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公开(公告)号：US10012438B2
公开(公告)日：2018-07-03
申请号：US15057148
申请日：2016-03-01
申请人： Hai Du , Neil M. Prosser , Yang Luo , Neil A. Stephenson
发明人： Hai Du , Neil M. Prosser , Yang Luo , Neil A. Stephenson
IPC分类号： F25J1/00 , F25J3/04 , B01D53/047
CPC分类号： F25J3/04733 , B01D53/047 , B01D2253/102 , B01D2253/108 , B01D2253/116 , B01D2257/11 , F25J3/0409 , F25J3/04096 , F25J3/04103 , F25J3/04296 , F25J3/04303 , F25J3/04412 , F25J3/04678 , F25J3/04739 , F25J3/04884 , F25J3/04939 , F25J2205/02 , F25J2205/60 , F25J2245/58 , F25J2250/02 , F25J2270/02 , F25J2290/34
摘要： A method and apparatus for argon recovery in which an impure argon stream is separated from air within a cryogenic air separation unit having a divided wall argon rejection/rectification column. The resulting argon stream is subsequently recovered and purified within an integrated pressure swing adsorption system to produce product grade argon.
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公开(公告)号：US20170030642A1
公开(公告)日：2017-02-02
申请号：US15057148
申请日：2016-03-01
申请人： Hai Du , Neil M. Prosser , Yang Luo , Neil A. Stephenson
发明人： Hai Du , Neil M. Prosser , Yang Luo , Neil A. Stephenson
IPC分类号： F25J3/04 , B01D53/047
CPC分类号： F25J3/04733 , B01D53/047 , B01D2253/102 , B01D2253/108 , B01D2253/116 , B01D2257/11 , F25J3/0409 , F25J3/04096 , F25J3/04103 , F25J3/04296 , F25J3/04303 , F25J3/04412 , F25J3/04678 , F25J3/04739 , F25J3/04884 , F25J3/04939 , F25J2205/02 , F25J2205/60 , F25J2245/58 , F25J2250/02 , F25J2270/02 , F25J2290/34
摘要： A method and apparatus for argon recovery in which an impure argon stream is separated from air within a cryogenic air separation unit having a divided wall argon rejection/rectification column. The resulting argon stream is subsequently recovered and purified within an integrated pressure swing adsorption system to produce product grade argon.
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公开(公告)号：US10012437B2
公开(公告)日：2018-07-03
申请号：US15057152
申请日：2016-03-01
申请人： Hai Du , Neil M. Prosser , Yang Luo , Neil A. Stephenson
发明人： Hai Du , Neil M. Prosser , Yang Luo , Neil A. Stephenson
IPC分类号： F25J3/04 , B01D53/047 , C01B23/00
CPC分类号： F25J3/04412 , B01D53/047 , B01D2256/18 , B01D2257/102 , B01D2257/104 , C01B23/0036 , C01B23/0078 , C01B2210/0034 , C01B2210/0045 , C01B2210/0048 , F25J3/0409 , F25J3/04096 , F25J3/04103 , F25J3/04296 , F25J3/04303 , F25J3/04678 , F25J3/04733 , F25J3/04739 , F25J3/04884 , F25J3/04939 , F25J2205/02 , F25J2205/60 , F25J2245/58 , F25J2250/02 , F25J2270/02 , F25J2290/34
摘要： A method and apparatus for argon recovery in which an impure argon stream is separated from air within a cryogenic air separation unit having a divided wall argon rejection/rectification column. The resulting argon stream is subsequently recovered and purified within an integrated pressure swing adsorption system to produce product grade argon.
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4.发明申请METHOD AND APPARATUS FOR ARGON RECOVERY IN A CRYOGENIC AIR SEPARATION UNIT INTEGRATED WITH A PRESSURE SWING ADSORPTION SYSTEM 有权用压力旋转吸附系统集成的低温空气分离单元中ARGON回收的方法和装置公开(公告)号：US20170030639A1
公开(公告)日：2017-02-02
申请号：US15057152
申请日：2016-03-01
申请人： Hai Du , Neil M. Prosser , Yang Luo , Neil A. Stephenson
发明人： Hai Du , Neil M. Prosser , Yang Luo , Neil A. Stephenson
IPC分类号： F25J3/04 , F25J3/02 , B01D53/047
CPC分类号： F25J3/04412 , B01D53/047 , B01D2256/18 , B01D2257/102 , B01D2257/104 , C01B23/0036 , C01B23/0078 , C01B2210/0034 , C01B2210/0045 , C01B2210/0048 , F25J3/0409 , F25J3/04096 , F25J3/04103 , F25J3/04296 , F25J3/04303 , F25J3/04678 , F25J3/04733 , F25J3/04739 , F25J3/04884 , F25J3/04939 , F25J2205/02 , F25J2205/60 , F25J2245/58 , F25J2250/02 , F25J2270/02 , F25J2290/34
摘要： A method and apparatus for argon recovery in which an impure argon stream is separated from air within a cryogenic air separation unit having a divided wall argon rejection/rectification column. The resulting argon stream is subsequently recovered and purified within an integrated pressure swing adsorption system to produce product grade argon.
摘要翻译： 一种用于氩气回收的方法和装置，其中不纯的氩气流在具有分隔壁氩排斥/精馏塔的低温空气分离单元内与空气分离。 随后将所得氩气流在集成的变压吸附系统中回收和纯化，以产生产品级氩气。
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公开(公告)号：US10018413B2
公开(公告)日：2018-07-10
申请号：US15057156
申请日：2016-03-01
申请人： Hai Du , Neil A. Stephenson , Neil M. Prosser
发明人： Hai Du , Neil A. Stephenson , Neil M. Prosser
IPC分类号： F25J3/02 , F25J3/04 , B01D53/047
CPC分类号： F25J3/04412 , B01D3/141 , B01D53/047 , B01D2256/18 , B01D2257/102 , B01D2257/104 , F25J3/0409 , F25J3/04096 , F25J3/04103 , F25J3/04296 , F25J3/04303 , F25J3/04678 , F25J3/04733 , F25J3/04739 , F25J3/04884 , F25J3/04939 , F25J2200/80 , F25J2205/02 , F25J2205/60 , F25J2245/58 , F25J2250/02 , F25J2270/02 , F25J2290/34
摘要： A method and apparatus for increasing argon recovery in which an impure argon stream is separated from air within a cryogenic air separation unit and purified within an integrated, multi-stage pressure swing adsorption system to produce product grade argon with high argon recovery levels.
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6.发明申请METHOD AND APPARATUS FOR INCREASING ARGON RECOVERY IN A CRYOGENIC AIR SEPARATION UNIT INTEGRATED WITH A PRESSURE SWING ADSORPTION SYSTEM 有权用于增加压缩空气分离单元中ARGON回收的方法和装置与压力旋转吸收系统公开(公告)号：US20170030640A1
公开(公告)日：2017-02-02
申请号：US15057156
申请日：2016-03-01
申请人： Hai Du , Neil A. Stephenson , Neil M. Prosser
发明人： Hai Du , Neil A. Stephenson , Neil M. Prosser
IPC分类号： F25J3/04 , F25J3/02 , B01D53/047
CPC分类号： F25J3/04412 , B01D53/047 , B01D2256/18 , B01D2257/102 , B01D2257/104 , F25J3/0409 , F25J3/04096 , F25J3/04103 , F25J3/04296 , F25J3/04303 , F25J3/04678 , F25J3/04733 , F25J3/04739 , F25J3/04884 , F25J3/04939 , F25J2200/80 , F25J2205/02 , F25J2205/60 , F25J2245/58 , F25J2250/02 , F25J2270/02 , F25J2290/34
摘要： A method and apparatus for increasing argon recovery in which an impure argon stream is separated from air within a cryogenic air separation unit and purified within an integrated, multi-stage pressure swing adsorption system to produce product grade argon with high argon recovery levels.
摘要翻译： 一种用于增加氩气回收的方法和装置，其中不纯的氩气流与低温空气分离装置内的空气分离，并在集成的多级变压吸附系统内纯化，以产生具有高氩回收水平的产品级氩气。
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公开(公告)号：US09222727B2
公开(公告)日：2015-12-29
申请号：US13782636
申请日：2013-03-01
CPC分类号： F25J3/08 , C01B23/0052 , C01B23/0068 , C01B23/0078 , C01B2210/0021 , C01B2210/0034 , C01B2210/0045 , F25J3/04733 , F25J2205/60 , F25J2220/44
摘要： The invention relates to a process for removing oxygen from liquid argon using a TSA (temperature swing adsorption) cyclical process that includes cooling an adsorbent bed to sustain argon in a liquid phase; supplying the adsorbent bed with a liquid argon feed that is contaminated with oxygen and purifying the liquid argon thereby producing an argon product with less oxygen contaminant than is in the initial liquid argon feed; draining the purified residual liquid argon product and sending purified argon out of the adsorbent bed. Regeneration of specially prepared adsorbent allows the adsorbent bed to warm up to temperatures that preclude the use of requiring either vacuum or evacuation of adsorbent from the bed.
摘要翻译： 本发明涉及使用TSA（变温吸附）循环过程从液氩中除去氧气的方法，其包括冷却吸附床以维持液相氩; 向吸附床提供被氧气污染的液态氩气进料并净化液态氩气，从而产生比初始液态氩气进料中氧气污染物少的氩气产物; 排出纯化的残余液氩产品并将纯化的氩气送出吸附剂床。 特别制备的吸附剂的再生允许吸附剂床温热到不需要真空或从床抽真空吸附剂的温度。
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公开(公告)号：US10295255B2
公开(公告)日：2019-05-21
申请号：US15244359
申请日：2016-08-23
申请人： Philip A. Barrett , Neil A. Stephenson , Nicholas R. Stuckert , Michael Freiert , Hai Du , Rachael A. Masin , Garrett R. Swindlehurst
发明人： Philip A. Barrett , Neil A. Stephenson , Nicholas R. Stuckert , Michael Freiert , Hai Du , Rachael A. Masin , Garrett R. Swindlehurst
摘要： An adsorption process for xenon recovery from a cryogenic liquid or gas stream is described wherein a bed of adsorbent is contacted with the aforementioned xenon containing liquid or gas stream and adsorbs the xenon selectively from this fluid stream. The adsorption bed is operated to at least near full breakthrough with xenon to enable a deep rejection of other stream components, prior to regeneration using the temperature swing method. Operating the adsorption bed to near full breakthrough with xenon, prior to regeneration, enables production of a high purity product from the adsorption bed and further enables oxygen to be used safely as a purge gas, even in cases where hydrocarbons are co-present in the feed stream.
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公开(公告)号：US20180058758A1
公开(公告)日：2018-03-01
申请号：US15244359
申请日：2016-08-23
申请人： Philip A. Barrett , Neil A. Stephenson , Nicholas R. Stuckert , Michael Freiert , Hai Du , Rachael A. Masin , Garrett R. Swindlehurst
发明人： Philip A. Barrett , Neil A. Stephenson , Nicholas R. Stuckert , Michael Freiert , Hai Du , Rachael A. Masin , Garrett R. Swindlehurst
IPC分类号： F25J3/06
CPC分类号： F25J3/0685 , B01D53/0462 , B01D2253/106 , B01D2253/108 , B01D2257/11 , B01D2257/402 , B01D2257/702 , B01D2259/40056 , B01J20/186 , B01J20/3092 , B01J20/3408 , B01J20/3458 , B01J2220/56 , C01B23/0068 , C01B23/0078 , C01B2210/0037 , C01B2210/007 , F25J3/0695 , F25J2205/68 , F25J2205/70 , F25J2215/36 , Y02C20/10 , Y02P20/153
摘要： An adsorption process for xenon recovery from a cryogenic liquid or gas stream is described wherein a bed of adsorbent is contacted with the aforementioned xenon containing liquid or gas stream and adsorbs the xenon selectively from this fluid stream. The adsorption bed is operated to at least near full breakthrough with xenon to enable a deep rejection of other stream components, prior to regeneration using the temperature swing method. Operating the adsorption bed to near full breakthrough with xenon, prior to regeneration, enables production of a high purity product from the adsorption bed and further enables oxygen to be used safely as a purge gas, even in cases where hydrocarbons are co-present in the feed stream.
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10.发明授权公开(公告)号：US09676629B2
公开(公告)日：2017-06-13
申请号：US14734522
申请日：2015-06-09
申请人： Hai Du , Scot E. Jaynes , Steven R. Falta , Neil A. Stephenson
发明人： Hai Du , Scot E. Jaynes , Steven R. Falta , Neil A. Stephenson
CPC分类号： C01B23/0078 , B01D53/0438 , B01D53/0462 , B01D2256/18 , B01D2257/102 , B01D2257/104 , B01D2259/402 , C01B2210/0034 , C01B2210/0045 , F25J3/04775 , F25J3/08 , F25J2205/64
摘要： The present invention generally relates to a method to enhance heat transfer in the temperature swing adsorption process (TSA) and to an intensified TSA process for gas/liquid purification or bulk separation. Helium is designed as the heat carrier media to directly bring heat/cool to the adsorbent bed during the TSA cycling process. With helium's superior heat conductivity, the time consuming regeneration steps (warming, regeneration and precooling) of TSA process can be significantly reduced and allowing for the TSA process to be intensified.
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