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    Continuous method for producing ortho-substituted anilines in a flow reactor
    1.
    发明授权
    Continuous method for producing ortho-substituted anilines in a flow reactor 有权
    在流动反应器中生产邻位取代的苯胺的连续方法

    公开(公告)号：US09527808B2

    公开(公告)日：2016-12-27

    申请号：US14427471

    申请日：2013-09-12

    Applicant: BAYER CROPSCIENCE AG ,  BAYER TECHNOLOGY SERVICES GMBH

    Inventor： Mark James Ford ,  Christian Severins

    IPC: C07C211/00 ,  C07C319/20 ,  C07D251/16 ,  C07D209/34 ,  C07D251/20 ,  C07D403/04

    CPC classification number: C07C319/20 ,  C07D209/34 ,  C07D251/16 ,  C07D251/20 ,  C07D403/04 ,  C07C323/58

    Abstract: Continuous process for preparing ortho-substituted anilines of the formula in a flow reactor in the presence of a nitrogen base not having an NH group, and multistage process for preparing herbicidal N-alkyl-N-[2-(1,3,5-triazin-2-ylcarbonyl)-phenyl]alkansulphonamides of the formula (4-1) wherein the continuous process for preparing ortho-substituted anilines of the formula (4) in a flow reactor constitutes the first process step of the multistage process for preparing the herbicidal active ingredients of the formula (4-1).

    Abstract translation: 用于在流动反应器中生产邻位取代的苯胺的连续方法在不具有NH基团的氮基的存在下，在流动反应器中制备邻位取代的苯胺的连续方法，以及用于制备除草N-烷基 - 式（4-1）的N- [2-（1,3,5-三嗪-2-基羰基） - 苯基]烷磺酰胺，其中在流动反应器中制备式（4）的邻位取代的苯胺的连续方法 构成了用于制备式（4-1）的除草活性成分的多级方法的第一种方法步骤。

    Alkaline earth metal-complexed metal bisamides
    3.
    发明授权
    Alkaline earth metal-complexed metal bisamides 有权
    碱土金属络合金属双酰胺

    公开(公告)号：US09334292B2

    公开(公告)日：2016-05-10

    申请号：US14378998

    申请日：2013-02-13

    Applicant: BAYER INTELLECTUAL PROPERTY GMBH ,  BAYER CROPSCIENCE AG

    Inventor： Mark James Ford ,  Marc Mosrin

    IPC: C07F3/06 ,  C07F3/02

    CPC classification number: C07F3/06 ,  C07D211/12 ,  C07F19/005

    Abstract: The present invention relates to alkaline earth metal-complexed metal bisamides of the formula (I), to a process for preparation thereof and to the use thereof for metallation of aromatics, heteroaromatics, alkenes, alkynes and other organic compounds having activated C—H bonds.

    Abstract translation: 本发明涉及式（I）的碱土金属络合金属双酰胺，其制备方法及其用于芳族化合物，杂芳族化合物，烯烃，炔烃和其它具有活化C-H键的有机化合物的金属化的用途 。

    Process for the preparation of oxindoles and ortho-substituted anilines and their use as intermediates for syntheses
    4.
    发明授权
    Process for the preparation of oxindoles and ortho-substituted anilines and their use as intermediates for syntheses 有权
    制备羟吲哚和邻位取代苯胺的方法及其作为合成中间体的用途

    公开(公告)号：US09242934B2

    公开(公告)日：2016-01-26

    申请号：US13915898

    申请日：2013-06-12

    Applicant: Bayer CropScience AG

    Inventor： Mark James Ford ,  Gunter Karig

    IPC: C07D209/34 ,  C07C323/58

    CPC classification number: C07D209/34 ,  C07C323/58

    Abstract: The present invention relates to processes for the preparation of oxindoles and ortho-substituted anilines and their use as intermediates for syntheses. The invention further relates to a process for the preparation of compounds of formula (4): where a mixture of an aniline (compound of formula Q) is reacted with a thioether (compound of formula W): in the presence of a chlorinating agent and an organic solvent at a reaction temperature in the range above −65° C. In a subsequent process, this compound is further reacted in the presence of an acid catalyst to give the indole of formula (7) or the oxindole of formula (8):

    Abstract translation: 本发明涉及制备羟吲哚和邻位取代苯胺的方法及其作为合成中间体的用途。 本发明还涉及制备式（4）化合物的方法：其中苯胺（式Q化合物）的混合物与硫醚（式W化合物）反应：在氯化剂和 在随后的方法中，该化合物在酸催化剂的存在下进一步反应，得到式（7）的吲哚或式（8）的羟吲哚， ：

    CONTINUOUS METHOD FOR PRODUCING ORTHO-SUBSTITUTED ANILINES IN A FLOW REACTOR
    5.
    发明申请
    CONTINUOUS METHOD FOR PRODUCING ORTHO-SUBSTITUTED ANILINES IN A FLOW REACTOR 有权
    在流动反应器中生产正交取代的苯胺的连续方法

    公开(公告)号：US20150210637A1

    公开(公告)日：2015-07-30

    申请号：US14427471

    申请日：2013-09-12

    Applicant: BAYER CROPSCIENCE AG ,  BAYER TECHNOLOGY SERVICES GmbH

    Inventor： Mark James Ford ,  Christian Severins

    IPC: C07C319/20 ,  C07D403/04 ,  C07D251/20 ,  C07D209/34

    CPC classification number: C07C319/20 ,  C07D209/34 ,  C07D251/16 ,  C07D251/20 ,  C07D403/04 ,  C07C323/58

    Abstract: Continuous method for producing ortho-substituted anilines in a flow reactorContinuous process for preparing ortho-substituted anilines of the formula in a flow reactor in the presence of a nitrogen base not having an NH group, and multistage process for preparing herbicidal N-alkyl-N-[2-(1,3,5-triazin-2-ylcarbonyl)-phenyl]alkansulphonamides of the formula (4-1) wherein the continuous process for preparing ortho-substituted anilines of the formula (4) in a flow reactor constitutes the first process step of the multistage process for preparing the herbicidal active ingredients of the formula (4-1).

    Abstract translation: 用于在流动反应器中生产邻位取代的苯胺的连续方法在不具有NH基团的氮基的存在下，在流动反应器中制备邻位取代的苯胺的连续方法，以及用于制备除草N-烷基 - 式（4-1）的N- [2-（1,3,5-三嗪-2-基羰基） - 苯基]烷磺酰胺，其中在流动反应器中制备式（4）的邻位取代的苯胺的连续方法 构成了用于制备式（4-1）的除草活性成分的多级方法的第一种方法步骤。

    PROCESS FOR THE PREPARATION OF OXINDOLES AND ORTHO-SUBSTITUTED ANILINES AND THEIR USE AS INTERMEDIATES FOR SYNTHESES
    8.
    发明申请
    PROCESS FOR THE PREPARATION OF OXINDOLES AND ORTHO-SUBSTITUTED ANILINES AND THEIR USE AS INTERMEDIATES FOR SYNTHESES 有权
    制备氧化物和取代的苯胺的方法及其作为合成中间体的使用

    公开(公告)号：US20130281711A1

    公开(公告)日：2013-10-24

    申请号：US13915898

    申请日：2013-06-12

    Applicant: Bayer CropScience AG

    Inventor： Mark James Ford ,  Gunter Karig

    IPC: C07D209/34

    CPC classification number: C07D209/34 ,  C07C323/58

    Abstract: The present invention relates to processes for the preparation of oxindoles and ortho-substituted anilines and their use as intermediates for syntheses. The invention further relates to a process for the preparation of compounds of formula (4): where a mixture of an aniline (compound of formula Q) is reacted with a thioether (compound of formula W): in the presence of a chlorinating agent and an organic solvent at a reaction temperature in the range above −65° C.In a subsequent process, this compound is further reacted in the presence of an acid catalyst to give the indole of formula (7) or the oxindole of formula (8):

    Abstract translation: 本发明涉及制备羟吲哚和邻位取代苯胺的方法及其作为合成中间体的用途。 本发明还涉及制备式（4）化合物的方法：其中苯胺（式Q化合物）的混合物与硫醚（式W化合物）反应：在氯化剂和 在随后的方法中，该化合物在酸催化剂的存在下进一步反应，得到式（7）的吲哚或式（8）的羟吲哚， ：

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