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公开(公告)号：US09522981B1
公开(公告)日：2016-12-20
申请号：US15189624
申请日：2016-06-22
发明人： Klaus Dziwok , Helmut Coutelle , Robert G. Briell , Tyler Nash
CPC分类号： C08J3/203 , C01B33/44 , C08J2331/00 , C08J2363/00 , C08J2367/02 , C08K3/346 , C08K9/04 , C08L63/00 , C08L67/06 , C09D7/44 , C09D163/00 , C09D167/06 , C09J11/06 , C09J163/00 , C09J167/06 , C09K8/18 , C09K8/20 , C08K3/34
摘要： The invention relates to the use of at least one mixed mineral organoclay rheology additive, which comprises or consists of a quaternary alkyl-ammonium salt treated mineral clay mixture prepared by forming an aqueous hormite clay slurry (a), forming an aqueous smectite clay slurry (b), combining the aqueous hormite clay slurry (a) with the aqueous smectite clay slurry (b) to form a combined clay slurry (c), treating the combined clay slurry (c) with one or more quaternary alkyl-ammonium salts, in which the aqueous hormite clay slurry (a) being formed by dispersing a fraction of one or more hormite clays selected from the group of sepiolites and palygorskites in an aqueous medium to form a dispersion, and whereby the hormite clay fraction employed contains less than 3.0% by weight of Al2O3, less than 1.0% by weight of Fe2O3, and less than 3.5% by weight of the combination of Al2O3 and Fe2O3; and the aqueous smectite clay slurry (b) being formed by dispersing a fraction of one or more smectite clays in an aqueous medium to form a dispersion, and in that the weight of the hormite clay content exceeds the weight of the smectite clay content in the combined clay slurry (c); and subjecting the hormite clay slurry (a) and the smectite clay slurry (b) to high speed fluid shear before combining both slurries and/or after having both slurries combined and wherein the one or more hormite clays employed in the formation of the aqueous hormite clay slurry (a) exhibit a methylene blue exchange capacity below 20 mmol methylene blue per 100 g of the one or more hormite clays in dry state and whereby the hormite clay fraction employed in the formation of the aqueous hormite clay slurry (a) shows an integral breadth B=(net area of reflection)/(net height of reflection) of the (110) reflection in an X-ray powder pattern recorded on an oriented glycolated sample of the hormite clay fraction using CuKα-radiation of less than 0.800 scan units, in a liquid composition. The invention also relates to a process for producing a mixed mineral organoclay rheology additive and the use of the thus produced additive as a thickening agent in liquid compositions.
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公开(公告)号：US09546252B1
公开(公告)日：2017-01-17
申请号：US15189584
申请日：2016-06-22
发明人： Klaus Dziwok , Helmut Coutelle , Robert G. Briell , Tyler Nash
CPC分类号： C09J11/06 , C08J3/215 , C08J2367/02 , C08K3/346 , C08K9/04 , C08L67/06 , C09D7/43 , C09D167/06 , C09J167/06 , C09K8/14 , C08K3/34
摘要： The invention relates to the use of at least one mixed mineral organoclay rheology additive, which comprises or consists of a quaternary alkyl-ammonium salt treated mineral clay mixture prepared by forming an aqueous hormite clay slurry (a), forming an aqueous smectite clay slurry (b), combining the aqueous hormite clay slurry (a) with the aqueous smectite clay slurry (b) to form a combined clay slurry (c), treating the combined clay slurry (c) with one or more quaternary alkyl-ammonium salts, separating the thus produced quaternary alkyl-ammonium salt treated mineral clay mixture from the aqueous medium, in which the aqueous hormite clay slurry (a) being formed by (i.1) dispersing a fraction of one or more hormite clays selected from the group of sepiolites and palygorskites in an aqueous medium to form a dispersion, and the aqueous smectite clay slurry (b) being formed by (ii.1) dispersing a fraction of one or more smectite clays in an aqueous medium to form a dispersion, and in that the weight of the hormite clay content exceeds the weight of the smectite clay content in the combined clay slurry (c), and subjecting the dispersions formed in (i.1) and (ii.1) to high speed fluid shear before carrying out step iii. and/or after having carried out step and wherein the fraction of one or more hormite clays employed in the formation of the aqueous hormite clay slurry (a) has an integral breadth B defined according of the reflection with Miller indices (110) of less than 0.800 scan units in an X-ray powder pattern recorded on an oriented glycolated sample of the hormite clay fraction using Cu-Kα1-radiation, in a liquid composition comprising at least one unsaturated polyester. The invention also relates to a process for producing a mixed mineral organoclay rheology additive and the use of the thus produced additive as a thickening agent in liquid compositions.
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公开(公告)号：US09670339B1
公开(公告)日：2017-06-06
申请号：US15355447
申请日：2016-11-18
申请人： BYK-Chemie, GmbH , BYK USA, Inc.
发明人： Klaus Dziwok , Helmut Coutelle , Robert G. Briell , Tyler Nash
CPC分类号： C08K9/04 , C01B33/44 , C08J3/203 , C08J2363/02 , C08K3/346 , C08K5/19 , C09C1/42 , C08L63/00
摘要： The invention relates to the use of at least one mixed mineral organoclay rheology additive in a liquid composition comprising at least one epoxy resin, the additive comprises or consists of a quaternary alkyl-ammonium salt treated mineral clay mixture prepared by forming an aqueous hormite clay slurry (a), forming an aqueous smectite clay slurry (b), combining the aqueous hormite clay slurry (a) with the aqueous smectite clay slurry (b) to form a combined clay slurry (c), treating the combined clay slurry (c) with one or more quaternary alkyl-ammonium salts, and separating the produced quaternary alkyl-ammonium salt treated mineral clay mixture from the aqueous medium. The invention also relates to a process for producing a mixed mineral organoclay rheology additive and the use of the thus produced additive as a thickening agent in liquid compositions.
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公开(公告)号：US20240308859A1
公开(公告)日：2024-09-19
申请号：US18271487
申请日：2022-01-13
申请人： BYK-Chemie GmbH
发明人： Hussein Kalo , Hubert Schiessling , Udo Krappe , Berthold Jacobs , Maximilian Böhmer , Tyler Nash
CPC分类号： C01B33/22 , C09C1/3018 , C09C3/041 , C09D7/61 , C01P2002/72 , C01P2004/61
摘要： The invention relates to material comprising a layered material having the composition Nax[Mg3-zLiy]Si4O10(T)2, wherein x is in the range of 0.4 to 0.8, y is in the range of 0.0 to 0.8, 5z is in the range of 0.2 to 0.8, T independent of each occurrence represents F or OH, and x+(3−z)+y≤4, wherein the powder X-ray diffraction pattern of the layered material has a 001 peak in the range of 8.00 to 5.88° 2Theta, and wherein the 001 peak has a full width at half of the peak maximum 10 of larger than 0.10°, and wherein the layered material has a Z-average particle size of 500 nm or higher, determined by dynamic laser light scattering on an aqueous dispersion of the material containing at most 1.5% by weight of the material.
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公开(公告)号：US09637614B1
公开(公告)日：2017-05-02
申请号：US15355514
申请日：2016-11-18
申请人： BYK-Chemie, GmbH , BYK USA, Inc.
发明人： Klaus Dziwok , Helmut Coutelle , Robert G. Briell , Tyler Nash
摘要： The invention relates to the use of at least one mixed mineral organoclay rheology additive, which comprises or consists of a quaternary alkyl-ammonium salt treated mineral clay mixture prepared by forming an aqueous hormite clay slurry (a), forming an aqueous smectite clay slurry (b), combining the aqueous hormite clay slurry (a) with the aqueous smectite clay slurry (b) to form a combined clay slurry (c), treating the combined clay slurry (c) with one or more quaternary alkyl-ammonium salts, and separating the thus produced quaternary alkyl-ammonium salt treated mineral clay mixture from the aqueous medium. The invention also relates to a process for producing a mixed mineral organoclay rheology additive and the use of the thus produced additive as a thickening agent in liquid compositions.
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