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公开(公告)号：US4335002A
公开(公告)日：1982-06-15
申请号：US169678
申请日：1980-07-17
申请人： Cynthia J. Mussinan , Braja D. Mookherjee , Manfred H. Vock , Frederick L. Schmitt , Edward J. Granda , Joaquin F. Vinals , Jacob Kiwala
发明人： Cynthia J. Mussinan , Braja D. Mookherjee , Manfred H. Vock , Frederick L. Schmitt , Edward J. Granda , Joaquin F. Vinals , Jacob Kiwala
CPC分类号： C11B9/0015 , A23L27/2024 , A24B15/32
摘要： Described are cis-3-hexenyl derivatives having the generic structure: ##STR1## wherein R is one of the moieties: ##STR2## which are useful in foodstuffs, flavorings, fragrances, perfumed articles (e.g. anionic, cationic or nonionic detergents, dryer-added fabric softener articles and cosmetic powders) and smoking tobacco flavorings; processes for producing such cis-3-hexenyl derivatives and products produced according to such processes which include chemical compounds in addition to said cis-3-hexenyl derivatives.
摘要翻译： 描述了具有以下通用结构的顺式-3-己烯基衍生物：其中R是部分之一：可用于食品，调味品，香料，加香制品（例如阴离子，阳离子或非离子型洗涤剂 ，干燥剂添加织物柔软剂制品和化妆品粉末）和吸烟烟草调味剂; 制备这种顺式-3-己烯基衍生物的方法和根据这些方法生产的产物，除了所述顺式-3-己烯基衍生物外，还包括化学化合物。
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2.发明授权Use of a mixture of isomers of caryophyllene alcohol or dihydro caryophyllene alcohol in augmenting or enhancing the aroma or taste of smoking tobacco, smoking tobacco articles and/or smoking tobacco flavors 失效使用石竹烯醇或二氢叶绿素醇的异构体混合物来增强或增强吸烟烟草，烟草制品和/或烟草香精的香气或味道
公开(公告)号：US4280515A
公开(公告)日：1981-07-28
申请号：US106154
申请日：1979-12-21
申请人： Cynthia J. Mussinan , Braja D. Mookherjee , Manfred H. Vock , Joaquin F. Vinals , Jacob Kiwala , Frederick L. Schmitt
发明人： Cynthia J. Mussinan , Braja D. Mookherjee , Manfred H. Vock , Joaquin F. Vinals , Jacob Kiwala , Frederick L. Schmitt
CPC分类号： C11B9/0049 , A24B15/345 , C07C29/10 , C07C2102/32
摘要： Described is the use of a mixture of isomers of caryophyllene alcohol or dihydro caryophyllene alcohol including 10,10-dimethyl-2,6-dimethylene bicyclo(7.2.0)undecan-5-ol in augmenting or enhancing the aroma or taste of smoking tobacco, smoking tobacco articles and smoking tobacco flavors. The mixture of isomers of caryophyllene alcohol and dihydro caryophyllene alcohol are prepared by isomerizing caryophyllene oxide or dihydro caryophyllene oxide using an aluminum isopropylate catalyst and a toluene solvent at temperatures in the range of from about 100.degree. C. up to about 150.degree. C.
摘要翻译： 描述的是使用含有10,10-二甲基-2,6-二亚甲基双环（7.2.0）十一烷-5-醇的石竹烯醇或二氢叶绿素醇的异构体混合物来增强或增强吸烟烟草的香味或味道 ，吸烟烟草制品和吸烟烟草香精。 石竹烯醇和二氢叶绿素醇的异构体的混合物是通过使用异丙醇铝催化剂和甲苯溶剂在约100℃至约150℃的温度范围内异构化氧化石脑烯或二氢氧化烯烃来制备的。
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3.发明授权Use of mixture containing caryophyllene alcohols in augmenting or enhancing the aroma of a solid or liquid anionic, cationic or nonionic detergent 失效使用含有石竹烯醇的混合物可增强或增强固体或液体阴离子，阳离子或非离子型洗涤剂的香气
公开(公告)号：US4247409A
公开(公告)日：1981-01-27
申请号：US105886
申请日：1979-12-21
申请人： Cynthia J. Mussinan , Braja D. Mookherjee , Manfred H. Vock , Joaquin F. Vinals , Jacob Kiwala , Frederick L. Schmitt
发明人： Cynthia J. Mussinan , Braja D. Mookherjee , Manfred H. Vock , Joaquin F. Vinals , Jacob Kiwala , Frederick L. Schmitt
摘要： Described is a process for augmenting or enhancing the aroma of a solid or liquid anionic, cationic or nonionic detergent comprising the step of intimately admixing with a solid or liquid anionic, cationic or nonionic detergent base, a product prepared by a process comprising the steps of (i) intimately admixing aluminum isopropylate, toluene and a caryophyllene derivative selected from the group consisting of caryophyllene oxide and dihydro caryophyllene oxide to form a mixture; (ii) heating the resulting mixture at a temperature of from 100.degree. C. up to 150.degree. C. for a period of time from about one up to about five hours; and (iii) the rearranged caryophyllene oxide or dihydro caryophyllene oxide, a mixture of alcohols, from the reaction mass; the concentration of aluminum isopropylate catalyst in the reaction mass varying from about 0.025 molar up to about 0.75 molar; and the concentration of caryophyllene oxide or dihydro caryophyllene oxide in the reaction mass varying from about 0.25 molar up to about 1.00 molar.
摘要翻译： 描述了用于增强或增强固体或液体阴离子，阳离子或非离子洗涤剂的香味的方法，其包括与固体或液体阴离子，阳离子或非离子洗涤剂基质紧密混合的步骤，通过包括以下步骤的方法制备的产物： （i）密切混合异丙醇铝，甲苯和选自由石竹烯氧化物和二氢烯烃氧化物组成的组的石竹烯衍生物以形成混合物; （ii）将所得混合物在100℃至150℃的温度下加热约1至5小时的时间; 和（iii）来自反应物质的重排的石竹烯氧化物或二氢石竹烯氧化物，醇的混合物; 反应物质中异丙醇铝催化剂的浓度从约0.025摩尔至约0.75摩尔变化; 并且反应物质中的石竹烯氧化物或二氢叶绿素氧化物的浓度从约0.25摩尔至约1.00摩尔变化。
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4.发明授权Derivatives of cis-3-hexenol and process for producing compositions of matter containing cis-3-hexenal and products produced thereby and organoleptic uses thereof 失效顺式-3-己烯醇的衍生物及其制备含有顺式-3-己烯醛的物质组合物的方法及由此产生的产物及其感官用途
公开(公告)号：US4312766A
公开(公告)日：1982-01-26
申请号：US169813
申请日：1980-07-17
申请人： Cynthia J. Mussinan , Braja D. Mookherjee , Manfred H. Vock , Frederick L. Schmitt , Edward J. Granda , Joaquin F. Vinals , Jacob Kiwala
发明人： Cynthia J. Mussinan , Braja D. Mookherjee , Manfred H. Vock , Frederick L. Schmitt , Edward J. Granda , Joaquin F. Vinals , Jacob Kiwala
CPC分类号： A24B15/32 , A23L27/2024
摘要： Described are cis-3-hexenyl derivatives having the generic structure: ##STR1## wherein R is one of the moieties: ##STR2## which are useful in foodstuffs, flavorings, fragrances, perfumed articles (e.g. anionic, cationic or nonionic detergents, dryer-added fabric softener articles and cosmetic powders) and smoking tobacco flavorings; processes for producing such cis-3-hexenyl derivatives and products produced according to such processes which include chemical compounds in addition to said cis-3-hexenyl derivatives.
摘要翻译： 描述了具有以下通用结构的顺式-3-己烯基衍生物：其中R是可用于食品，调味品，香料，加香制品（例如阴离子，阳离子或非离子洗涤剂，干燥剂 - 添加织物柔软剂制品和化妆粉）和吸烟烟草调味剂; 制备这种顺式-3-己烯基衍生物的方法和根据这些方法生产的产物，除了所述顺式-3-己烯基衍生物外，还包括化学化合物。
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5.发明授权Uses of hexenol derivatives in augementing or enhancing the aroma or taste of smoking tobacco compositions and smoking tobacco articles 失效使用己烯醇衍生物处理或增强吸烟烟草组合物和烟草制品的香气或味道
公开(公告)号：US4319586A
公开(公告)日：1982-03-16
申请号：US169901
申请日：1980-07-17
申请人： Cynthia J. Mussinan , Braja D. Mookherjee , Manfred H. Vock , Frederick L. Schmitt , Edward J. Granda , Joaquin F. Vinals , Jacob Kiwala
发明人： Cynthia J. Mussinan , Braja D. Mookherjee , Manfred H. Vock , Frederick L. Schmitt , Edward J. Granda , Joaquin F. Vinals , Jacob Kiwala
CPC分类号： A24B15/32 , A23L27/2024
摘要： Described are processes for augmenting or enhancing the aroma or taste of a smoking tobacco comprising the step of intimately admixing with smoking tobacco an aroma or taste augmenting or enhancing quantity of at least one substance selected from the group consisting of:A. A composition of matter consisting essentially of cis-3-hexenal, cis-3-hexenyl-cis-3-hexenoate, trans-2-hexenal, and cis-3-hexenol;B. A composition of matter consisting essentially of cis-3-hexenal, cis-3-hexenyl-cis-3-hexenoate, cis-3-hexenyl formate and trans-2-hexenal;C. A composition of matter consisting essentially of cis-3-hexenal, cis-3-hexenyl-cis-3-hexenoate, cis-3-hexenol, cis-3-hexenyl formate and trans-2-hexenal; andD. Cis-3-hexenyl methyl ether.Also described are smoking tobacco compositions produced according to the above process. Also described are smoking tobacco articles comprising a cylindrically shaped body of smoking tobacco; in intimate contact with said cylindrically shaped body along its length, a wrapper; and in intimate contact with one end of said cylindrically shaped body, a filter; and in intimate contact with either said filter, said wrapper or said cylindrically shaped body at least one substance selected from the group consisting of:A. A composition of matter consisting essentially of cis-3-hexenal, cis-3-hexenyl-cis-3-hexenoate, trans-2-hexenal, and cis-3-hexenol;B. A composition of matter consisting essentially of cis-3-hexenal, cis-3-hexenyl-cis-3-hexenoate, cis-3-hexenyl formate and trans-2-hexenal;C. A composition of matter consisting essentially of cis-3-hexenal, cis-3-hexenyl-cis-3-hexenoate, cis-3-hexenol, cis-3-hexenyl formate and trans-2-hexenal; andD. Cis-3-hexenyl methyl ether.
摘要翻译： 描述了用于增强或增强烟草的香气或味道的方法，其包括与吸烟烟草充分混合的香味或味道增强或增加量的选自以下的物质的步骤：A.物质组合物 基本上由顺式-3-己烯醛，顺式-3-己烯基 - 顺式-3-己烯酸酯，反式-2-己烯醛和顺式-3-己烯醇组成; B.基本上由顺式-3-己烯醛，顺式-3-己烯基 - 顺式-3-己烯酸酯，顺式-3-己烯甲酸酯和反式-2-己烯醛组成的物质组合物; C.基本上由顺式-3-己烯醛，顺式-3-己烯基 - 顺式-3-己烯酸酯，顺式-3-己烯醇，顺式-3-己烯甲酸酯和反式-2-己烯醛组成的物质组合物。 和D.Cis-3-己烯基甲基醚。 还描述了根据上述方法制备的烟草烟草组合物。 还描述了包括吸烟烟草的圆柱形体的烟草制品; 沿其长度与所述圆柱形体紧密接触，包裹物; 并且与所述圆柱形体的一端紧密接触，过滤器; 并且与所述过滤器，所述包装物或所述圆柱形主体紧密接触至少一种选自以下的物质：A.主要由顺式-3-己烯醛，顺式-3-己烯基 - 顺式 - 3-己烯酸酯，反式-2-己烯醛和顺式-3-己烯醇; B.基本上由顺式-3-己烯醛，顺式-3-己烯基 - 顺式-3-己烯酸酯，顺式-3-己烯甲酸酯和反式-2-己烯醛组成的物质组合物; C.基本上由顺式-3-己烯醛，顺式-3-己烯基 - 顺式-3-己烯酸酯，顺式-3-己烯醇，顺式-3-己烯甲酸酯和反式-2-己烯醛组成的物质组合物。 和D.Cis-3-己烯基甲基醚。
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6.发明授权Process for augmenting or enhancing the aroma of detergent using derivatives of cis-3-hexenol 失效使用顺式-3-己烯醇衍生物增强或增强洗涤剂香气的方法
公开(公告)号：US4267066A
公开(公告)日：1981-05-12
申请号：US169812
申请日：1980-07-17
申请人： Cynthia J. Mussinan , Braja D. Mookherjee , Manfred H. Vock , Frederick L. Schmitt , Edward J. Granda , Joaquin F. Vinals , Jacob Kiwala
发明人： Cynthia J. Mussinan , Braja D. Mookherjee , Manfred H. Vock , Frederick L. Schmitt , Edward J. Granda , Joaquin F. Vinals , Jacob Kiwala
CPC分类号： A24B15/32 , A23L27/2024 , A23L27/2026 , C11D3/50 , C11D9/442
摘要： Described is a process for augmenting or enhancing the aroma of solid or liquid anionic, cationic or nonionic detergent comprising the step of intimately admixing with a solid or liquid anionic, cationic or nonionic detergent base an aroma augmenting or enhancing quantity of at least one substrate selected from the group consisting of:A. A composition of matter consisting essentially of cis-3-hexenal, cis-3-hexenyl-cis-3-hexenoate, trans-2-hexenal, and cis-3-hexenol;B. A composition of matter consisting essentially of cis-3-hexenal, cis-3-hexenyl-cis-3-hexenoate, cis-3-hexenyl formate and trans-2-hexenal;C. A composition of matter consisting essentially of cis-3-hexenal, cis-3-hexenyl-cis-3-hexenoate, cis-3-hexenol, cis-3-hexenyl formate and trans-2-hexenal; andD. Cis-3-hexenyl methyl ether.
摘要翻译： 描述了一种用于增强或增强固体或液体阴离子，阳离子或非离子洗涤剂的香气的方法，其包括与固体或液体阴离子，阳离子或非离子洗涤剂基质充分混合或增强量的至少一种选择的底物的步骤 由以下组成：A.基本上由顺式-3-己烯醛，顺式-3-己烯基 - 顺式-3-己烯酸酯，反式-2-己烯醛和顺式-3-己烯醇组成的物质组合物; B.基本上由顺式-3-己烯醛，顺式-3-己烯基 - 顺式-3-己烯酸酯，顺式-3-己烯甲酸酯和反式-2-己烯醛组成的物质组合物; C.基本上由顺式-3-己烯醛，顺式-3-己烯基 - 顺式-3-己烯酸酯，顺式-3-己烯醇，顺式-3-己烯甲酸酯和反式-2-己烯醛组成的物质组合物。 和D.Cis-3-己烯基甲基醚。
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公开(公告)号：US4229599A
公开(公告)日：1980-10-21
申请号：US947186
申请日：1978-09-29
申请人： Cynthia J. Mussinan , Braja D. Mookherjee , Manfred H. Vock , Joaquin F. Vinals , Jacob Kiwala , Frederick L. Schmitt
发明人： Cynthia J. Mussinan , Braja D. Mookherjee , Manfred H. Vock , Joaquin F. Vinals , Jacob Kiwala , Frederick L. Schmitt
CPC分类号： A24B15/345 , C07C29/56 , C11B9/0049 , C07B2200/07 , C07C2102/32
摘要： A process for preparing a mixture of isomers of caryophyllene alcohol and dihydrocaryophyllene alcohol including 10,10-dimethyl-2,6-dimethylene bicyclo[7.2.0]undecan-5-ol by isomerizing caryophyllene oxide or dihydrocaryophyllene oxide using an aluminum isopropylate catalyst in a toluene solvent at temperatures in the range of from about 100.degree. C. up to about 150.degree. C. is described.
摘要翻译： 使用异丙醇铝催化剂异构化氧化石脑烯或二氢氧杂环戊烯来制备石竹烯醇和二氢石竹烯醇的异构体混合物的方法，该方法包括10,10-二甲基-2,6-二亚甲基双环[7.2.0]十一烷-5-醇 描述了在约100℃至约150℃的温度范围内的甲苯溶剂。
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8.发明授权Derivatives of cis-3-hexenol and process for producing compositions of matter containing cis-3-hexenal and products produced thereby and organoleptic uses thereof 失效顺式-3-己烯醇的衍生物及其制备含有顺式-3-己烯醛的物质组合物的方法及由此产生的产物及其感官用途
公开(公告)号：US4280933A
公开(公告)日：1981-07-28
申请号：US169902
申请日：1980-07-17
申请人： Cynthia J. Mussinan , Braja D. Mookherjee , Manfred H. Vock , Frederick L. Schmitt , Edward J. Granda , Joaquin F. Vinals , Jacob Kiwala
发明人： Cynthia J. Mussinan , Braja D. Mookherjee , Manfred H. Vock , Frederick L. Schmitt , Edward J. Granda , Joaquin F. Vinals , Jacob Kiwala
CPC分类号： A24B15/32 , A23L27/2024
摘要： Described are cis-3-hexenyl derivatives having the generic structure: ##STR1## wherein R is one of the moieties: ##STR2## which are useful in foodstuffs, flavorings, fragrances, perfumed articles (e.g. anionic, cationic or nonionic detergents, dryer-added fabric softener articles and cosmetic powders) and smoking tobacco flavorings; processes for producing such cis-3-hexenyl derivatives and products produced according to such processes which include chemical compounds in addition to said cis-3-hexenyl derivatives.
摘要翻译： 描述了具有以下通用结构的顺式-3-己烯基衍生物：其中R是可用于食品，调味品，香料，加香制品（例如阴离子，阳离子或非离子洗涤剂，干燥剂 - 添加织物柔软剂制品和化妆粉）和吸烟烟草调味剂; 制备这种顺式-3-己烯基衍生物的方法和根据这些方法生产的产物，除了所述顺式-3-己烯基衍生物外，还包括化学化合物。
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公开(公告)号：US4267076A
公开(公告)日：1981-05-12
申请号：US105924
申请日：1979-12-21
申请人： Braja D. Mookherjee , Cynthia J. Mussinan , Manfred H. Vock , Joaquin F. Vinals , Jacob Kiwala , Frederick L. Schmitt
发明人： Braja D. Mookherjee , Cynthia J. Mussinan , Manfred H. Vock , Joaquin F. Vinals , Jacob Kiwala , Frederick L. Schmitt
CPC分类号： C07C29/10 , A24B15/345 , C11B9/0049 , C07C2102/32
摘要： A process for preparing a mixture of isomers of caryophyllene alcohol and dihydrocaryophyllene alcohol including 10,10-dimethyl-2,6-dimethylene bicyclo[7.2.0]undecan-5-ol by isomerizing caryophyllene oxide or dihydrocaryophyllene oxide using an aluminum isopropylate catalyst in a toluene solvent at temperatures in the range of from about 100.degree. C. up to about 150.degree. C. is described.
摘要翻译： 使用异丙醇铝催化剂异构化氧化石脑烯或二氢氧杂环戊烯来制备石竹烯醇和二氢石竹烯醇的异构体混合物的方法，该方法包括10,10-二甲基-2,6-二亚甲基双环[7.2.0]十一烷-5-醇 描述了在约100℃至约150℃的温度范围内的甲苯溶剂。
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10.发明授权Use of mixture containing caryophyllene alcohols for augmenting or enhancing the aroma or taste of foodstuffs 失效使用含有石竹烯醇的混合物来增强或增强食品的香气或味道
公开(公告)号：US4250201A
公开(公告)日：1981-02-10
申请号：US106155
申请日：1979-12-21
申请人： Cynthia J. Mussinan , Braja D. Mookherjee , Manfred H. Vock , Joaquin F. Vinals , Jacob Kiwala , Frederick L. Schmitt
发明人： Cynthia J. Mussinan , Braja D. Mookherjee , Manfred H. Vock , Joaquin F. Vinals , Jacob Kiwala , Frederick L. Schmitt
CPC分类号： C07C29/56 , A24B15/345 , A24D3/14 , C07C29/00 , C07C35/23 , C11B9/0003 , C11B9/0049 , C11D3/50 , C07C2102/32
摘要： Described is the use for augmenting or enhancing the flavor of foodstuffs of a product containing isomers of caryophyllene alcohol and other compounds produced by isomerizing caryophyllene oxide using an aluminum isopropylate catalyst in a toluene solvent at temperatures in the range of from about 100.degree. C. up to about 150.degree. C. and then fractionally distilling the resulting reaction product and isolating certain fractions of the reaction product.
摘要翻译： 描述了用于增加或增强含有石竹烯醇异构体的产品的食品的味道的用途，以及使用异丙醇铝催化剂在甲苯溶剂中异构化石脑烯氧化物制备的其它化合物的食品的风味，其用量范围为约100℃ 至约150℃，然后分馏蒸馏所得反应产物并分离反应产物的某些馏分。
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