is an anion leaving group; to produce a metal complex of the formula DMR1R2 wherein DH is a 1-monoacyldipyrromethane. The methods and complexes are useful for the purification and synthesis of dipyrromethanes and porphyrins.
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9.发明申请Synthesis of Phosphono-Substituted Porphyrin Compounds for Attachment to Metal Oxide Surfaces 失效用于附着到金属氧化物表面的膦酰取代的卟啉化合物的合成公开(公告)号：US20070055060A1
公开(公告)日：2007-03-08
申请号：US11553542
申请日：2006-10-27
IPC分类号： C07D487/22 , C07F9/547
CPC分类号： H01L51/0077 , C07F9/6524 , H01G9/2031 , H01L51/4226 , Y02E10/542 , Y02P70/521
摘要： A method of making a phosphono-substituted dipyrromethane comprises reacting an aldehyde or acetal having at least one phosphono group substituted thereon with pyrrole to produce a phosphono-substituted dipyrromethane; and wherein the phosphono is selected from the group consisting of dialkyl phosphono, diaryl phosphono, and dialkylaryl phosphono. Additional methods, intermediates and products are also described.
摘要翻译： 制备膦酰取代的二吡咯甲烷的方法包括使具有至少一个被取代的膦酰基的醛或缩醛与吡咯反应以产生膦酰取代的二吡咯烷; 并且其中膦酰基选自二烷基膦酰基，二芳基膦酰基和二烷基芳基膦酰基。 还描述了其它方法，中间体和产物。
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10.发明申请公开(公告)号：US20050282778A1
公开(公告)日：2005-12-22
申请号：US10872321
申请日：2004-06-18
IPC分类号： A61K31/69 , C07D487/22 , C07F5/02
CPC分类号： C07D207/333 , C07F5/02
摘要： A method of making a metal complex comprises combining a 1-monoacyldipyrromethane with a compound of the formula R1R2MX, wherein M is boron, R1 and R2 are each independently organic substituents; and X is an anion leaving group; to produce a metal complex of the formula DMR1R2 wherein DH is a 1-monoacyldipyrromethane. The methods and complexes are useful for the purification and synthesis of dipyrromethanes and porphyrins.
摘要翻译： 一种制备金属络合物的方法包括将1-单酰基二吡咯甲烷与式R 1 2 R 2 MX的化合物组合，其中M是硼，R 1， R 2和R 2各自独立地为有机取代基; X为阴离子离去基团; 以制备其中DH是1-单酰基二吡咯甲烷的式DMR 1 R 2的金属络合物。 该方法和配合物可用于双嘧磺隆和卟啉的纯化和合成。
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