公开(公告)号：US06706233B2

公开(公告)日：2004-03-16

申请号：US10029747

申请日：2001-12-18

申请人： Carlos R. Araya ,  John H. Brennan ,  Gary G. Squier ,  Kathleen A. Wexell ,  Elizabeth M. Vileno

发明人： Carlos R. Araya ,  John H. Brennan ,  Gary G. Squier ,  Kathleen A. Wexell ,  Elizabeth M. Vileno

IPC分类号： C04B3332

CPC分类号： C04B38/0006 ,  C04B35/195 ,  C04B35/48 ,  C04B35/565 ,  C04B35/64 ,  H05B6/80 ,  H05B2206/046 ,  C04B40/0218

摘要： The method for heating a plurality of ceramic bodies, includes: a) providing ceramic-forming raw materials and blending the raw materials with an effective amount of vehicle and forming aids to form a plastic mixture therefrom and thereafter forming the plastic raw material mixture into a plurality of green bodies; b) placing each one of the plurality of green bodies in proximity to an adjacent one of the plurality of green bodies such that upon heating with electromagnetic waves each green body is subject to no more than about 1.5 times the power density at the boundary than in the bulk thereof; and c) drying the green bodies utilizing energy in the form of electromagnetic waves. When the ceramic is a honeycomb cellular cordierite body, the method further includes heating the green bodies up to a maximum temperature of between about 1360° C. and about 1435° C. to produce fired bodies that are predominantly cordierite, wherein the firing includes utilizing a combination of microwave and convective or radiative heating during periods where the green bodies are subject to an endothermic reaction or phase transition. The method for the firing of a honeycomb cellular cordierite bodies further includes placing each one of the plurality of green bodies in proximity to an adjacent one of the plurality of green bodies within a firing chamber such that upon heating with electromagnetic waves each green body is subject to no more than about 5 times the power density at the boundary than in the bulk thereof.

摘要翻译： 用于加热多个陶瓷体的方法包括：a）提供陶瓷成形原料，并将原料与有效量的车辆和成型助剂混合以形成塑料混合物，然后将塑料原料混合物形成为 多个生坯体; b）将所述多个生坯体中的每一个放置在所述多个生坯体中相邻的一个生坯体附近，使得在用电磁波加热时，每个生坯体的功率密度不超过约1.5倍 在边界比在其大部分; 和c）利用电磁波形式的能量干燥生物体。当陶瓷是蜂窝状堇青石体时，该方法还包括将生物体加热至约1360℃至约1435℃的最高温度 以生产主要为堇青石的烧制体，其中焙烧包括在生坯体经受吸热反应或相变的时段期间利用微波和对流或辐射加热的组合。蜂窝状蜂窝状堇青石烧制方法 身体还包括将多个生坯体中的每一个放置在烧制室内的多个生坯体中相邻的一个之上，使得当用电磁波加热时，每个生坯体的功率密度不超过约5倍 在边界比在其大部分。

公开(公告)号：US06555036B1

公开(公告)日：2003-04-29

申请号：US10047492

申请日：2001-10-26

申请人： John H. Brennan ,  Tudor C. Gheorghiu ,  Mark A. Spetseris

发明人： John H. Brennan ,  Tudor C. Gheorghiu ,  Mark A. Spetseris

IPC分类号： C04B3332

CPC分类号： F27D21/00 ,  F27D19/00

摘要： A process for automatically controlling combustible vapors during debinding and firing of ceramic products which includes establishing a maximum percentage of lower flammability limit (LFL) setpoint no greater than 50%; measuring continuously the percentage of LFL in the kiln atmosphere; and, maintaining the measured percentage of LFL to be less than or equal to the maximum percentage of LFL setpoint by an action selected from the group consisting of increasing gas volume delivered to the kiln, decreasing O2 concentration in the kiln, decreasing heating rate in the firing cycle, and combinations thereof.

摘要翻译： 一种在脱蜡和焙烧陶瓷产品时自动控制可燃蒸汽的方法，其中包括确定最低百分比的最低燃烧极限（LFL）设定值不大于50％; 在窑气中连续测量LFL的百分比; 并且通过选自以下的动作将LFL的测量百分比维持在小于或等于LFL设定值的最大百分比，该动作选自增加输送到窑的气体体积，降低窑中的O2浓度，降低窑炉中的加热速率 烧制循环及其组合。

公开(公告)号：US07198673B2

公开(公告)日：2007-04-03

申请号：US11059980

申请日：2005-02-16

申请人： John H. Brennan ,  Michael W. Price ,  Juergen Tinz ,  Liming Wang

发明人： John H. Brennan ,  Michael W. Price ,  Juergen Tinz ,  Liming Wang

IPC分类号： C30B11/00

CPC分类号： C30B33/00 ,  C30B29/12 ,  Y10T117/10 ,  Y10T117/1016 ,  Y10T117/1024

摘要： A method of making below 250-nm UV light transmitting optical fluoride lithography crystals includes applying heat along a shortest path of conduction of a selected optical fluoride crystal, heating the optical fluoride crystal to an annealing temperature, holding the temperature of the optical fluoride crystal at the annealing temperature, and gradually cooling the optical fluoride crystal to provide a low-birefringence optical fluoride crystal for transmitting below 250-nm UV light.

摘要翻译： 制造低于250nm的UV光透射​​光学氟化物光刻晶体的方法包括沿着所选择的氟化物晶体的最短导通路径施加热量，将氟化物晶体加热到退火温度，将氟化物晶体的温度保持在 退火温度，并逐渐冷却光氟化物晶体，以提供低于250nm紫外光的低双折射氟化物晶体。

公开(公告)号：US06997987B2

公开(公告)日：2006-02-14

申请号：US10611505

申请日：2003-06-30

申请人： John H. Brennan ,  Michael W. Price ,  Juergen Tinz ,  Liming Wang

发明人： John H. Brennan ,  Michael W. Price ,  Juergen Tinz ,  Liming Wang

IPC分类号： C30B11/04

CPC分类号： C30B33/00 ,  C30B29/12 ,  Y10T117/10 ,  Y10T117/1016 ,  Y10T117/1024

摘要： A method of making below 250-nm UV light transmitting optical fluoride lithography crystals includes applying heat along a shortest path of conduction of a selected optical fluoride crystal, heating the optical fluoride crystal to an annealing temperature, holding the temperature of the optical fluoride crystal at the annealing temperature, and gradually cooling the optical fluoride crystal to provide a low-birefringence optical fluoride crystal for transmitting below 250-nm UV light.

摘要翻译： 制造低于250nm的UV光透射​​光学氟化物光刻晶体的方法包括沿着所选择的氟化物晶体的最短导通路径施加热量，将氟化物晶体加热到退火温度，将氟化物晶体的温度保持在 退火温度，并逐渐冷却光氟化物晶体，以提供低于250nm紫外光的低双折射氟化物晶体。

公开(公告)号：US06537481B2

公开(公告)日：2003-03-25

申请号：US09727184

申请日：2000-11-30

申请人： John H. Brennan

发明人： John H. Brennan

IPC分类号： H05B664

CPC分类号： F27B17/0016 ,  C04B35/64 ,  F27D19/00 ,  F27D2099/0028

摘要： A ceramic article is fired using a combination of microwave energy and conventional heating energy according to a microwave power-time heating schedule comprising a series of separate firing segments at predetermined microwave power settings, the core and surface temperatures of the article being monitored during firing to determine the core-surface temperature differential, that differential being controlled and limited to prevent cracking of the ceramic article by adjusting the level of applied conventional heat energy during firing.

摘要翻译： 根据微波功率时间加热方案，使用微波能量和常规加热能量的组合来烧制陶瓷制品，所述微波功率时间加热方案包括在预定的微波功率设置下的一系列单独的点火段，所述制品在烧制过程中被监测的核心和表面温度 确定芯表面温差，该差异被控制和限制，以防止在烧制期间调节常规热能的水平来陶瓷制品的开裂。

公开(公告)号：US07238319B2

公开(公告)日：2007-07-03

申请号：US10606509

申请日：2003-06-26

申请人： John H. Brennan ,  Gregory P. Dillon ,  Tudor C. Gheorghiu ,  Michael J. Vayansky

发明人： John H. Brennan ,  Gregory P. Dillon ,  Tudor C. Gheorghiu ,  Michael J. Vayansky

IPC分类号： C04B33/32 ,  C04B28/00

CPC分类号： C04B38/00 ,  C04B35/195 ,  C04B35/63 ,  C04B35/632 ,  C04B35/6365 ,  C04B35/638 ,  C04B2111/00129 ,  C04B2111/0081 ,  C04B2235/3217 ,  C04B2235/3445 ,  C04B2235/349 ,  C04B2235/449 ,  C04B38/067

摘要： A method for fabricating a green ceramic article containing organic compounds. The method involves first heating the green ceramic article to sequentially remove the organic compounds such that the organic compound with the lowest weight loss onset temperature is substantially removed prior to the next higher weight loss onset temperature organic compound. The organic compounds include but are not limited to at least an oil or oil-based compound having a flash point or an ignition temperature, higher than the weight loss onset temperature. For this system the temperature during heating is maintained below the flash point of the oil or oil-based compound until substantial removal thereof from the green ceramic structural body. After the organic compounds are substantially removed, the green ceramic article is further fired to a temperature and for a time to obtain a final fired body.

摘要翻译： 一种制造含有机化合物的生陶瓷制品的方法。 该方法包括首先加热生陶瓷制品以顺序地除去有机化合物，使得在下一个更高的重量损失开始温度的有机化合物之前基本上除去具有最低重量损失起始温度的有机化合物。 有机化合物包括但不限于至少具有高于重量损失开始温度的具有闪点或着火温度的油或油基化合物。 对于该系统，加热期间的温度保持低于油或油基化合物的闪点，直到其从绿色陶瓷结构体基本上除去。 在有机化合物基本上除去之后，将生坯陶瓷制品进一步烧制至一段温度以获得最终的烧制体。

公开(公告)号：US06344635B2

公开(公告)日：2002-02-05

申请号：US09817393

申请日：2001-03-26

申请人： John H. Brennan

发明人： John H. Brennan

IPC分类号： H05B664

CPC分类号： H05B6/80 ,  C04B35/64 ,  F27B17/00 ,  F27D19/00 ,  F27D2099/0028 ,  H05B2206/046

摘要： A method of firing ceramic materials involving placing the ceramic material in a microwave heating apparatus having a microwave cavity and subjecting the ceramic material to combination of microwave radiation and conventional heat energy according to predetermined time-temperature profile. The time-temperature profile, ranging from room temperature the sintering soak temperature, comprises a series of target heating rate temperature setpoints and a series of corresponding core and surface temperature setpoints with each of the core and surface temperature setpoints being offset from the target heating rate setpoints a predetermined offset temperature. In a preferred embodiment, the method involves continuously measuring the ceramic body core temperature, TC, and the surface temperature TS and independently controlling the microwave power and the conventional heat in response to the core temperature value and the surface temperature value, respectively. Preferably, controlling of the microwave power involves adjusting the microwave power in response to a difference between core temperature setpoint and a biased core measured temperature, and controlling of the conventional heat involves adjusting the conventional heat in response to the difference between the surface temperature setpoint and a biased surface temperature.

摘要翻译： 一种烧制陶瓷材料的方法，包括将陶瓷材料放置在具有微波腔的微波加热装置中，并根据预定的时间 - 温度曲线使陶瓷材料与微波辐射和常规热能组合。 时间 - 温度曲线，从室温，烧结保温温度，包括一系列目标加热速率温度设定点和一系列对应的核心和表面温度设定点，其中每个核心和表面温度设定点偏离目标加热速率 给定一个预定的偏移温度。 在一个优选实施例中，该方法包括分别连续地测量陶瓷体芯温度TC和表面温度TS，并分别响应于芯温度值和表面温度值独立地控制微波功率和常规热量。 优选地，微波功率的控制包括响应于芯温度设定点和偏置芯测量温度之间的差异来调节微波功率，并且常规热的控制包括响应于表面温度设定点和 偏压表面温度。

公开(公告)号：US06344634B2

公开(公告)日：2002-02-05

申请号：US09727021

申请日：2000-11-30

申请人： John H. Brennan

发明人： John H. Brennan

IPC分类号： H05B664

CPC分类号： H05B6/80 ,  C04B35/64 ,  F27B17/00 ,  F27D19/00 ,  F27D2099/0028 ,  H05B2206/046

摘要： A method of firing ceramic materials involving placing the ceramic material in a microwave heating apparatus having a microwave cavity and subjecting the ceramic material to combination of microwave radiation and conventional heat energy according to predetermined time-temperature profile. The time-temperature profile, ranging from room temperature the sintering soak temperature, comprises a series of target heating rate temperature setpoints and a series of corresponding core and surface temperature setpoints with each of the core and surface temperature setpoints being offset from the target heating rate setpoints a predetermined offset temperature. The method involves continuously measuring the ceramic body core temperature, TC, and the surface temperature TS. Controlling of the microwave power involves adjusting the microwave power in response to a difference between core temperature setpoint and a biased core measured temperature. Controlling of the conventional heat involves adjusting the conventional heat in response to the difference between the surface temperature setpoint and a biased surface temperature. The method involves continuing to deliver and control the microwave power and the conventional heat until the ceramic body has reached is sintering soak temperature.

摘要翻译： 一种烧制陶瓷材料的方法，包括将陶瓷材料放置在具有微波腔的微波加热装置中，并根据预定的时间 - 温度曲线使陶瓷材料与微波辐射和常规热能组合。 时间 - 温度曲线，从室温，烧结保温温度，包括一系列目标加热速率温度设定点和一系列对应的核心和表面温度设定点，其中每个核心和表面温度设定点偏离目标加热速率 给定一个预定的偏移温度。 该方法包括连续测量陶瓷体芯温度TC和表面温度TS。 微波功率的控制涉及根据核心温度设定值与偏置核心测量温度之间的差异调整微波功率。 常规热的控制包括响应于表面温度设定点和偏置表面温度之间的差异来调节常规热量。 该方法包括继续传送和控制微波功率和常规热量，直到陶瓷体达到烧结保温温度。