公开(公告)号：US20140054521A1

公开(公告)日：2014-02-27

申请号：US13671150

申请日：2012-11-07

申请人： HY-POWER NANO INC.

发明人： Hadi K. Mahabadi ,  Juan-Pablo Bravo-Vasquez ,  Sinoj Abraham ,  Guibin Ma ,  Nathan Gerein

IPC分类号： C01G19/02 ,  H01B1/08 ,  G02B1/00

CPC分类号： C01G19/02 ,  B82Y20/00 ,  B82Y30/00 ,  C01G19/00 ,  C01P2002/72 ,  C01P2002/76 ,  C01P2004/03 ,  C01P2004/20 ,  C01P2004/32 ,  C01P2004/51 ,  C01P2004/62 ,  C01P2004/64 ,  C01P2006/80 ,  C03C17/007 ,  C03C2217/231 ,  C03C2218/114 ,  G02B1/002 ,  G02B5/206 ,  G02B5/208 ,  G02B2207/101 ,  H01B1/08

摘要： Disclosed herein are indium-tin-oxide nanoparticles and a method for continuously producing precipitated indium-tin nanoparticles having a particle size range of substantially from about 10 nm to about 200 nm and a substantially consistent ratio of indium to tin in the resultant nanoparticles across the duration of the continuous process, based on the ratio of indium to tin in a seeding solution. The method comprises preparing intermediate indium and tin compounds of the general formula [M(OH)xCy], where M represents the indium or tin ionic component of indium or tin salts, C represents the cationic component of indium or tin salt(s), x is a number greater than 0 and y=[M*valance−x]/C* valance in the seeding solution. The intermediate compounds are continuously precipitated with a base solution in a reaction vessel initially having a solvent contained therein. The method also provides a means for controlling the shape of the resultant nanoparticles. The resultant indium-tin nanoparticles may be further processed into dispersions.

摘要翻译： 本文公开了铟锡氧化物纳米颗粒和用于连续生产具有基本上约10nm至约200nm的粒度范围的沉淀的铟锡纳米颗粒的方法，并且在所得纳米颗粒中的铟与锡的比例基本上一致 基于接种溶液中铟与锡的比例，连续过程的持续时间。 该方法包括制备通式[M（OH）xCy]的中间体铟和锡化合物，其中M表示铟或锡盐的铟或锡离子组分，C表示铟或锡盐的阳离子组分， x是接种溶液中大于0且y = [M * valance-x] / C *值的数。 中间体化合物在最初具有其中包含溶剂的反应容器中用碱溶液连续沉淀。 该方法还提供了用于控制所得纳米颗粒的形状的手段。 所得的铟锡纳米颗粒可进一步加工成分散体。

公开(公告)号：US09296622B2

公开(公告)日：2016-03-29

申请号：US13671150

申请日：2012-11-07

申请人： HY-POWER NANO INC.

发明人： Hadi K Mahabadi ,  Juan-Pablo Bravo-Vasquez ,  Sinoj Abraham ,  Guibun Ma ,  Nathan Gerein

IPC分类号： F21V9/04 ,  F21V9/06 ,  G02B5/22 ,  G02B5/26 ,  C01G19/02 ,  G02B1/00 ,  H01B1/08 ,  C01G19/00 ,  G02B5/20 ,  B82Y20/00 ,  B82Y30/00 ,  C03C17/00 ,  C01G17/02 ,  C01G21/02

CPC分类号： C01G19/02 ,  B82Y20/00 ,  B82Y30/00 ,  C01G19/00 ,  C01P2002/72 ,  C01P2002/76 ,  C01P2004/03 ,  C01P2004/20 ,  C01P2004/32 ,  C01P2004/51 ,  C01P2004/62 ,  C01P2004/64 ,  C01P2006/80 ,  C03C17/007 ,  C03C2217/231 ,  C03C2218/114 ,  G02B1/002 ,  G02B5/206 ,  G02B5/208 ,  G02B2207/101 ,  H01B1/08

摘要： Disclosed herein are indium-tin-oxide nanoparticles and a method for continuously producing precipitated indium-tin nanoparticles having a particle size range of substantially from about 10 nm to about 200 nm and a substantially consistent ratio of indium to tin in the resultant nanoparticles across the duration of the continuous process, based on the ratio of indium to tin in a seeding solution. The method comprises preparing intermediate indium and tin compounds of the general formula [M(OH)xCy], where M represents the indium or tin ionic component of indium or tin salts, C represents the cationic component of indium or tin salt(s), x is a number greater than 0 and y=[M*valance−x]/C* valance in the seeding solution. The intermediate compounds are continuously precipitated with a base solution in a reaction vessel initially having a solvent contained therein. The method also provides a means for controlling the shape of the resultant nanoparticles. The resultant indium-tin nanoparticles may be further processed into dispersions.

摘要翻译： 本文公开了铟锡氧化物纳米颗粒和用于连续生产具有基本上约10nm至约200nm的粒度范围的沉淀的铟锡纳米颗粒的方法，并且在所得纳米颗粒中的铟与锡的比例基本上一致 基于接种溶液中铟与锡的比例，连续过程的持续时间。 该方法包括制备通式[M（OH）xCy]的中间体铟和锡化合物，其中M表示铟或锡盐的铟或锡离子组分，C表示铟或锡盐的阳离子组分， x是接种溶液中大于0且y = [M * valance-x] / C *值的数。 中间体化合物在最初具有其中包含溶剂的反应容器中用碱溶液连续沉淀。 该方法还提供了用于控制所得纳米颗粒的形状的手段。 所得的铟锡纳米颗粒可进一步加工成分散体。