Process and apparatus for flow injection extraction
    1.
    发明授权
    Process and apparatus for flow injection extraction 失效
    流动注射提取的工艺和设备

    公开(公告)号:US4399102A

    公开(公告)日:1983-08-16

    申请号:US232214

    申请日:1981-02-06

    IPC分类号: B01D11/04 G01N35/08 G01N1/14

    摘要: A process and an apparatus for flow extraction whereby a substance dissolved in a first solvent is extracted over to a second solvent which is insoluble in the first. The two solvents are brought together via two legs in a T-tube, and the mixture exits through the third leg, the cross-sectional areas of the legs being dimensioned to produce segmented flow with alternating plugs of the second and first solvents. The ratio between the cross-sectional areas of the tube legs for the first and second solvents is 2-8:1, preferably 4:1. Between the first and third legs carrying the confluent flows, the ratio between the cross-sectional areas thereof is reduced to 0.7-1.2:1, preferably 1:1, at a distance from the juncture which is 1-3 times the inner diameter of the third leg. The confluent flow is led through a spiral hose, producing a powerful extraction due to the counter-current turbulence.

    摘要翻译: 一种用于流动提取的方法和装置,其中溶解在第一溶剂中的物质被萃取到不溶于第一溶剂的第二溶剂中。 这两种溶剂通过T型管中的两条腿接合在一起,并且混合物通过第三腿离开,腿的横截面面积的尺寸被设计成产生具有第二和第一溶剂的交替塞的分段流。 第一和第二溶剂的管腿的横截面积之间的比率为2-8:1,优选为4:1。 在承载汇合流动的第一和第三腿之间,其横截面积之间的比率在距离接合点的1-3倍的距离处减小到0.7-1.2:1,优选为1:1, 第三条腿 汇合流动通过螺旋软管引导,由于逆流湍流产生强大的提取。

    Process for flow injection extraction
    2.
    发明授权
    Process for flow injection extraction 失效
    流动注射提取工艺

    公开(公告)号:US4546088A

    公开(公告)日:1985-10-08

    申请号:US482054

    申请日:1983-04-04

    IPC分类号: B01D11/04 G01N35/08 G01N1/00

    摘要: A process and an apparatus for flow extraction whereby a substance dissolved in a first solvent is extracted over to a second solvent which is insoluble in the first. The two solvents are brought together via two legs in a T-tube, and the mixture exits through the third leg, the cross-sectional areas of the legs being dimensioned to produce segmented flow with alternating plugs of the second and first solvents. The ratio between the cross-sectional areas of the tube legs for the first and second solvents is 2-8:1, preferably 4:1. Between the first and third legs carrying the confluent flows, the ratio between the cross-sectional areas thereof is reduced to 0.7-1.2:1, preferably 1:1, at a distance from the juncture which is 1-3 times the inner diameter of the third leg. The confluent flow is led through a spiral hose, producing a powerful extraction due to the counter-current turbulence.

    摘要翻译: 一种用于流动提取的方法和装置,其中溶解在第一溶剂中的物质被萃取到不溶于第一溶剂的第二溶剂中。 这两种溶剂通过T型管中的两条腿接合在一起,并且混合物通过第三腿离开,腿的横截面面积的尺寸被设计成产生具有第二和第一溶剂的交替塞的分段流。 第一和第二溶剂的管腿的横截面积之间的比率为2-8:1,优选为4:1。 在承载汇合流动的第一和第三腿之间,其横截面积之间的比率在距离接合点的1-3倍的距离处减小到0.7-1.2:1,优选为1:1, 第三条腿 汇合流动通过螺旋软管引导,由于逆流湍流产生强大的提取。