METHOD FOR PREPARING HIGH-SILICA Y ZEOLITE

    公开(公告)号:US20250033984A1

    公开(公告)日:2025-01-30

    申请号:US18359247

    申请日:2023-07-26

    Abstract: A method is disclosed for making a high-silica zeolite having an FAU framework structure. The method includes: (1) preparing a reaction mixture comprising: (a) a source of silica; (b) a source of alumina; (c) a source of an alkali or alkaline earth metal cation; (d) an organic structure directing agent containing at least one cation selected from a 1,2-dimethyl-3-(3-methylbenzyl) imidazolium cation, a 1-ethyl-3-methylimidazolium cation, and a 1-butyl-3-methylimidazolium cation; (e) a source of hydroxide ions; and (f) water; (2) heating the reaction mixture under crystallization conditions including a temperature of from 80° C. to 200° C. for a time sufficient to form crystals of the high-silica zeolite; and (3) recovering at least a portion of the high-silica zeolite from step (2).

    METHOD FOR PREPARING ALUMINOSILICATE SSZ-82

    公开(公告)号:US20240383762A1

    公开(公告)日:2024-11-21

    申请号:US18319462

    申请日:2023-05-17

    Abstract: A method is disclosed making aluminosilicate SSZ-82. The method includes (1) preparing a reaction mixture comprising: an amorphous alumina source comprising predominantly aluminum hydroxide; an amorphous silica source comprising predominantly colloidal silica; a source of an alkali metal cation; an organic structure directing agent comprising a 1,6-bis(N-cyclohexylpyrrolidinium)hexane dication; hydroxide ions; seed crystals, wherein the seed crystals comprise a crystalline molecular sieve having an SSZ-82 framework; and water; (2) heating the reaction mixture under crystallization conditions including a temperature of from 100° C. to 200° C. for a time sufficient to form crystals of the aluminosilicate zeolite; and (3) recovering at least a portion of the aluminosilicate zeolite from step (2).

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