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    Process for the production of finely divided solid cyanuric chloride
    1.
    发明授权
    Process for the production of finely divided solid cyanuric chloride 失效
    生产精细分散固体氰基氯化物的方法

    公开(公告)号：US4038276A

    公开(公告)日：1977-07-26

    申请号：US716353

    申请日：1976-08-20

    申请人： Friedhelm Geiger ,  Werner Heimberger ,  Theodor Lussling

    发明人： Friedhelm Geiger ,  Werner Heimberger ,  Theodor Lussling

    IPC分类号： C07D251/28

    CPC分类号： C07D251/28

    摘要： Finely divided solid cyanuric chloride is produced by feeding a jet of liquid cyanuric chloride into a separatory container, cooling the liquid cyanuric chloride with recycling inert gases to such an extent that the cyanuric chloride is separated in crystalline form, washing the thereby warmed cyanuric chloride vapor or dust containing gases free of cyanuric chloride in countercurrent flow with an inert liquid that is a good solvent for cyanuric chloride in a washing column connected to the outlet side of the separatory column, thus simultaneously cooling the gases, and subsequently again returning the gases to the separatory container, while the temperature of the cyanuric chloride containing washing liquid which has increased in the washing process is again brought to the original temperature by leading it in the cycle over a heat exchanger and spraying the inside of the pipe connected to the separatory container and leading to the washing column constantly with the washing liquid while dividing a partial stream of the cyanuric chloride containing washing liquid in a distillation column into pure liquid cyanuric chloride which is recycled into the separatory column and into pure washing liquid which is recycled into the washing column.

    Process for obtaining D,L-homocystine (I)
    6.
    发明授权
    Process for obtaining D,L-homocystine (I) 失效
    获得D，L-高胆固醇（I）的方法

    公开(公告)号：US4550199A

    公开(公告)日：1985-10-29

    申请号：US590058

    申请日：1984-03-15

    申请人： Michael Karrenbauer ,  Axel Kleemann ,  Theodor Lussling ,  Fritz Schafer

    发明人： Michael Karrenbauer ,  Axel Kleemann ,  Theodor Lussling ,  Fritz Schafer

    IPC分类号： C07C319/24 ,  C07C67/00 ,  C07C313/00 ,  C07C323/58 ,  C07C149/243

    CPC分类号： C07C319/24

    摘要： D,L-Homocystine is obtained by treating an aqueous solution of the disodium salt of D,L-homocysteine having a concentration between 0.4 and 1.6 moles/l and an initial pH between 7.0 and 8.0 under vigorous stirring with at least the equivalent amount of an aqueous solution of hydrogen peroxide and after the end of the oxidation adjusting the pH to about 5.3. The hydrogen peroxide solution can be employed with a concentration between 20 and 60 weight percent.

    摘要翻译： D，L-高密半胱氨酸通过在剧烈搅拌下处理浓度为0.4〜1.6摩尔/升的D，L-高半胱氨酸的二钠盐水溶液，并在至少等量的 过氧化氢水溶液，氧化结束后将pH调节至约5.3。 过氧化氢溶液可以使用浓度在20至60重量％之间。

    Process for the purification of tryptophane and derivatives of tryptophane
    10.
    发明授权
    Process for the purification of tryptophane and derivatives of tryptophane 失效
    色氨酸和色氨酸衍生物的纯化方法

    公开(公告)号：US4283337A

    公开(公告)日：1981-08-11

    申请号：US94801

    申请日：1979-11-15

    申请人： Theodor Lussling ,  Alfred Maierhofer ,  Paul Scherberich

    发明人： Theodor Lussling ,  Alfred Maierhofer ,  Paul Scherberich

    IPC分类号： C07D209/20

    CPC分类号： C07D209/20

    摘要： Tryptophane and tryptophane derivatives are purified by treating them in an inert solvent at a temperature between about 20.degree. C. and the boiling point of the mixture with a salt of dithionous acid. Preferably there is used as solvent a mixture of water and a lower aliphatic carboxylic acid. Normally a single treatment results in a pure, colorless, satisfactory product.

    摘要翻译： 色氨酸和色氨酸衍生物通过在惰性溶剂中在约20℃和混合物与二硫酸盐的沸点之间的温度下处理来纯化。 优选地，作为溶剂使用水和低级脂肪族羧酸的混合物。 通常单次处理会产生纯净，无色，令人满意的产品。