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    Preparation of carbonyl halides of more than 7 carbon atoms
    1.
    发明授权
    Preparation of carbonyl halides of more than 7 carbon atoms 失效
    制备大于7个碳原子的羰基卤化物

    公开(公告)号：US4900479A

    公开(公告)日：1990-02-13

    申请号：US205160

    申请日：1988-06-10

    申请人： Enrique Freudenberg ,  Peter Wittmer ,  Andreas Hohmann ,  Hans-Heinrich Bechtolsheimer

    发明人： Enrique Freudenberg ,  Peter Wittmer ,  Andreas Hohmann ,  Hans-Heinrich Bechtolsheimer

    IPC分类号： C07C51/00 ,  C07C51/60 ,  C07C51/64 ,  C07C53/42 ,  C07C67/00

    CPC分类号： C07C51/60

    摘要： Carbonyl halides of the general formula I ##STR1## where R is an organic radical of more than 7 carbon atoms and X is chlorine or bromine, are prepared by reacting carboxylic acids of the general formula II ##STR2## where R has the abovementioned meaning, with phosphorus chlorides or bromides by treating these reaction mixtures with carboxamide/hydrochloride or hydrobromide mixtures which are not homogeneously miscible with the carbonyl halides I and then separating off the carboxamide hydrochloride or hydrobromide phase.

    摘要翻译： 其中R是大于7个碳原子的有机基团，X是氯或溴的通式I（I）的羰基酰卤是通过使通式II的羧酸（II） R具有上述含义，用氯化磷或溴化物，通过用羧酰胺/盐酸盐或氢溴酸盐混合物处理这些反应混合物，其与羰基卤化物I不能均匀混溶，然后分离羧酰胺盐酸盐或氢溴酸盐相。

    Stabilized aqueous alkyldiketene emulsions
    2.
    发明授权
    Stabilized aqueous alkyldiketene emulsions 失效
    稳定的水性氨基酸乳化剂

    公开(公告)号：US5154763A

    公开(公告)日：1992-10-13

    申请号：US639093

    申请日：1991-01-09

    申请人： Peter Ksoll ,  Erwin Hahn ,  Peter Wittmer ,  Andreas Hohmann ,  Arnold De Clercq ,  Ulrich Riebeling

    发明人： Peter Ksoll ,  Erwin Hahn ,  Peter Wittmer ,  Andreas Hohmann ,  Arnold De Clercq ,  Ulrich Riebeling

    IPC分类号： B01F17/00 ,  B01J13/00 ,  C07C45/90 ,  C07C49/88 ,  C07D305/12 ,  C07D315/00 ,  D21H17/06 ,  D21H17/07 ,  D21H17/17 ,  D21H17/46 ,  D21H21/14

    CPC分类号： C07D315/00 ,  C07C45/90 ,  D21H17/06 ,  D21H17/07 ,  D21H17/17

    摘要： Stabilized aqueous C.sub.14 -C.sub.22 -alkyldiketene emulsions containing, as essential components:(a) from 10 to 60% w/w of at least one C.sub.14 -C.sub.22 -alkyldiketene,(b) from 1 to 10% w/w of at least one protective colloid and(c) from 0.1 to 20% w/w of at least one ester of formula I ##STR1## in which R.sup.1 and R.sup.2 each denote C.sub.14 -C.sub.22 -alkyl, R.sup.1 differing in this case from R.sup.2 by at least 4 carbon atoms in the alkyl chain, and/or the same or different C.sub.14 -C.sub.22 -alkenyl groups, or at least one ester of the formula R.sup.3 --O--CO--O--R.sup.4 (II), in which R.sup.3 and R.sup.4 are alkyl or alkenyl radicals of from 2 to 22 carbon atoms or at least one urethane of formula III ##STR2## in which R.sup.5, R.sup.6 and R.sup.7 are the same or different alkyl or alkenyl radicals of from 2 to 22 carbon atoms and one of the substituents R.sup.5, R.sup.6 and R.sup.7 contains at least 12 carbon atoms,and showing a ratio of emulsified components (a):(c) from 200:1 to 1:1 and the use of compounds of formulae I to III as stabilizers for the preparation of alkyldiketene emulsions containing at least 10% w/w and preferably from 16 to 40% w/w of emulsified alkyldiketene.

    摘要翻译： 含有作为必要组分的稳定的C14-C22-烷基二乙烯基水乳液：（a）10至60％w / w的至少一种C14-C22-烷基二乙烯基，（b）1至10％w / w的至少一种 保护胶体和（c）0.1至20％w / w的至少一种式I（I）的酯，其中R 1和R 2各自表示C 14 -C 22 - 烷基，R 1在这种情况下不同于R 2， 烷基链中至少4个碳原子，和/或相同或不同的C 14 -C 22 - 烯基或至少一个式R 3 -O-CO-O-R 4（II）的酯，其中R 3和R 4是 具有2至22个碳原子的烷基或烯基或至少一个式III的氨基甲酸酯其中R 5，R 6和R 7是相同或不同的具有2至22个碳原子的烷基或烯基，一个 的取代基R 5，R 6和R 7含有至少12个碳原子，并且显示出乳化组分（a）：（c）的比例为200:1至1:1，并且使用式I至III的化合物作为稳定剂 烷基染料的制备 含有至少10％w / w，优选16至40％w / w的乳化的烷基染料的乳液。

    Preparation of carbonyl chlorides
    3.
    发明授权
    Preparation of carbonyl chlorides 失效
    碳氟化合物的制备

    公开(公告)号：US5245063A

    公开(公告)日：1993-09-14

    申请号：US757388

    申请日：1991-09-10

    申请人： Peter Ksoll ,  Wolfgang Reuther ,  Andreas Hohmann ,  Peter Wittmer

    发明人： Peter Ksoll ,  Wolfgang Reuther ,  Andreas Hohmann ,  Peter Wittmer

    IPC分类号： C07C51/60

    CPC分类号： C07C51/60

    摘要： A process for preparing carbonyl chlorides of the formula I ##STR1## where R is C.sub.1 -C.sub.30 -alkyl, C.sub.2 -C.sub.30 -alkenyl or C.sub.2 -C.sub.30 -alkynyl, from essentially equimolar amounts of a carboxylic acid of the formula II ##STR2## where R has the abovementioned meanings, and phosgene COCl.sub.2 (III), in the presence of a catalytic adduct of phosgene and N,N-disubstituted formamide or the hydrochlorides thereof, of the formula IV where R.sup.1 and R.sup.2 are each, independently of one another, C.sub.1 -C.sub.3 -alkyl or together are a C.sub.4 -C.sub.5 -alkylene chain which may be interrupted by oxygen or by nitrogen which carries C.sub.1 -C.sub.3 -alkyl or CHO, and n is 0, 1 or 2, wherein the reaction is carried out with a stationary phase of the catalytic adduct, is described.

    摘要翻译： 制备式I的羰基氯的方法（I）其中R是C 1 -C 30 - 烷基，C 2 -C 30 - 烯基或C 2 -C 30 - 炔基，基本上等摩尔量的式II的羧酸 （IV）的光气和N，N-二取代的甲酰胺或其盐酸盐的催化加合物存在下，其中R具有上述含义的光学（II）和光气COCl 2（III） 其中R 1和R 2各自独立地为C 1 -C 3 - 烷基或一起为可被氧或携带C 1 -C 3烷基或CHO的氮中断的C 4 -C 5 - 亚烷基链，并且n为0 ，1或2，其中所述反应用催化加合物的固定相进行。