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1.发明授权
公开(公告)号：US5211877A
公开(公告)日：1993-05-18
申请号：US401261
申请日：1989-08-31
申请人： Dirk Andrejewski , Magdi Gohary , Hans-Joachim Luckas , Rainer Winkler , Franz-Heinrich Kreuzer
发明人： Dirk Andrejewski , Magdi Gohary , Hans-Joachim Luckas , Rainer Winkler , Franz-Heinrich Kreuzer
IPC分类号： B01J20/283 , B01J20/281 , C07C69/88 , C07C69/90 , C07C69/92 , C07F7/18 , C07J9/00 , C08G77/06 , C08G77/38 , C08L83/04 , C08L83/07 , C09D7/00 , C09K19/40 , G01N30/88 , G02F1/13
CPC分类号： C09K19/408 , C08G77/38 , C09D7/007
摘要： The present invention relates to liquid-crystalline compounds and to a process for preparing liquid-crystalline polyorganosiloxanes having methacryloxy and/or acryloxy groups by the reaction of organosiloxanes having hydrogen atoms bonded directly to silicon atoms and/or organosilanes which can be condensed to form organosiloxanes having hydrogen atoms bonded directly to silicon atoms, with alkenes and/or alkynes having mesogenic groups, which comprises reacting in a first step the organosiloxanes with an alkene and/or alkyne having at least one non-enolic hydroxyl group protected by a protective group, and in a second step the protective group is removed and the hydroxyl group which is now free is esterified with (meth)acrylic acid, esters, anhydrides and/or halides thereof and thereafter optionally condensing the organosilanes to organosiloxanes.
摘要翻译： 本发明涉及液晶化合物以及具有甲基丙烯酰氧基和/或丙烯酰氧基的液晶聚有机硅氧烷的方法，该有机硅氧烷具有直接键合在硅原子上的氢原子的有机硅氧烷和/或可以缩合形成有机硅氧烷的有机硅烷 具有与硅原子直接键合的氢原子和具有介晶基团的烯烃和/或炔烃，其包括在第一步骤中使有机硅氧烷与具有被保护基保护的至少一个非烯醇羟基的烯烃和/或炔烃反应， 并且在第二步中，除去保护基，并且现在游离的羟基用（甲基）丙烯酸，酯，酸酐和/或卤化物酯化，然后任选地将有机硅烷缩合成有机硅氧烷。
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2.发明授权Process for the preparation of liquid-crystalline polyorganosiloxanes containing (meth)acryloxy groups 失效制备含有（甲基）丙烯酰氧基的液晶聚有机硅氧烷的方法
公开(公告)号：US5641850A
公开(公告)日：1997-06-24
申请号：US555957
申请日：1995-11-09
IPC分类号： G03F7/075 , C07F7/08 , C07F7/21 , C08G77/12 , C08G77/22 , C08G77/38 , C09D183/07 , C09K19/40 , G02B5/20 , G02B5/30 , G02F1/13 , C08G77/04
CPC分类号： C07F7/0879 , C07F7/0852 , C07F7/21 , C08G77/38 , C09K19/408
摘要： Liquid-crystalline polyorganosiloxanes containing methacryloxy and/or acryloxy groups are prepared by reaction of polyorganosiloxanes containing hydrogen atoms bonded directly to silicon atoms with alkenes and/or alkynes containing mesogenic groups in two steps, wherein the polyorganosiloxanes mentioned are reacted in a first step with alkene and/or alkyne containing mesogenic groups and are reacted in a second step with an alkene and/or alkyne containing at least one methacryloxy and/or acryloxy group and mesogenic groups.
摘要翻译： 含有甲基丙烯酰氧基和/或丙烯酰氧基的液晶聚有机硅氧烷是通过将含有直接键合硅原子的氢原子的聚有机硅氧烷与含有介晶基团的烯烃和/或含有介晶基团的炔两步反应来制备的，其中所述的聚有机硅氧烷在第一步中与烯烃反应 和/或含炔的介晶基团，并且在第二步中与含有至少一个甲基丙烯酰氧基和/或丙烯酰氧基和介晶基团的烯烃和/或炔反应。
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3.发明授权Method for the production of organosiloxanes modified by a phosphonic acid ester 有权用膦酸酯改性的有机硅氧烷的制造方法公开(公告)号：US07491784B2
公开(公告)日：2009-02-17
申请号：US10595701
申请日：2004-10-28
IPC分类号： C08G77/22
CPC分类号： C08G77/30 , C08G77/395
摘要： Phosphone ester modified organosilicon compounds are prepared by reacting phosphonic ester-functionalized alkoxysilane with a silanol-functional organosilicon compound. The product is produced in high yield and purity.
摘要翻译： 通过膦酸酯官能化的烷氧基硅烷与硅烷醇官能的有机硅化合物反应来制备膦酯改性的有机硅化合物。 该产品以高产率和纯度生产。
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4.发明申请Method for the production of organosiloxanes modified by a phosponic acid ester 有权生产由磷酸酯改性的有机硅氧烷的方法公开(公告)号：US20070167597A1
公开(公告)日：2007-07-19
申请号：US10595701
申请日：2004-10-28
CPC分类号： C08G77/30 , C08G77/395
摘要： Phosphone ester modified organosilicon compounds are prepared by reacting phosphonic ester-functionalized alkoxysilane with a silanol-functional organosilicon compound. The product is produced in high yield and purity.
摘要翻译： 通过膦酸酯官能化的烷氧基硅烷与硅烷醇官能的有机硅化合物反应来制备膦酯改性的有机硅化合物。 该产品以高产率和纯度生产。
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公开(公告)号：US20070049718A1
公开(公告)日：2007-03-01
申请号：US10595035
申请日：2004-07-01
IPC分类号： C08G77/22
CPC分类号： C08G77/30 , C07F9/4012
摘要： Phosphonate-functional organosilicon compounds in which the phosphonate ester group is linked to silicon by an Si—C—P linkage are prepared rapidly and in high yield by the hydrolysis and polycondensation of phosphonate-functional alkoxysilanes with water.
摘要翻译： 膦酸酯基团通过Si-C-P键与硅连接的膦酸酯官能的有机硅化合物通过膦酸酯官能的烷氧基硅烷与水的水解和缩聚快速且高产率地制备。
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