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1.发明授权Anionic polyalkoxy group comprising surfactants on basis of guerbet-alcohols, method of manufacture and use in enhanced oil recovery (EOR) applications 有权基于优尔特 - 醇的基于表面活性剂的阴离子聚烷氧基，制备方法和用于增强采油（EOR）应用中公开(公告)号：US09296942B2
公开(公告)日：2016-03-29
申请号：US14201323
申请日：2014-03-07
Applicant: Board of Regents, The University of Texas System , BASF SE
Inventor： Upali P. Weerasooriya , Gary A. Pope , Christian Bittner , Gunter Oetter , Jack F. Tinsley , Christian Spindler , Gabriela Alvarez Jurgenson , Sophie Vogel
IPC: E21B43/16 , C09K8/584 , C07C305/10 , C07C309/10 , C08G65/26 , C08G65/334
CPC classification number: C09K8/584 , C07C305/10 , C07C309/10 , C08G65/2609 , C08G65/3344 , E21B43/16
Abstract: Compositions and methods of synthesis of anionic surfactants by alkoxylation of a Guerbet alcohol (GA) having 12 to 36 carbon atoms using butylene oxide, and optionally propylene oxide and/or ethylene oxide followed by the incorporation of a terminal anionic group are described herein. The GA of the present invention is made by a facile and inexpensive method that involves high temperature base catalyzed dimerization of alcohols with 6 to 18 carbon atoms. The large hydrophobe ether surfactants of the present invention find uses in enhanced oil recovery (EOR) applications where it is used for solubilization and mobilization of oil and for environmental cleanup. Further, the hydrophobe alkoxylated GA without anionic terminal group can be used as an ultra-high molecular weight non-ionic surfactant.
Abstract translation: 本文描述了通过使用环氧丁烷和任选的环氧丙烷和/或环氧乙烷烷氧基化具有12至36个碳原子的格伯特醇（GA），然后引入末端阴离子基团来合成阴离子表面活性剂的组合物和方法。 本发明的GA通过易于且廉价的方法制备，其涉及具有6至18个碳原子的醇的高温碱催化二聚。 本发明的大型疏水醚表面活性剂用于增强采油（EOR）应用中，其用于溶解和动员油并用于环境清洁。 此外，不含阴离子末端基团的疏水基烷氧基化GA可用作超高分子量非离子表面活性剂。
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公开(公告)号：US11643491B2
公开(公告)日：2023-05-09
申请号：US17286468
申请日：2019-10-17
Applicant: BASF SE
Inventor： Faissal-Ali El-Toufaili , Dennis Loesch , Anna-Corina Schmidt , Tobias Joachim Zimmermann , Markus Ostermayr , Jack F. Tinsley , Brent Busby
CPC classification number: C08F220/56 , B01J19/06 , C08J3/075 , C09K8/588 , C09K8/68 , C12P13/02 , C12Y402/01084 , B01J2219/0002 , C08F2800/10 , C08F2800/20
Abstract: Process for producing aqueous polyacrylamide concentrates by polymerizing an aqueous solution comprising at least acrylamide thereby obtaining an aqueous polyacrylamide gel, comminuting said aqueous polyacrylamide gel and mixing it with an aqueous liquid, wherein the manufacturing steps are allocated to two different locations A and B and the process comprises the step of transporting an aqueous polyacrylamide concentrate hold in a suitable transport unit from a location A to a location B. Modular, relocatable plant for manufacturing aqueous polyacrylamide, wherein the units of the plant are located at two different locations A and B.
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公开(公告)号：US20210388256A1
公开(公告)日：2021-12-16
申请号：US17286469
申请日：2019-10-17
Applicant: BASF SE
Inventor： Faissal-Ali EL-Toufailli , Dennis Loesch , Anna-Corina Schmidt , Tobias Joachim Zimmermann , Markus Ostermayr , Jack F. Tinsley , Brent Busby
IPC: C09K8/68 , C09K8/88 , E21B43/267 , E21B15/00
Abstract: Process of fracturing subterranean, oil- and/or gas-bearing formations by injecting an aqueous fracturing fluid into a wellbore at a rate and pressure sufficient to penetrate into the formation, and to initiate or extend fractures in the formation, wherein the aqueous fracturing fluid is obtained by mixing at least an aqueous base fluid and an aqueous polyacrylamide concentrate having a concentration of 3.1 to 14.9% by weight of polyacrylamides, relating to the total of all components of the aqueous polyacrylamide concentrate, and wherein at least a part of the aqueous fracturing fluid injected additionally comprises a proppant.
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Patent Agency Ranking
公开(公告)号：US20210347924A1
公开(公告)日：2021-11-11
申请号：US17286468
申请日：2019-10-17
Applicant: BASF SE
Inventor： Faissal-Ali El-Toufaili , Dennis Loesch , Anna-Corina Schmidt , Tobias Joachim Zimmermann , Markus Ostermayr , Jack F. Tinsley , Brent Busby
Abstract: Process for producing aqueous polyacrylamide concentrates by polymerizing an aqueous solution comprising at least acrylamide thereby obtaining an aqueous polyacrylamide gel, comminuting said aqueous polyacrylamide gel and mixing it with an aqueous liquid, wherein the manufacturing steps are allocated to two different locations A and B and the process comprises the step of transporting an aqueous polyacrylamide concentrate hold in a suitable transport unit from a location A to a location B. Modular, relocatable plant for manufacturing aqueous polyacrylamide, wherein the units of the plant are located at two different locations A and B.
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公开(公告)号：US11725102B2
公开(公告)日：2023-08-15
申请号：US17286477
申请日：2019-10-17
Applicant: BASF SE
Inventor： Faissal-Ali El-Toufaili , Dennis Loesch , Anna-Corina Schmidt , Tobias Joachim Zimmermann , Markus Ostermayr , Jack F. Tinsley , Brent Busby , Daniel Barrera-Medrano
CPC classification number: C08L33/26 , C09K8/588 , E21B43/162
Abstract: Process of providing polyacrylamides to a site-of-use comprising at least the steps of mixing a polyacrylamide powder at a manufacturing site with an aqueous liquid, thereby obtaining a homogeneous aqueous polyacrylamide concentrate, transporting said concentrate in a transport unit from the manufacturing site to the site-of-use, and removing the homogeneous aqueous concentrate from the transport unit at the site-of-use. Process of treating subterranean, oil and/or gas bearing formations by injecting an aqueous treatment fluid into at least one wellbore, wherein the aqueous treatment fluid is manufactured by mixing at least an aqueous base fluid with said homogeneous aqueous polyacrylamide concentrate at the site-of-use.
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公开(公告)号：US11608468B2
公开(公告)日：2023-03-21
申请号：US17286469
申请日：2019-10-17
Applicant: BASF SE
Inventor： Faissal-Ali El-Toufaili , Dennis Loesch , Anna-Corina Schmidt , Tobias Joachim Zimmermann , Markus Ostermayr , Jack F. Tinsley , Brent Busby
IPC: C09K8/68 , E21B43/267 , C09K8/88 , E21B15/00
Abstract: Process of fracturing subterranean, oil-and/or gas-bearing formations by injecting an aqueous fracturing fluid into a wellbore at a rate and pressure sufficient to penetrate into the formation, and to initiate or extend fractures in the formation, wherein the aqueous fracturing fluid is obtained by mixing at least an aqueous base fluid and an aqueous polyacrylamide concentrate having a concentration of 3.1 to 14.9% by weight of polyacrylamides, relating to the total of all components of the aqueous polyacrylamide concentrate, and wherein at least a part of the aqueous fracturing fluid injected additionally comprises a proppant.
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公开(公告)号：US11225857B2
公开(公告)日：2022-01-18
申请号：US16627473
申请日：2018-07-11
Applicant: BASF SE
Inventor： Christian Bittner , Guenter Oetter , Jack F. Tinsley , Hans-Christian Raths , Marcel Patrik Kienle , Sebastian Alexander Weisse
Abstract: The present invention relates to a method for the production of crude oil from subterranean, oil-bearing formations comprising at least the following steps of providing an aqueous surfactant composition comprising water and a surfactant mixture, injecting said surfactant composition into the subterranean, oil-bearing formation through at least one injection well, thereby reducing the crude oil-water interfacial tension to less than 0.1 mN/m, and withdrawing crude oil from the formation through at least one production well, wherein the surfactant mixture comprises at least a surfactant (A) having the general formula R1—O—(CH2CH(R2)O)a—(CH2CH(CH3)O)b—(CH2CH2O)c—R3—Y−M+ (I) and a solubility enhancer (B) having the general formula R4—O—(CH2CH(CH3)O)x—(CH2CH2O)y—R3—Y−M+ (II), wherein R1 to R4, a, b, c, x, y, Y and M have the meaning as defined the the description and claims. The invention further relates to said aqueous surfactant composition and methods for preparing the same as well as the use of solubility enhancer (B) for enhancing the solubility of anionic surfactant (A).
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8.发明申请NOVEL ANIONIC POLYALKOXY GROUP COMPRISING SURFACTANTS ON BASIS OF GUERBET-ALCOHOLS, METHOD OF MANUFACTURE AND USE IN ENHANCED OIL RECOVERY (EOR) APPLICATIONS 有权包含表面活性剂的新型阴离子聚烷氧基基团，其用于制备和使用增强油回收（EOR）应用的方法公开(公告)号：US20140182851A1
公开(公告)日：2014-07-03
申请号：US14201323
申请日：2014-03-07
Applicant: BASF SE , Board of Regents, The University of Texas System
Inventor： Upali P. Weerasooriya , Gary A. Pope , Christian Bittner , Gunter Oetter , Jack F. Tinsley , Christian Spindler , Gabriela Alvarez Jurgenson , Sophie Vogel
CPC classification number: C09K8/584 , C07C305/10 , C07C309/10 , C08G65/2609 , C08G65/3344 , E21B43/16
Abstract: Compositions and methods of synthesis of anionic surfactants by alkoxylation of a Guerbet alcohol (GA) having 12 to 36 carbon atoms using butylene oxide, and optionally propylene oxide and/or ethylene oxide followed by the incorporation of a terminal anionic group are described herein. The GA of the present invention is made by a facile and inexpensive method that involves high temperature base catalyzed dimerization of alcohols with 6 to 18 carbon atoms. The large hydrophobe ether surfactants of the present invention find uses in enhanced oil recovery (EOR) applications where it is used for solubilization and mobilization of oil and for environmental cleanup. Further, the hydrophobe alkoxylated GA without anionic terminal group can be used as an ultra-high molecular weight non-ionic surfactant.
Abstract translation: 本文描述了通过使用环氧丁烷和任选的环氧丙烷和/或环氧乙烷烷氧基化具有12至36个碳原子的格伯特醇（GA），然后引入末端阴离子基团来合成阴离子表面活性剂的组合物和方法。 本发明的GA通过易于且廉价的方法制备，其涉及具有6至18个碳原子的醇的高温碱催化二聚。 本发明的大型疏水醚表面活性剂用于增强采油（EOR）应用中，其用于溶解和动员油并用于环境清洁。 此外，不含阴离子末端基团的疏水基烷氧基化GA可用作超高分子量非离子表面活性剂。
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