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    Reaction of organic compounds over macroporous supported catalysts comprising boron oxide
    5.
    发明授权
    Reaction of organic compounds over macroporous supported catalysts comprising boron oxide 失效
    有机化合物与包含氧化硼的大孔载体催化剂反应

    公开(公告)号：US06432861B1

    公开(公告)日：2002-08-13

    申请号：US09349082

    申请日：1999-07-08

    申请人： Boris Breitscheidel ,  Uwe Diehlmann ,  Alois Kindler ,  Jochem Henkelmann ,  Arnd Böttcher

    发明人： Boris Breitscheidel ,  Uwe Diehlmann ,  Alois Kindler ,  Jochem Henkelmann ,  Arnd Böttcher

    IPC分类号： C08F804

    CPC分类号： C08F8/04 ,  B01J21/02

    摘要： In a process for reacting an organic compound in the presence of a catalyst comprising, as active metal, at least one metal of transition group VIII of the Periodic Table, either alone or together with at least one metal of transition group I or VII of the Periodic Table, in an amount of from 0.01 to 30% by weight, based on the total weight of the catalyst, applied to a support containing macropores, the support comprises, as a support component, boron(III) oxide in an amount of from 10 to 100% by weight, based on the total weight of the support.

    摘要翻译： 在一种催化剂存在下使有机化合物反应的方法，该催化剂包含作为活性金属的至少一种元素周期表第VIII族金属，单独或与至少一种第 周期表，以基于催化剂总重量的0.01至30重量％的量施用于含有大孔的载体，载体包含作为载体组分的氧化硼（III），其量为 10至100重量％，基于载体的总重量。

    Preparation of alkynediols
    6.
    发明授权
    Preparation of alkynediols 失效
    炔二醇的制备

    公开(公告)号：US06369282B1

    公开(公告)日：2002-04-09

    申请号：US09577127

    申请日：2000-05-24

    申请人： Alois Kindler ,  Thomas Preiss ,  Jochem Henkelmann

    发明人： Alois Kindler ,  Thomas Preiss ,  Jochem Henkelmann

    IPC分类号： C07C3118

    CPC分类号： C07C29/42 ,  C07C33/044 ,  C07C33/046

    摘要： The process for preparing alkynediols of the formula (I) R1R2C(OH)—C≡C—C(OH)R1R2  (I) where R1, R2 are each independently H, or a C1-20-hydrocarbon radical which may be substituted by one or more C1-6-alkyls and/or be interrupted by nonadjacent heteroatoms and/or contain C—C double or triple bonds, by reacting compounds of the formula (II) R1—C(═O)—R2  (II) with acetylene in a polar aprotic solvent is carried out in the presence of basic alkali metal salts as catalysts.

    摘要翻译： 制备式（I）的炔二醇的方法，其中R 1，R 2各自独立地为H，或可被一个或多个C 1-6 - 烷基取代和/或被不相邻的杂原子中断的C 1-20烃基和/ 或含有CC双键或三键，通过使式（II）化合物与极性非质子溶剂中的乙炔反应，在碱性碱金属盐作为催化剂的存在下进行。

    Method for producing alkyne diols
    7.
    发明授权
    Method for producing alkyne diols 失效
    炔二醇的制备方法

    公开(公告)号：US06297407B1

    公开(公告)日：2001-10-02

    申请号：US09744437

    申请日：2001-01-24

    申请人： Alois Kindler ,  Melanie Brunner ,  Christian Tragut ,  Jochem Henkelmann

    发明人： Alois Kindler ,  Melanie Brunner ,  Christian Tragut ,  Jochem Henkelmann

    IPC分类号： C07C3118

    CPC分类号： C07C29/42 ,  C07C33/042 ,  C07C33/044

    摘要： The invention relates to a method for producing alkyne diols by reacting ketones with acetylenic hydrocarbons in an organic solvent in the presence of a base which contains potassium alcoholates of primary and/or secondary alcohols. The alkyne diols are produced while forming adducts which precipitate out of the reaction mixture and which are comprised of alkyne monoalcohols and/or alkyne diols and a base. The stoichiometries of the reaction partners are selected such that gelatinous adducts are formed which comprise a spherical surface, whereby the reaction mixture remains agitable during the entire reaction.

    摘要翻译： 本发明涉及一种在含有伯醇和/或仲醇的醇钾的碱存在下，通过酮与炔烃在有机溶剂中反应制备炔烃的方法。 产生炔二醇，同时形成从反应混合物中沉淀的加合物，其由炔一醇和/或炔二醇和碱组成。 选择反应伴侣的化学计量，使得形成包含球形表面的凝胶状加合物，由此在整个反应期间反应混合物保持敏感。

    Method for the production of acetylene alcohols
    8.
    发明申请
    Method for the production of acetylene alcohols 审中-公开
    生产乙炔醇的方法

    公开(公告)号：US20050272963A1

    公开(公告)日：2005-12-08

    申请号：US10523925

    申请日：2003-07-23

    申请人： Jochem Henkelmann ,  Alois Kindler ,  Jan-Dirk Arndt ,  Katrin Klass

    发明人： Jochem Henkelmann ,  Alois Kindler ,  Jan-Dirk Arndt ,  Katrin Klass

    IPC分类号： C07B61/00 ,  C07C29/42 ,  C07C33/042 ,  C07C33/048 ,  C07C33/14 ,  C07C33/48 ,  C07C403/00 ,  C07C33/04 ,  C07F1/02

    CPC分类号： C07C29/42 ,  C07C403/08 ,  C07C2601/16 ,  C07C33/042 ,  C07C33/048 ,  C07C33/14 ,  C07C33/48

    摘要： The present invention relates to a process for preparing acetylene alcohols of the general formula I where R1 and R2 may be the same or different and are each independently hydrogen, a saturated or a mono- or polyunsaturated C1-C30-alkyl, aryl, cycloalkylalkyl or cycloalkyl radical, each of which may optionally be substituted, or a group of the general formula (II) where R3 and R4 may be the same or different and are each independently hydrogen or a saturated or a mono- or polyunsaturated C1-C30-alkyl, aryl, cycloalky alkyl or cycloalkyl radical, each of which may optionally be substituted, and the dashed line may represent an additional double bond, by monoethynylating a ketone of the general formula R1—CO—R2 by (a) reacting lithium with a C1-C10-alkyl halide (b) feeding in acetylene gas (c) adding the ketone.

    摘要翻译： 本发明涉及一种制备通式I的乙炔醇的方法，其中R 1和R 2可以相同或不同，各自独立地为氢，饱和的 或单或多不饱和C 1 -C 30 - 烷基，芳基，环烷基烷基或环烷基，其各自可以任选被取代，或一个通式 （II）其中R 3和R 4可以相同或不同，各自独立地为氢或饱和或单不饱和或不饱和的C 1〜 其中每一个可以被任选地被取代，并且虚线可以代表另外的双键，通过使通式（I）的酮单乙炔基化， 通过（a）使锂与C 1 -C 10 - 烷基 - 取代的C 1 -C 10 - 烷基 卤化物（b）在乙炔气中进料（c）加入酮。