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    Preparation of tetrachloro-3-iminoisoindolin-1-one
    2.
    发明授权
    Preparation of tetrachloro-3-iminoisoindolin-1-one 失效
    制备四氯-3-亚氨基异吲哚啉-1-酮

    公开(公告)号：US4751314A

    公开(公告)日：1988-06-14

    申请号：US907586

    申请日：1986-09-15

    申请人： Erwin Hahn ,  Heinrich Kowarsch

    发明人： Erwin Hahn ,  Heinrich Kowarsch

    IPC分类号： C07D209/50

    CPC分类号： C07D209/50

    摘要： Tetrachloro-3-iminosisoindolin-1-one (I) or its alkali metal salt (Ia) is prepared by reacting tetrachloro-ortho-phthalodinitrile with lithium hydroxide, sodium hydroxide and/or potassium hydroxide in substantially anhydrous tert-butanol and, if desired, liberating (I) from (Ia) by means of a dilute acid.

    摘要翻译： 四氯-3-亚氨基二吲哚啉-1-酮（I）或其碱金属盐（Ia）通过四氯邻苯二甲腈与氢氧化锂，氢氧化钠和/或氢氧化钾在基本无水的叔丁醇中反应制备，如果需要 ，通过稀酸从（Ia）释放（I）。

    Dyes having a diazo component and an isoquinoline coupling component
    3.
    发明授权
    Dyes having a diazo component and an isoquinoline coupling component 失效
    具有重氮组分和异喹啉偶联组分的染料

    公开(公告)号：US4491544A

    公开(公告)日：1985-01-01

    申请号：US409144

    申请日：1982-08-18

    申请人： Volker Radtke ,  Heinrich Kowarsch ,  Erwin Hahn ,  Peter Hauser

    发明人： Volker Radtke ,  Heinrich Kowarsch ,  Erwin Hahn ,  Peter Hauser

    IPC分类号： C08K5/00 ,  C08K5/22 ,  C09B29/42 ,  C09B29/44 ,  C09B33/12 ,  C09D11/00 ,  C09D11/02 ,  C09B1/20 ,  C09B29/00 ,  C09B29/033

    CPC分类号： C09B33/12 ,  C09B29/3617

    摘要： A compound having the formula (I): ##STR1## wherein D is a radical of a heterocyclic or aromatic component selected from the group of aniline, anthraquinone, phthalimide or aminobenzene radicals, wherein the radical is unsubstituted or is substituted by fluorine, chlorine, bromine, nitro, C.sub.1 -C.sub.4 -alkyl, C.sub.1 -C.sub.4 -alkoxy, trifluoromethyl, cyano, C.sub.1 -C.sub.4 -alkylsulfonyl, carboxylic acid ester groups, carbamyl, sulfamyl, 1,3,4- or 1,2,4-oxadiazolyl or acylamino groups; X is CO-- or --SO.sub.2 --; and R is an aliphatic, aromatic or heterocyclic radical selected from the group of C.sub.1 -C.sub.20 alkyl which is unsubstituted or is substituted by chlorine, bromine, cyano or dialkylamino groups; or phenyl or methyl groups unsubstituted or substituted by fluorine, bromine, methyl, ethyl, methoxy, ethoxy, cyano, carbamyl, sulfamyl or acylamino groups; or amino group; or a radical of the formula: ##STR2## wherein ring a is unsubstituted or is substituted by nitro, fluro, bromine or methoxy groups; and ring b is unsubstituted or is substituted by chlorine, bromine or nitro groups.The majority of the compounds of the formula (I) have yellow hues and are used as pigments in printing inks and finishes, and as disperse dyes for synthetic fibers.

    摘要翻译： 具有式（I）的化合物：其中D是选自苯胺，蒽醌，邻苯二甲酰亚胺或氨基苯基的杂环或芳族成分的基团，其中该基团是未取代的或被氟取代的 ，氯，溴，硝基，C 1 -C 4 - 烷基，C 1 -C 4 - 烷氧基，三氟甲基，氰基，C 1 -C 4 - 烷基磺酰基，羧酸酯基，氨基甲酰基，氨磺酰基，1,3,4-或1,2,4 - 恶二唑基或酰氨基; X是CO-或-SO 2 - ; 并且R是选自未被取代或被氯，溴，氰基或二烷基氨基取代的C 1 -C 20烷基的脂族，芳族或杂环基; 或未被取代或被氟，溴，甲基，乙基，甲氧基，乙氧基，氰基，氨基甲酰基，氨基磺酰基或酰氨基取代的苯基或甲基; 或氨基; 或下式的基团：其中环a未被取代或被硝基，氟，溴或甲氧基取代; 环b是未取代的或被氯，溴或硝基取代。 大多数式（I）化合物具有黄色色调，并用作印刷油墨和表面处理剂中的颜料，并用作合成纤维的分散染料。

    Preparation of J-acid urea
    4.
    发明授权
    Preparation of J-acid urea 失效
    制备J-酸尿素

    公开(公告)号：US5144064A

    公开(公告)日：1992-09-01

    申请号：US764359

    申请日：1991-09-23

    申请人： Erwin Hahn ,  Udo Mayer ,  Friedrich-Wilhelm Raulfs ,  Ulrike Schloesser

    发明人： Erwin Hahn ,  Udo Mayer ,  Friedrich-Wilhelm Raulfs ,  Ulrike Schloesser

    IPC分类号： C07C303/22 ,  C07C309/51

    CPC分类号： C07C303/22

    摘要： J-Acid urea of the formula ##STR1## is prepared by reacting 7-amino-4-hydroxynaphthalene-2-sulfonic acid (J-acid) with urea at from 100.degree. to 140.degree. C. under a pressure ranging from atmospheric pressure to 10 bar in an inert solvent to a partial extent, precipitating unconverted J-acid in an acidic medium and separating it off, and, if desired, isolating J-acid urea from the resulting neutralized solution by salting out.

    摘要翻译： 通过使7-氨基-4-羟基萘-2-磺酸（J-酸）与尿素在100-140℃下在大气压至大约压力的压力下反应制备式“IMAGE”的γ-酸尿素 10巴在惰性溶剂中的一部分程度，在酸性介质中沉淀未转化的J-酸，并将其分离出来，如果需要，通过盐析从得到的中和溶液中分离出J-酸尿素。

    Preparation of N-hydroxypyrazoles
    5.
    发明授权
    Preparation of N-hydroxypyrazoles 失效
    N-羟基吡唑的制备

    公开(公告)号：US4945167A

    公开(公告)日：1990-07-31

    申请号：US367047

    申请日：1989-06-16

    申请人： Ulf Baus ,  Wolfgang Reuther ,  Erwin Hahn

    发明人： Ulf Baus ,  Wolfgang Reuther ,  Erwin Hahn

    IPC分类号： C07D231/12 ,  C07D231/16 ,  C07D521/00

    CPC分类号： C07D231/12 ,  C07D231/16 ,  C07D233/56 ,  C07D249/08

    摘要： N-hydroxypyrazoles of the general formula I ##STR1## where R.sup.1, R.sup.2 and R.sup.3 may be identical or different and are each hydrogen or halogen, are prepared by a process in which a pyrazole of the general formula II ##STR2## where R.sup.1, R.sup.2 and R.sup.3 have the meanings stated for formula I, is reacted with an aliphatic or aromatic peroxocarboxylic acid, preferably in the presence of from 0 to 15 moles of an alkali metal hydroxide, alkaline earth metal hydroxide, alkali meteal carbonate or alkaline earth metal carbonate in such a way that the reaction temperature is from -5.degree. C. to 60.degree.C.The reaction can be carried out in water as a solvent or in a 2-phase system consisting of water and an inert organic solvent which is poorly miscible with water, in the presence or absence of a suitable phase transfer catalyst. The peroxocarboxylic acid can be prepared in the reaction mixture before the reaction from H.sub.2 O.sub.2 and an acyl halide or a carboxylic anhydride or can be used in the form of an alkali metal salt or alkaline earth metal salt.

    摘要翻译： 其中R 1，R 2和R 3可以相同或不同并且各自为氢或卤素的通式I（I）的N-羟基吡唑通过其中通式II的吡唑（IMAGE）（ II）其中R 1，R 2和R 3具有式I所述的含义，与脂族或芳族过氧羧酸反应，优选在0至15摩尔碱金属氢氧化物，碱土金属氢氧化物，碱金属碳酸盐 或碱土金属碳酸盐，使得反应温度为-5℃至60℃。该反应可以在作为溶剂的水中或在由水和惰性有机物组成的2相体系中进行 在有或没有合适的相转移催化剂的情况下与水很难混溶的溶剂。 过氧化羧酸可以在与H 2 O 2和酰卤或羧酸酐反应之前在反应混合物中制备，或者可以以碱金属盐或碱土金属盐的形式使用。

    Tetrachloroperylene-3,4,9,10-tetracarboxylic acid diimide pigment and its use
    6.
    发明授权
    Tetrachloroperylene-3,4,9,10-tetracarboxylic acid diimide pigment and its use 失效
    四氯化苯-3,4,9,10-四羧酸二酰亚胺颜料及其用途

    公开(公告)号：US4846892A

    公开(公告)日：1989-07-11

    申请号：US92600

    申请日：1987-09-03

    申请人： Georg Henning ,  Erwin Hahn ,  Peter Hauser ,  Manfred Patsch

    发明人： Georg Henning ,  Erwin Hahn ,  Peter Hauser ,  Manfred Patsch

    IPC分类号： C08K5/3412 ,  C08K5/3437 ,  C09B5/62 ,  C09B67/48 ,  C09D7/12 ,  C09D11/02

    CPC分类号： C09B5/62 ,  C09B67/0025

    摘要： A tetrachloroperylene-3,4,9,10-tetracarboxylic acid diimide pigment which contains not less than 85% by weight of the tetrachloro compound of the formula ##STR1## which is present to the extent of not less than 95% by weight in the .beta.-modification and which, in an X-ray spectrum, exhibits 2.sup..crclbar. CuK.sub..alpha. main lines at 9.0.degree., 13.3.degree., 15.0.degree., 16.8.degree., 19.1.degree., 21.5.degree., 24.2.degree., 25.4.degree., 26.5.degree., 27.0.degree. and 27.5.degree..In finishes, the pigment gives very brilliant colorations which are very highly lightfast and fast to weathering and which, upon weathering, neither bleach nor darken up.

    摘要翻译： 含有不少于85重量％的式“IMAGE”的四氯化合物的四氯化亚丙基-3,4,9,10-四羧酸二酰亚胺颜料，其量为不少于95重量％ 在9.0°，13.3°，15.0°，16.8°，19.1°，21.5°，24.2度，25.4度，26.5度，X射线谱中显示2（ - ）CuKα主线， 27.0°和27.5°。 在表面处理中，颜料产生非常明亮的着色，其具有非常高的耐光性和耐候性，并且在风化时，既不漂白也不变暗。

    Bisazo compounds containing anthranilic acid and thiazole moieties
    7.
    发明授权
    Bisazo compounds containing anthranilic acid and thiazole moieties 失效
    含有邻氨基苯甲酸和噻唑部分的双偶氮化合物

    公开(公告)号：US4694075A

    公开(公告)日：1987-09-15

    申请号：US820018

    申请日：1986-01-21

    申请人： Horst Colberg ,  Erwin Hahn

    发明人： Horst Colberg ,  Erwin Hahn

    IPC分类号： C09B44/02 ,  C09B31/14 ,  C09B44/08 ,  D06P1/04 ,  D06P1/41

    CPC分类号： C09B44/02

    摘要： The compounds of the formula ##STR1## where Y is hydrogen, chlorine, bromine or nitro, Z is hydrogen, chlorine, bromine, a sulfonic ester group or unsubstituted or substituted sulfamyl, X is --O-- or ##STR2## R is alkylene which may or may not be interrupted by oxygen or ##STR3## m is 0 or 1, p is 1 or 2, R.sup.1 and R.sup.2 independently of one another are each hydrogen, unsubstituted or substituted alkyl, alkenyl, cycloalkyl, aralkyl, or aryl, or R.sup.1 and R.sup.2 together with the nitrogen form a heterocyclic structure, R.sup.3 is hydrogen or unsubstituted or substituted alkyl, R.sup.6 and R.sup.7 independently of one another are each hydrogen, unsubstituted or substituted alkyl, alkoxy or acylamino, K is a radical of a coupling component, A.crclbar. is an anion, R.sup.4 is unsubtituted or substituted alkyl and R.sup.5 is hydrogen or C.sub.1 -C.sub.4 -alkyl, and the radical ##STR4## may furthermore be an unsubstituted or substituted piperazine radical, are useful for dyeing acid-modified fibers, leather and in particular paper.

    摘要翻译： 其中Y是氢，氯，溴或硝基，Z是氢，氯，溴，磺酸酯基或未取代或取代的亚磺酰基的式“IMAGE”的化合物，X是-O-或R是 氧可以或不会被氧中断，或者m为0或1，p为1或2，R 1和R 2彼此独立地为氢，未取代或取代的烷基，烯基，环烷基，芳烷基或芳基，或 R 1和R 2与氮一起形成杂环结构，R 3为氢或未取代或取代的烷基，R 6和R 7彼此独立地为氢，未取代或取代的烷基，烷氧基或酰氨基，K为偶联组分的基团， A（ - ）是阴离子，R4是未取代的或取代的烷基，R5是氢或C1-C4-烷基，基团还可以是未取代或取代的哌嗪基，可用于染色酸改性纤维， 皮革，特别是纸张。

    Recycling of cured aminoplast resins
    10.
    发明授权
    Recycling of cured aminoplast resins 失效
    固化的氨基塑料树脂的回收

    公开(公告)号：US5382476A

    公开(公告)日：1995-01-17

    申请号：US247184

    申请日：1994-05-20

    申请人： Juergen Weiser ,  Wolfgang Reuther ,  Erwin Hahn

    发明人： Juergen Weiser ,  Wolfgang Reuther ,  Erwin Hahn

    IPC分类号： C08G14/10 ,  C08J11/16 ,  C09D161/34 ,  C14C3/20 ,  B32B9/04 ,  C14C9/00

    CPC分类号： C08J11/16 ,  C08G14/10 ,  C09D161/34 ,  C14C3/20 ,  C08J2361/20 ,  Y02W30/705 ,  Y10T428/31504 ,  Y10T428/4935

    摘要： Cured aminoplast resins are recycled by a process in which said resins, which may contain fillers, are treated with an aqueous sulfite, hydrogen sulfite or disulfite solution and the resulting low molecular weight degradation products are used in chemical processes. The resulting low molecular weight degradation products of cured aminoplast resins are used for coating moldings, for tanning leather and skins and for the production of moldings which contain cured aminoplast resins or consist thereof.

    摘要翻译： 固化的氨基塑料树脂通过其中可以含有填料的所述树脂用亚硫酸氢盐，亚硫酸氢盐或二亚硫酸盐溶液处理的方法再循环，并且所得到的低分子量降解产物用于化学方法。 所得到的固化的氨基塑料树脂的低分子量降解产物用于涂布模制品，用于鞣制皮革和皮肤，以及用于生产包含固化的氨基塑料树脂或由其组成的模制品。