摘要:
Preparation of alkanolamines having improved color quality by treating the alkanolamine with an effective amount of phosphorous acid or hypophosphorous acid or compounds thereof initially at elevated temperature over a period of at least 5 min (step a), and then distilling it in the presence of an effective amount of one of these phosphorus compounds (step b).
摘要:
Monoisopropylamine is prepared by reacting acetone with ammonia and with hydrogen at elevated temperature and elevated pressure in the presence of a catalyst, wherein the catalytically active mass of the catalyst comprises, after its preparation and before the treatment with hydrogen, from 20 to 90% by weight of aluminum oxide (Al2O3), zirconium dioxide (ZrO2), titanium dioxide (TiO2) and/or silicon dioxide (SiO2), from 1 to 70% by weight of oxygen-containing compounds of copper, calculated as CuO, from 1 to 70% by weight of oxygen-containing compounds of nickel, calculated as NiO, and from 1 to 70% by weight of oxygen-containing compounds of cobalt, calculated as CoO.
摘要翻译:通过使丙酮与氨和氢气在升高的温度和升高的压力下在催化剂存在下反应制备单异丙胺,其中催化活性物质在其制备之后和在用氢处理之前包含20-90% 氧化铝(Al 2 O 3),二氧化锆(ZrO 2),二氧化钛(TiO 2)和/或二氧化硅(SiO 2)的重量,1至70重量%的以CuO计的氧含氧化合物,1至 70重量%的以NiO计的含氧化合物的镍和1-70重量%的以CoO计的钴的含氧化合物。
摘要:
A catalyst comprising, based on the total weight of the catalyst,more than 6-50% by weight of cobalt, nickel or a mixture thereof,0.001-25% by weight of ruthenium,0-10% by weight of copper and0-5% by weight of promoterson a porous metal oxide carrier can be prepared by(a) impregnating the carrier with the metals, promoters or compounds thereof,(b) drying and calcining the impregnated carrier and(c) reducing the calcined carrier in a stream of hydrogen,carrier not being impregnated with halogen compounds.
摘要:
In a process for preparing 1,3,5-tris(2-hydroxyalkyl) isocyanurates from cyanuric acid and aliphatic epoxides, the reaction is carried out in the presence of catalytic amounts of an organic phosphorus compound.