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    Free-radical-initiated crosslinking of polymers
    2.
    发明申请
    Free-radical-initiated crosslinking of polymers 审中-公开
    自由基引发的聚合物交联

    公开(公告)号：US20070173613A1

    公开(公告)日：2007-07-26

    申请号：US10583299

    申请日：2004-12-24

    申请人： Bharat Chaudhary ,  Yunwa Cheung ,  Randall Cuntala ,  Mohamed Esseghir ,  John Klier

    发明人： Bharat Chaudhary ,  Yunwa Cheung ,  Randall Cuntala ,  Mohamed Esseghir ,  John Klier

    IPC分类号： C08F8/30

    CPC分类号： C08L101/00 ,  C08F8/30 ,  C08K5/14 ,  C08K5/3435 ,  C08L23/10 ,  C08L23/22 ,  C08L2666/04

    摘要： The present invention is a free-radical carbon-FRTS-carbon crosslinkable polymeric composition. The resulting carbon-FRTS-carbon crosslinked polymer is prepared from at least one polymer which upon forming free radicals preferentially degrades or carbon-carbon crosslinks. The present invention permits suppression of the preferential reaction while permitting the polymer to be carbon-FRTS-carbon crosslinked through a free-radical trapping species. Suppressing the undesirable degradation or carbon-carbon crosslinking reaction and permitting the desirable carbon-FRTS-carbon crosslinking reaction yield a uniquely crosslinked polymer.

    摘要翻译： 本发明是一种自由基碳-FRTS-碳可交联聚合物组合物。 所得到的碳-FRTS-碳交联聚合物由至少一种形成自由基优先降解或碳 - 碳交联的聚合物制备。 本发明允许抑制优选反应，同时允许聚合物是通过自由基捕获物质交联的碳-FRTS-碳。 抑制不期望的降解或碳 - 碳交联反应并允许所需的碳-FFR-碳交联反应产生独特的交联聚合物。

    Rheology modification of polymers
    3.
    发明申请
    Rheology modification of polymers 审中-公开
    聚合物的流变改性

    公开(公告)号：US20070142565A1

    公开(公告)日：2007-06-21

    申请号：US10583296

    申请日：2004-12-24

    申请人： Bharat Chaudhary ,  Randall Cuntala ,  Mohamed Esseghir ,  John Klier ,  Yunwa Cheung

    发明人： Bharat Chaudhary ,  Randall Cuntala ,  Mohamed Esseghir ,  John Klier ,  Yunwa Cheung

    IPC分类号： C08F120/10

    CPC分类号： C08F8/50

    摘要： The present invention is a rheology-modifiable polymeric composition. The resulting rheology-modified polymer is prepared from at least one polymer which upon forming free radicals preferentially degrades or carbon-carbon crosslinks. The present invention permits suppression of the preferential reaction while permitting the polymer to be coupled through a free-radical trapping species. Suppressing the undesirable degradation or carbon-carbon crosslinking reaction and permitting the desirable coupling reaction yield a rheology-modified polymer.

    摘要翻译： 本发明是可流变改性的聚合物组合物。 所得到的流变改性聚合物由至少一种形成自由基优先降解或碳 - 碳交联的聚合物制备。 本发明允许抑制优选反应，同时允许聚合物通过自由基捕获物质偶联。 抑制不期望的降解或碳 - 碳交联反应并允许所需的偶联反应产生流变改性聚合物。

    Silane moisture cured heat resistant fibers made from polyolefin elastomers
    4.
    发明申请
    Silane moisture cured heat resistant fibers made from polyolefin elastomers 审中-公开
    由聚烯烃弹性体制成的硅烷湿固化耐热纤维

    公开(公告)号：US20060100385A1

    公开(公告)日：2006-05-11

    申请号：US10541829

    申请日：2004-02-04

    申请人： Parvinder Walia ,  Rajen Patel ,  John Klier ,  John Weaver ,  Mladen Ladika ,  Mohamed Esseghir ,  Jeffrey Cogen

    发明人： Parvinder Walia ,  Rajen Patel ,  John Klier ,  John Weaver ,  Mladen Ladika ,  Mohamed Esseghir ,  Jeffrey Cogen

    IPC分类号： C08F297/02

    CPC分类号： D01F6/30 ,  C08F8/42 ,  C08F255/00 ,  C08F255/02 ,  C08L51/06 ,  C08F10/00 ,  C08F230/08 ,  C08L2666/02

    摘要： An improved process for crosslinking a polyolefin polymer is described. The process involves grafting a silane material onto the polyolefin based polymer in the presence of a free radical generating initiator material and then hydrolyzing the silane material to form crosslinks. By using an effective molar ratio of silane material to free radical of 40 or greater in the grafting reaction, premature crosslinking is controlled and the grafted polymer can be shaped first and then crosslinked. In another aspect of the invention, the crosslinking process is improved by adding a catalyst for the hydrolysis catalyst to the surface of a shaped article made from the grafted polymer. Grafted polymer and articles made from the grafted polymer, particularly fibers, are also disclosed.

    摘要翻译： 描述了一种交联聚烯烃聚合物的改进方法。 该方法包括在产生自由基的引发剂材料的存在下将硅烷材料接枝到聚烯烃基聚合物上，然后水解硅烷材料以形成交联。 通过在接枝反应中使用硅烷材料与自由基的自由基的有效摩尔比为40以上，控制过早交联，接枝聚合物首先被成型然后交联。 在本发明的另一方面，通过向由接枝聚合物制成的成型制品的表面添加用于水解催化剂的催化剂来改善交联过程。 接枝聚合物和由接枝聚合物，特别是纤维制成的制品也被公开。

    Nitroxide Compounds for Minimizing Scorch in Crosslinkable Compositions
    5.
    发明申请
    Nitroxide Compounds for Minimizing Scorch in Crosslinkable Compositions 失效
    用于最小化可交联组合物焦烧的硝酸化合物

    公开(公告)号：US20090069469A1

    公开(公告)日：2009-03-12

    申请号：US12267909

    申请日：2008-11-10

    申请人： Mohamed Esseghir ,  Bharat I. Chaudhary ,  Jeffrey M. Cogen ,  John Klier ,  Jinder Jow ,  Robert F. Eaton ,  Suzanne M. Guerra

    发明人： Mohamed Esseghir ,  Bharat I. Chaudhary ,  Jeffrey M. Cogen ,  John Klier ,  Jinder Jow ,  Robert F. Eaton ,  Suzanne M. Guerra

    IPC分类号： C08K5/3435 ,  C07D211/94

    CPC分类号： C08F2/38 ,  C08F4/00 ,  C08K5/0025 ,  C08K5/3435

    摘要： Scorch is inhibited during the free-radical crosslinking of a crosslinkable polymer, e.g., an EPDM, by incorporating into the polymer before melt processing and crosslinking a scorch inhibiting amount of a derivative, preferably an ether, ester or urethane derivative, of a TEMPO compound, e.g., 4-hydroxy-tetrahydrocarbylpiperidin-1-oxyl. The scorch inhibitors of this invention perform as well, if not better, than their 4-hydroxy-tetrahydrocarbylpiperidin-1-oxyl counterparts in similar polymer compositions and under similar conditions in terms of scorch inhibition and ultimate degree of crosslinking, but exhibit less volatility and less migration within the polymer composition.

    摘要翻译： 在可交联聚合物（例如EPDM）的自由基交联期间，通过在熔融加工和交联焦烧抑制量的TEMPO化合物的衍生物，优选醚，酯或氨基甲酸酯衍生物的交联之前引入聚合物中，焦烧被抑制 ，例如4-羟基 - 四氢环丁基哌啶-1-基。 在类似的聚合物组合物和类似的条件下，本发明的焦烧抑制剂（如果不是更好）也与其4-羟基 - 四烃基哌啶-1-氧基对应物一样，在焦烧抑制和最终交联度方面也表现出较低的挥发性， 聚合物组合物内迁移少。

    Nitroxide compounds for minimizing scorch in crosslinkable compositions
    6.
    发明授权
    Nitroxide compounds for minimizing scorch in crosslinkable compositions 失效
    用于最小化可交联组合物中焦化的硝酸氧化物

    公开(公告)号：US07465769B2

    公开(公告)日：2008-12-16

    申请号：US11539815

    申请日：2006-10-09

    申请人： Mohamed Esseghir ,  Bharat I. Chaudhary ,  Jeffrey M. Cogen ,  John Klier ,  Jinder Jow ,  Robert F. Eaton ,  Suzanne M. Guerra

    发明人： Mohamed Esseghir ,  Bharat I. Chaudhary ,  Jeffrey M. Cogen ,  John Klier ,  Jinder Jow ,  Robert F. Eaton ,  Suzanne M. Guerra

    IPC分类号： C08F8/30

    CPC分类号： C08F2/38 ,  C08F4/00 ,  C08K5/0025 ,  C08K5/3435

    摘要： Scorch is inhibited during the free-radical crosslinking of a crosslinkable polymer, e.g., an EPDM, by incorporating into the polymer before melt processing and crosslinking a scorch inhibiting amount of a derivative, preferably an ether, ester or urethane derivative, of a TEMPO compound, e.g., 4-hydroxy-tetrahydrocarbylpiperidin-1-oxyl. The scorch inhibitors of this invention perform as well, if not better, than their 4-hydroxy-tetrahydrocarbylpiperidin-1-oxyl counterparts in similar polymer compositions and under similar conditions in terms of scorch inhibition and ultimate degree of crosslinking, but exhibit less volatility and less migration within the polymer composition.

    摘要翻译： 在可交联聚合物（例如EPDM）的自由基交联期间，通过在熔融加工和交联焦烧抑制量的TEMPO化合物的衍生物，优选醚，酯或氨基甲酸酯衍生物的交联之前引入聚合物中，焦烧被抑制 ，例如4-羟基 - 四氢环丁基哌啶-1-基。 在类似的聚合物组合物和类似的条件下，本发明的焦烧抑制剂（如果不是更好）也与其4-羟基 - 四烃基哌啶-1-氧基对应物一样，在焦烧抑制和最终交联度方面也表现出较低的挥发性， 聚合物组合物内迁移少。

    Nitroxide Compounds for Minimizing Scorch in Crosslinkable Compositions
    7.
    发明申请
    Nitroxide Compounds for Minimizing Scorch in Crosslinkable Compositions 失效
    用于最小化可交联组合物焦烧的硝酸化合物

    公开(公告)号：US20080085973A1

    公开(公告)日：2008-04-10

    申请号：US11539815

    申请日：2006-10-09

    申请人： Mohamed Esseghir ,  Bharat I. Chaudhary ,  Jeffrey M. Cogen ,  John Klier ,  Jinder Jow ,  Robert F. Eaton ,  Suzanne M. Guerra

    发明人： Mohamed Esseghir ,  Bharat I. Chaudhary ,  Jeffrey M. Cogen ,  John Klier ,  Jinder Jow ,  Robert F. Eaton ,  Suzanne M. Guerra

    IPC分类号： C07D211/00 ,  C08F2/38

    CPC分类号： C08F2/38 ,  C08F4/00 ,  C08K5/0025 ,  C08K5/3435

    摘要： Scorch is inhibited during the free-radical crosslinking of a crosslinkable polymer, e.g., an EPDM, by incorporating into the polymer before melt processing and crosslinking a scorch inhibiting amount of a derivative, preferably an ether, ester or urethane derivative, of a TEMPO compound, e.g., 4-hydroxy-tetrahydrocarbylpiperidin-1-oxyl. The scorch inhibitors of this invention perform as well, if not better, than their 4-hydroxy-tetrahydrocarbylpiperidin-1-oxyl counterparts in similar polymer compositions and under similar conditions in terms of scorch inhibition and ultimate degree of crosslinking, but exhibit less volatility and less migration within the polymer composition.

    摘要翻译： 在可交联聚合物（例如EPDM）的自由基交联期间，通过在熔融加工和交联焦烧抑制量的TEMPO化合物的衍生物，优选醚，酯或氨基甲酸酯衍生物的交联之前引入聚合物中，焦烧被抑制 ，例如4-羟基 - 四氢环丁基哌啶-1-基。 在类似的聚合物组合物和类似的条件下，本发明的焦烧抑制剂（如果不是更好）也与其4-羟基 - 四烃基哌啶-1-氧基对应物一样，在焦烧抑制和最终交联度方面也表现出较低的挥发性， 聚合物组合物内迁移少。

    Nitroxide compounds for minimizing scorch in crosslinkable compositions
    8.
    发明授权
    Nitroxide compounds for minimizing scorch in crosslinkable compositions 失效
    用于最小化可交联组合物中焦化的硝酸氧化物

    公开(公告)号：US07842759B2

    公开(公告)日：2010-11-30

    申请号：US12267909

    申请日：2008-11-10

    申请人： Mohamed Esseghir ,  Bharat I. Chaudhary ,  Jeffrey M. Cogen ,  John Klier ,  Jinder Jow ,  Robert F. Eaton ,  Suzanne M. Guerra

    发明人： Mohamed Esseghir ,  Bharat I. Chaudhary ,  Jeffrey M. Cogen ,  John Klier ,  Jinder Jow ,  Robert F. Eaton ,  Suzanne M. Guerra

    IPC分类号： C08F8/30

    CPC分类号： C08F2/38 ,  C08F4/00 ,  C08K5/0025 ,  C08K5/3435

    摘要： Scorch is inhibited during the free-radical crosslinking of a crosslinkable polymer, e.g., an EPDM, by incorporating into the polymer before melt processing and crosslinking a scorch inhibiting amount of a derivative, preferably an ether, ester or urethane derivative, of a TEMPO compound, e.g., 4-hydroxy-tetrahydrocarbylpiperidin-1-oxyl. The scorch inhibitors of this invention perform as well, if not better, than their 4-hydroxy-tetrahydrocarbylpiperidin-1-oxyl counterparts in similar polymer compositions and under similar conditions in terms of scorch inhibition and ultimate degree of crosslinking, but exhibit less volatility and less migration within the polymer composition.

    摘要翻译： 在可交联聚合物（例如EPDM）的自由基交联期间，通过在熔融加工和交联焦烧抑制量的TEMPO化合物的衍生物，优选醚，酯或氨基甲酸酯衍生物的交联之前引入聚合物中，焦烧被抑制 ，例如4-羟基 - 四氢环丁基哌啶-1-基。 在类似的聚合物组合物和类似的条件下，本发明的焦烧抑制剂（如果不是更好）也与其4-羟基 - 四烃基哌啶-1-氧基对应物一样，在焦烧抑制和最终交联度方面也表现出较低的挥发性， 聚合物组合物内迁移少。