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    TRANSPARENT CONDUCTIVE NANO-COMPOSITES
    1.
    发明申请
    TRANSPARENT CONDUCTIVE NANO-COMPOSITES 有权
    透明导电纳米复合材料

    公开(公告)号：US20080191606A1

    公开(公告)日：2008-08-14

    申请号：US11965651

    申请日：2007-12-27

    申请人： David Bruce Geohegan ,  Ilya N. Ivanov ,  Alexander A. Puretzky ,  Stephen Jesse ,  Bin Hu

    发明人： David Bruce Geohegan ,  Ilya N. Ivanov ,  Alexander A. Puretzky ,  Stephen Jesse ,  Bin Hu

    IPC分类号： H01J1/63 ,  C23C16/26

    CPC分类号： H01L51/0048 ,  B82Y30/00 ,  B82Y40/00 ,  C01B32/16 ,  C01B32/17 ,  C01B32/174 ,  C01B2202/02 ,  C01B2202/08 ,  C01B2202/34 ,  C01B2202/36 ,  C08J5/005 ,  H01B1/24 ,  Y10S428/917

    摘要： The present invention, in one embodiment, provides a method of forming an organic electric device that includes providing a plurality of carbon nanostructures; and dispersing the plurality of carbon nanostructures in a polymeric matrix to provide a polymeric composite, wherein when the plurality of carbon nanostructures are present at a first concentration an interface of the plurality of carbon nanostructures and the polymeric matrix is characterized by charge transport when an external energy is applied, and when the plurality of carbon nanostructures are present at a second concentration the interface of the plurality of carbon nanostructures and the polymeric matrix are characterized by exciton dissociation when an external energy is applied, wherein the first concentration is less than the second concentration.

    摘要翻译： 本发明在一个实施方案中提供了一种形成有机电子器件的方法，该方法包括提供多个碳纳米结构; 以及将所述多个碳纳米结构分散在聚合物基质中以提供聚合物复合物，其中当所述多个碳纳米结构以第一浓度存在时，所述多个碳纳米结构和所述聚合物基体的界面的特征在于当外部 施加能量，并且当多个碳纳米结构以第二浓度存在时，当施加外部能量时，多个碳纳米结构和聚合物基体的界面的特征在于激子解离，其中第一浓度小于第二浓度 浓度。

    Transparent conductive nano-composites
    4.
    发明授权
    Transparent conductive nano-composites 有权
    透明导电纳米复合材料

    公开(公告)号：US07923922B2

    公开(公告)日：2011-04-12

    申请号：US11965651

    申请日：2007-12-27

    申请人： David Bruce Geohegan ,  Ilia N. Ivanov ,  Alexander A. Puretzky ,  Stephen Jesse ,  Bin Hu ,  Matthew Garrett ,  Bin Zhao

    发明人： David Bruce Geohegan ,  Ilia N. Ivanov ,  Alexander A. Puretzky ,  Stephen Jesse ,  Bin Hu ,  Matthew Garrett ,  Bin Zhao

    IPC分类号： H05B33/00

    CPC分类号： H01L51/0048 ,  B82Y30/00 ,  B82Y40/00 ,  C01B32/16 ,  C01B32/17 ,  C01B32/174 ,  C01B2202/02 ,  C01B2202/08 ,  C01B2202/34 ,  C01B2202/36 ,  C08J5/005 ,  H01B1/24 ,  Y10S428/917

    摘要： The present invention, in one embodiment, provides a method of forming an organic electric device that includes providing a plurality of carbon nanostructures; and dispersing the plurality of carbon nanostructures in a polymeric matrix to provide a polymeric composite, wherein when the plurality of carbon nanostructures are present at a first concentration an interface of the plurality of carbon nanostructures and the polymeric matrix is characterized by charge transport when an external energy is applied, and when the plurality of carbon nanostructures are present at a second concentration the interface of the plurality of carbon nanostructures and the polymeric matrix are characterized by exciton dissociation when an external energy is applied, wherein the first concentration is less than the second concentration.

    摘要翻译： 本发明在一个实施方案中提供了一种形成有机电子器件的方法，该方法包括提供多个碳纳米结构; 以及将所述多个碳纳米结构分散在聚合物基质中以提供聚合物复合物，其中当所述多个碳纳米结构以第一浓度存在时，所述多个碳纳米结构和所述聚合物基体的界面的特征在于当外部 施加能量，并且当多个碳纳米结构以第二浓度存在时，当施加外部能量时，多个碳纳米结构和聚合物基体的界面的特征在于激子解离，其中第一浓度小于第二浓度 浓度。

    Spatially resolved quantitative mapping of thermomechanical properties and phase transition temperatures using scanning probe microscopy
    5.
    发明授权
    Spatially resolved quantitative mapping of thermomechanical properties and phase transition temperatures using scanning probe microscopy 有权
    使用扫描探针显微镜空间解析热力学性质和相变温度的定量映射

    公开(公告)号：US08484759B2

    公开(公告)日：2013-07-09

    申请号：US12857894

    申请日：2010-08-17

    申请人： Stephen Jesse ,  Sergei V. Kalinin ,  Maxim P. Nikiforov

    发明人： Stephen Jesse ,  Sergei V. Kalinin ,  Maxim P. Nikiforov

    IPC分类号： G01Q60/58

    CPC分类号： G01Q60/58

    摘要： An approach for the thermomechanical characterization of phase transitions in polymeric materials (polyethyleneterephthalate) by band excitation acoustic force microscopy is developed. This methodology allows the independent measurement of resonance frequency, Q factor, and oscillation amplitude of a tip-surface contact area as a function of tip temperature, from which the thermal evolution of tip-surface spring constant and mechanical dissipation can be extracted. A heating protocol maintained a constant tip-surface contact area and constant contact force, thereby allowing for reproducible measurements and quantitative extraction of material properties including temperature dependence of indentation-based elastic and loss moduli.

    摘要翻译： 开发了通过频带激发声力显微镜对聚合物材料（聚对苯二甲酸乙二醇酯）中的相变的热机械表征的方法。 该方法允许独立测量作为尖端温度的函数的尖端表面接触面积的谐振频率，Q因子和振荡振幅，从而可以提取尖端表面弹簧常数和机械耗散的热演变。 加热方案保持了不变的顶表面接触面积和恒定的接触力，从而允许重复测量和定量提取材料性能，包括基于压痕的弹性和损耗模量的温度依赖性。

    SPATIALLY RESOLVED QUANTITATIVE MAPPING OF THERMOMECHANICAL PROPERTIES AND PHASE TRANSITION TEMPERATURES USING SCANNING PROBE MICROSCOPY
    6.
    发明申请
    SPATIALLY RESOLVED QUANTITATIVE MAPPING OF THERMOMECHANICAL PROPERTIES AND PHASE TRANSITION TEMPERATURES USING SCANNING PROBE MICROSCOPY 有权
    使用扫描探针显微镜空间分辨温度特性和相变过渡温度的定量映射

    公开(公告)号：US20110041223A1

    公开(公告)日：2011-02-17

    申请号：US12857894

    申请日：2010-08-17

    申请人： Stephen Jesse ,  Sergei V. Kalinin ,  Maxim P. Nikiforov

    发明人： Stephen Jesse ,  Sergei V. Kalinin ,  Maxim P. Nikiforov

    IPC分类号： G01Q20/00

    CPC分类号： G01Q60/58

    摘要： An approach for the thermomechanical characterization of phase transitions in polymeric materials (polyethyleneterephthalate) by band excitation acoustic force microscopy is developed. This methodology allows the independent measurement of resonance frequency, Q factor, and oscillation amplitude of a tip-surface contact area as a function of tip temperature, from which the thermal evolution of tip-surface spring constant and mechanical dissipation can be extracted. A heating protocol maintained a constant tip-surface contact area and constant contact force, thereby allowing for reproducible measurements and quantitative extraction of material properties including temperature dependence of indentation-based elastic and loss moduli.

    摘要翻译： 开发了通过频带激发声力显微镜对聚合物材料（聚对苯二甲酸乙二醇酯）中的相变的热机械表征的方法。 该方法允许独立测量作为尖端温度的函数的尖端表面接触面积的谐振频率，Q因子和振荡振幅，从而可以提取尖端表面弹簧常数和机械耗散的热演变。 加热方案保持了不变的顶表面接触面积和恒定的接触力，从而允许重复测量和定量提取材料性能，包括基于压痕的弹性和损耗模量的温度依赖性。

    SEM technique for imaging and measuring electronic transport in nanocomposites based on electric field induced contrast
    7.
    发明申请
    SEM technique for imaging and measuring electronic transport in nanocomposites based on electric field induced contrast 失效
    基于电场诱导对比的纳米复合材料成像和测量电子传输的SEM技术

    公开(公告)号：US20070164218A1

    公开(公告)日：2007-07-19

    申请号：US11331840

    申请日：2006-01-13

    申请人： Stephen Jesse ,  David Geohegan ,  Michael Guillorn

    发明人： Stephen Jesse ,  David Geohegan ,  Michael Guillorn

    IPC分类号： G01N23/225 ,  H01J37/256 ,  G21K7/00

    CPC分类号： G01N23/2251 ,  G01N23/2204 ,  H01J37/20 ,  H01J2237/2008 ,  H01J2237/24564 ,  H01J2237/2594

    摘要： Methods and apparatus are described for SEM imaging and measuring electronic transport in nanocomposites based on electric field induced contrast. A method includes mounting a sample onto a sample holder, the sample including a sample material; wire bonding leads from the sample holder onto the sample; placing the sample holder in a vacuum chamber of a scanning electron microscope; connecting leads from the sample holder to a power source located outside the vacuum chamber; controlling secondary electron emission from the sample by applying a predetermined voltage to the sample through the leads; and generating an image of the secondary electron emission from the sample. An apparatus includes a sample holder for a scanning electron microscope having an electrical interconnect and leads on top of the sample holder electrically connected to the electrical interconnect; a power source and a controller connected to the electrical interconnect for applying voltage to the sample holder to control the secondary electron emission from a sample mounted on the sample holder; and a computer coupled to a secondary electron detector to generate images of the secondary electron emission from the sample.

    摘要翻译： 描述了基于电场诱导对比的SEM成像和测量纳米复合材料中的电子传输的方法和装置。 一种方法包括将样品安装到样品架上，样品包括样品材料; 将样品架上的导线接合到样品上; 将样品架置于扫描电子显微镜的真空室中; 将引线从样品架连接到位于真空室外部的电源; 通过经由引线向样品施加预定的电压来控制来自样品的二次电子发射; 以及从样品产生二次电子发射的图像。 一种装置包括用于具有电互连的扫描电子显微镜的样品保持器，并且在与电互连电连接的样品保持器的顶部上的引线; 电源和连接到电互连的控制器，用于向样品架施加电压以控制来自安装在样品架上的样品的二次电子发射; 以及耦合到二次电子检测器以产生来自样品的二次电子发射的图像的计算机。

    Real space mapping of oxygen vacancy diffusion and electrochemical transformations by hysteretic current reversal curve measurements
    8.
    发明授权
    Real space mapping of oxygen vacancy diffusion and electrochemical transformations by hysteretic current reversal curve measurements 有权
    通过滞后电流反转曲线测量的氧空位扩散和电化学转换的实际空间映射

    公开(公告)号：US08752211B2

    公开(公告)日：2014-06-10

    申请号：US13566327

    申请日：2012-08-03

    申请人： Sergei V. Kalinin ,  Nina Balke ,  Albina Y. Borisevich ,  Stephen Jesse ,  Petro Maksymovych ,  Yunseok Kim ,  Evgheni Strelcov

    发明人： Sergei V. Kalinin ,  Nina Balke ,  Albina Y. Borisevich ,  Stephen Jesse ,  Petro Maksymovych ,  Yunseok Kim ,  Evgheni Strelcov

    IPC分类号： G01Q60/44

    CPC分类号： G01Q60/30

    摘要： An excitation voltage biases an ionic conducting material sample over a nanoscale grid. The bias sweeps a modulated voltage with increasing maximal amplitudes. A current response is measured at grid locations. Current response reversal curves are mapped over maximal amplitudes of the bias cycles. Reversal curves are averaged over the grid for each bias cycle and mapped over maximal bias amplitudes for each bias cycle. Average reversal curve areas are mapped over maximal amplitudes of the bias cycles. Thresholds are determined for onset and ending of electrochemical activity. A predetermined number of bias sweeps may vary in frequency where each sweep has a constant number of cycles and reversal response curves may indicate ionic diffusion kinetics.

    摘要翻译： 激发电压在纳米尺度网格上偏置离子导电材料样品。 偏置以最大幅度增加扫描调制电压。 当前的响应是在网格位置测量的。 电流响应反转曲线映射到偏置周期的最大幅度。 对于每个偏置周期，反转曲线在电网上进行平均，并映射到每个偏置周期的最大偏移幅度。 平均反转曲线区域映射到偏置周期的最大幅度。 确定电化学活性的起始和结束的阈值。 预定数量的偏置扫描可以在频率上变化，其中每个扫描具有恒定的循环次数，反转响应曲线可以指示离子扩散动力学。

    Real space mapping of ionic diffusion and electrochemical activity in energy storage and conversion materials
    9.
    发明授权
    Real space mapping of ionic diffusion and electrochemical activity in energy storage and conversion materials 有权
    能量储存和转换材料中离子扩散和电化学活性的实际空间映射

    公开(公告)号：US08719961B2

    公开(公告)日：2014-05-06

    申请号：US13291480

    申请日：2011-11-08

    申请人： Sergei V. Kalinin ,  Nina Balke ,  Amit Kumar ,  Nancy J. Dudney ,  Stephen Jesse

    发明人： Sergei V. Kalinin ,  Nina Balke ,  Amit Kumar ,  Nancy J. Dudney ,  Stephen Jesse

    IPC分类号： G01Q60/60

    CPC分类号： G01Q60/60 ,  G01Q60/02 ,  G01Q60/30

    摘要： A method and system for probing mobile ion diffusivity and electrochemical reactivity on a nanometer length scale of a free electrochemically active surface includes a control module that biases the surface of the material. An electrical excitation signal is applied to the material and induces the movement of mobile ions. An SPM probe in contact with the surface of the material detects the displacement of mobile ions at the surface of the material. A detector measures an electromechanical strain response at the surface of the material based on the movement and reactions of the mobile ions. The use of an SPM tip to detect local deformations allows highly reproducible measurements in an ambient environment without visible changes in surface structure. The measurements illustrate effective spatial resolution comparable with defect spacing and well below characteristic grain sizes of the material.

    摘要翻译： 用于探测自由电化学活性表面的纳米尺度上的移动离子扩散率和电化学反应性的方法和系统包括偏压材料表面的控制模块。 电激励信号被施加到材料并引起移动离子的移动。 与材料表面接触的SPM探针检测到材料表面上的移动离子的位移。 检测器基于移动离子的运动和反应来测量材料表面处的机电应变响应。 使用SPM尖端来检测局部变形允许在周围环境中进行高度可重复的测量，而没有表面结构的可见变化。 测量结果说明了有效的空间分辨率与缺陷间距相当，远远低于材料的特征晶粒尺寸。

    Spatially resolved thermal desorption/ionization coupled with mass spectrometry
    10.
    发明授权
    Spatially resolved thermal desorption/ionization coupled with mass spectrometry 有权
    空间分辨热解析/电离耦合质谱

    公开(公告)号：US08384020B2

    公开(公告)日：2013-02-26

    申请号：US12890225

    申请日：2010-09-24

    申请人： Stephen Jesse ,  Gary J. Van Berkel ,  Olga S. Ovchinnikova

    发明人： Stephen Jesse ,  Gary J. Van Berkel ,  Olga S. Ovchinnikova

    IPC分类号： H01J49/00

    CPC分类号： H01J49/0004 ,  G01Q30/02 ,  G01Q60/38 ,  H01J49/0413 ,  H01J49/049

    摘要： A system and method for sub-micron analysis of a chemical composition of a specimen are described. The method includes providing a specimen for evaluation and a thermal desorption probe, thermally desorbing an analyte from a target site of said specimen using the thermally active tip to form a gaseous analyte, ionizing the gaseous analyte to form an ionized analyte, and analyzing a chemical composition of the ionized analyte. The thermally desorbing step can include heating said thermally active tip to above 200° C., and positioning the target site and the thermally active tip such that the heating step forms the gaseous analyte. The thermal desorption probe can include a thermally active tip extending from a cantilever body and an apex of the thermally active tip can have a radius of 250 nm or less.

    摘要翻译： 描述了用于样品的化学组成的亚微米分析的系统和方法。 该方法包括提供用于评估的样本和热解吸探针，使用热活性尖端从所述样品的靶位点热解析分析物以形成气态分析物，电离气态分析物以形成离子化分析物，并分析化学物质 电离分析物的组成。 热解吸步骤可以包括将所述热活性尖端加热到高于200℃，并且定位靶部位和热活性尖端，使得加热步骤形成气态分析物。 热解吸探针可以包括从悬臂体延伸的热活性尖端，并且热活性尖端的顶点可以具有250nm或更小的半径。