ALCOHOL PRODUCTION METHOD AND COMPOSITION
    4.
    发明公开

    公开(公告)号:US20240109826A1

    公开(公告)日:2024-04-04

    申请号:US18505611

    申请日:2023-11-09

    IPC分类号: C07C29/10

    CPC分类号: C07C29/10

    摘要: A composition containing: a compound (2); a metal compound; and at least one selected from a compound (3) and a compound (4), the compound (3) being contained in an amount of 10000 ppm or less relative to the compound (2), the compound (4) being contained in an amount of 10000 ppm or less relative to the compound (2), the compound (2) being represented by the following formula (2):




    the compound (3) being represented by the following formula (3):




    and the compound (4) being represented by the following formula (4):




    wherein the various substituents of compounds (2), (3) and (4) are as defined herein.

    METHOD FOR PURIFYING ACRYLIC ACID ESTER COMPOUND

    公开(公告)号:US20230192590A1

    公开(公告)日:2023-06-22

    申请号:US18110060

    申请日:2023-02-15

    IPC分类号: C07C67/54

    CPC分类号: C07C67/54

    摘要: The present disclosure addresses the problem of providing a method for purifying an acrylic acid ester compound. This problem can be solved by a method for purifying a compound represented by formula (1)




    (wherein R1 and R2 are the same as or different and each represent an alkyl group, a fluoroalkyl group, an aryl group optionally having one or more substituent groups, a halogen atom, or a hydrogen atom, R3 is an alkyl group, a fluoroalkyl group, or an aryl group optionally having one or more substituent groups, and X is a fluoroalkyl group or a halogen atom), the method including step A of distilling composition A containing (a) the compound represented by formula (1), (b) an alcohol, and (c) a salt so as to obtain a concentrate containing the compound represented by formula (1).

    FLUOROLACTONE AND METHOD FOR PRODUCING SAME

    公开(公告)号:US20220064139A1

    公开(公告)日:2022-03-03

    申请号:US17521155

    申请日:2021-11-08

    IPC分类号: C07D319/12

    摘要: The present disclosure provides, for example, a method that can produce a fluorolactone compound from hexafluoropropylene oxide or the like in a single step. The present disclosure relates to a method for producing a compound represented by formula (1): wherein two R1 are the same and each is a fluorine atom or a fluoroalkyl group, the method comprising step A of reacting a compound represented by formula (2): wherein R1 is as defined above, with a compound represented by formula (3): wherein R31, R32, and R33 are the same or different and each is a hydrogen atom or an alkyl group, or two of them are optionally linked to each other to form a ring optionally having one or more substituents, and a compound represented by formula (4-1) or the like: wherein R41, R42, R43, and R44 are the same or different and each is a hydrogen atom ox an alkyl group, or two of them are optionally linked to each other to form a ring optionally having one or more substituents.

    METHOD FOR PRODUCING FLUOROVINYL ETHER COMPOUND

    公开(公告)号:US20210284593A1

    公开(公告)日:2021-09-16

    申请号:US17255689

    申请日:2019-06-26

    IPC分类号: C07C43/176 B01J31/16

    摘要: An object of the present invention is to provide, for example, a novel method for synthesizing a fluorovinyl ether compound from a fluorine-containing vinyl compound. This problem is solved by a method for producing a compound represented by formula (1): wherein Ra1 is a hydrogen atom, a halogeno group, an alkyl group, a fluoroalkyl group, or an aromatic group optionally having one or more substituents, Rf is a fluoro group or a perfluoroalkyl group, Ra2 is a hydrogen atom, a halogeno group, an alkyl group, a fluoroalkyl group, or an aromatic group optionally having one or more substituents, or (i) Ra1 and Ra2, (ii) Ra1 and Rf, or (iii) Rf and Ra2 may be linked to each other, Rb1 is RS, Rb2 is a hydrogen atom or RS, Rb3 is a hydrogen atom or RS, or two or three of Rb1, Rb2, and Rb3, taken together with the adjacent carbon atom, may form a ring optionally having one or more substituents, and RS, in each occurrence, is the same or different and represents a hydrocarbon group optionally having one or more substituents, the method comprising step A of reacting a compound represented by formula (2): wherein Rx is a leaving group, and other symbols are as defined above, with a compound represented by formula (3): wherein the symbols in the formula are as defined above, in the presence of a transition metal catalyst.

    METHOD FOR PRODUCING CARBONYL COMPOUND

    公开(公告)号:US20210002199A1

    公开(公告)日:2021-01-07

    申请号:US16978997

    申请日:2019-03-07

    摘要: A method for producing a carbonyl compound represented by formula (1): wherein R1 is hydrogen or an organic group; R2 is hydrogen or an organic group; and R3 is hydrogen or an organic group; or two or three of R1, R2, and R3 may be linked to form a ring that may have at least one substituent, the method comprising step A of oxidizing an olefin compound represented by formula (2): wherein symbols are as defined above, by an oxidizing agent in the presence of (a) a non-alcohol organic solvent, (b) water, (c) a metal catalyst, and (d) an additive represented by the formula: MXn, wherein M is an element belonging to any one of Group 1, Group 2, Group 13, Group 14, and Group 15 in the periodic table, or NR4, wherein R is hydrogen or a C1-10 organic group; X is halogen; and n is a number of 1 to 5.