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    Process for preparing oligo ethylene glycol methyl ether borate
    1.
    发明授权
    Process for preparing oligo ethylene glycol methyl ether borate 有权

    公开(公告)号：US11926639B2

    公开(公告)日：2024-03-12

    申请号：US17756443

    申请日：2020-11-19

    Applicant: BASF SE

    Inventor： Kathrin Luise Mariethres Werth ,  Thomas Holtmann ,  Rainer Papp ,  Mirko Haider ,  Joachim Wulff-Doering

    IPC: C07F5/04

    CPC classification number: C07F5/04

    Abstract: A process for preparing oligo ethylene glycol methyl ether borate involves feeding boric acid and oligo ethylene glycol monomethyl ether into a reactor, and reacting to obtain a raw product containing oligo ethylene glycol methyl ether borate, water, and unreacted boric acid and oligo ethylene glycol monomethyl ether. The raw product is fed to a reactive distillation device and boric acid is reacted with oligo ethylene glycmonomethyl ether for full conversion of boric acid. A distillate stream containing water is transferred from the top of the reactive distillation device to a condenser, and a condensed liquid stream is recycled to the top of the reactive distillation device. A bottom product stream containing oligo ethylene glycol methyl ether borate is withdrawn from the reactive distillation device. The bottom product stream is partially recycled to a reboiler. The resulting vapor stream is recycled to the bottom of the reactive distillation device.

    Process for preparing oligo ethylene glycol methyl ether borate
    4.
    发明申请
    Process for preparing oligo ethylene glycol methyl ether borate 有权

    公开(公告)号：US20230002421A1

    公开(公告)日：2023-01-05

    申请号：US17756443

    申请日：2020-11-19

    Applicant: BASF SE

    Inventor： Kathrin Luise Mariethres WERTH ,  Thomas Holtmann ,  Rainer Papp ,  Mirko Haider ,  Joachim Wulff-Doering

    IPC: C07F5/04

    Abstract: A process for preparing oligo ethylene glycol methyl ether borate involves feeding boric acid and oligo ethylene glycol monomethyl ether into a reactor, and reacting to obtain a raw product containing oligo ethylene glycol methyl ether borate, water, and unreacted boric acid and oligo ethylene glycol monomethyl ether. The raw product is fed to a reactive distillation device and boric acid is reacted with oligo ethylene glycmonomethyl ether for full conversion of boric acid. A distillate stream containing water is transferred from the top of the reactive distillation device to a condenser, and a condensed liquid stream is recycled to the top of the reactive distillation device. A bottom product stream containing oligo ethylene glycol methyl ether borate is withdrawn from the reactive distillation device. The bottom product stream is partially recycled to a reboiler. The resulting vapor stream is recycled to the bottom of the reactive distillation device.

    PROCESS FOR HYDROFORMYLATION OF OLEFINS
    5.
    发明申请
    PROCESS FOR HYDROFORMYLATION OF OLEFINS 有权
    烯烃氢化方法

    公开(公告)号：US20150141702A1

    公开(公告)日：2015-05-21

    申请号：US14542855

    申请日：2014-11-17

    Applicant: BASF SE

    Inventor： Rainer Papp ,  Jens Rudolph ,  Hans-Günter Thelen ,  Klaus Diehl

    IPC: C07C45/50

    CPC classification number: C07C45/50 ,  C07C47/02

    Abstract: In the hydroformylation of olefins having 6 to 20 carbon atoms in the presence of a cobalt catalyst in the presence of an aqueous phase with thorough mixing in a reactor, a hydroformylation products-containing first stream is withdrawn at the top of the reactor and an aqueous phase-containing second stream is withdrawn from the bottom of the reactor. The flow rate of the second stream is controlled in accordance with a temperature which is measured at a point in the bottom of the reactor or in a line leading out of the bottom of the reactor. The yield of crude hydroformylation product is increased as a result of stable sustained operation.

    Abstract translation: 在钴催化剂存在下，在水相存在下，在反应器中充分混合的情况下，在具有6至20个碳原子的烯烃的加氢甲酰基化中，在反应器顶部取出含有加氢甲酰化产物的第一物流， 从反应器的底部排出含相的第二物流。 根据在反应器底部或通过反应器底部的管线中测量的温度来控制第二流的流速。 由于稳定的持续操作，粗加氢甲酰化产物的产率增加。

    Hydroformylation method for the large-scale production of aldehydes and/or alcohols
    6.
    发明授权
    Hydroformylation method for the large-scale production of aldehydes and/or alcohols 有权

    公开(公告)号：US11014863B2

    公开(公告)日：2021-05-25

    申请号：US16613307

    申请日：2018-05-14

    Applicant: BASF SE

    Inventor： Stephan Zuend ,  Rainer Papp ,  Boris Breitscheidel ,  Armin Lange De Oliveira

    IPC: C07C29/00 ,  B01J23/00 ,  C07C29/149 ,  B01J23/72 ,  C07C31/12

    Abstract: A process for preparing C4 to C13 monohydroxy compounds from a bottom fraction arising in the distillation of a crude mixture of C4 to C13 oxo-process aldehydes from cobalt-catalyzed or rhodium-catalyzed hydroformylation, or in the distillation of a crude mixture of C4 to C13 oxo-process alcohols, which comprises contacting the bottom fraction in the presence of hydrogen with a catalyst comprising copper oxide and aluminum oxide, at a temperature of 150° C. to 300° C. and a pressure of 20 bar to 300 bar and subjecting the resulting crude hydrogenation product to distillation, and the amount of C4 to C13 monohydroxy compounds present in the crude hydrogenation product after the hydrogenation being greater than the amount of C4 to C13 monohydroxy compounds given stoichiometrically from the hydrogenation of the ester and aldehyde compounds present in the bottom fraction, including the C4 to C13 monohydroxy compounds still present in the bottom fraction before the hydrogenation.

    Cylindrical reactor and use thereof for continuous hydroformylation
    7.
    发明授权
    Cylindrical reactor and use thereof for continuous hydroformylation 有权

    公开(公告)号：US10315182B2

    公开(公告)日：2019-06-11

    申请号：US16064756

    申请日：2016-12-21

    Applicant: BASF SE

    Inventor： Rainer Papp ,  Oliver Christian Gobin ,  Oliver Bey ,  Jens Rudolph ,  Hans-Günter Thelen

    IPC: C07C45/50 ,  B01J10/00 ,  B01J19/24 ,  B01J19/00

    Abstract: Proposed is a cylindrical reactor (1) having a vertical longitudinal axis for continuous hydroformylation of a C6-C20-olefin or a mixture of C6-C20-olefins with synthesis gas in the presence of a homogeneously dissolved metal carbonyl complex catalyst, having a multiplicity of Field tubes (2) which are oriented parallel to the longitudinal axis of the reactor (1) and welded into a tube plate at the upper end of the reactor (1), having a circulation tube (3) open at both ends which envelops the Field tubes (2) and at its lower end projects beyond said tubes, having a jet nozzle (4) at the bottom of the reactor (1) for injecting the reactant mixture comprising the C6-C20-olefin, the synthesis gas and the metal carbonyl complex catalyst, wherein the Field tubes (2) are configured in terms of their number and their dimensions such that the total heat exchanger area of said tubes per unit internal volume of the reactor is in the range from 1 m2/m3 to 11 m2/m3 and the cross sectional area occupied by the Field tubes (2) per unit cross sectional area of the circulation tube (3) is in the range from 0.03 m2/m2 to 0.30 m2/m2, a gas distributor ring (5) is provided at the lower end of the circulation tube (3), at the inner wall thereof, via which a substream of the synthesis gas is feedable, and wherein one or more distributor trays (6) are provided in the circulation tube (3).

    Process for hydroformylation of olefins
    8.
    发明授权
    Process for hydroformylation of olefins 有权
    烯烃加氢甲酰化方法

    公开(公告)号：US09115069B2

    公开(公告)日：2015-08-25

    申请号：US14542855

    申请日：2014-11-17

    Applicant: BASF SE

    Inventor： Rainer Papp ,  Jens Rudolph ,  Hans-Günter Thelen ,  Klaus Diehl

    IPC: C07C45/50

    CPC classification number: C07C45/50 ,  C07C47/02

    Abstract: In the hydroformylation of olefins having 6 to 20 carbon atoms in the presence of a cobalt catalyst in the presence of an aqueous phase with thorough mixing in a reactor, a hydroformylation products-containing first stream is withdrawn at the top of the reactor and an aqueous phase-containing second stream is withdrawn from the bottom of the reactor. The flow rate of the second stream is controlled in accordance with a temperature which is measured at a point in the bottom of the reactor or in a line leading out of the bottom of the reactor. The yield of crude hydroformylation product is increased as a result of stable sustained operation.

    Abstract translation: 在钴催化剂存在下，在水相存在下，在反应器中充分混合的情况下，在具有6至20个碳原子的烯烃的加氢甲酰基化中，在反应器顶部取出含有加氢甲酰化产物的第一物流， 从反应器的底部排出含相的第二物流。 根据在反应器底部或通过反应器底部的管线中测量的温度来控制第二流的流速。 由于稳定的持续操作，粗加氢甲酰化产物的产率增加。

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