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公开(公告)号：US4237299A
公开(公告)日：1980-12-02
申请号：US748041
申请日：1976-12-06
IPC分类号： C07D213/08 , C07D213/09 , C07D213/12 , C07D213/16
CPC分类号： C07D213/08 , C07D213/12
摘要： Pyridine and 3-methylpyridine prepared by the catalytic reaction of acrolein or a mixture of acetaldehyde and acrolein with ammonia is recovered from the gas mixture formed by cooling the gas mixture and working up the condensate separated in the cooling. The gaseous mixture is first cooled to a temperature between 40.degree. and about 80.degree. C. and then cooled to a temperature between about 10.degree. and below 40.degree. C.
摘要翻译： 通过丙烯醛或乙醛和丙烯醛与氨的混合物的催化反应制备的吡啶和3-甲基吡啶从通过冷却气体混合物形成的气体混合物中回收并处理在冷却中分离的冷凝物。 首先将气体混合物冷却至40℃至80℃之间的温度，然后冷却至约10℃至40℃以下的温度。
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公开(公告)号：US4447615A
公开(公告)日：1984-05-08
申请号：US288186
申请日：1981-07-29
IPC分类号： C07D213/82 , C07D213/81 , C07D211/72 , C07D211/84 , C07D213/56
CPC分类号： C07D213/81
摘要： Crude nicotinamide is purified by a recrystallization and in this way freed especially from nicotinic acid and salts of nicotinic acid. As solvent there is used a 2-methylpropanol-1 containing water. The recrystallization takes place at a pH between about 7 and 10.
摘要翻译： 粗烟酰胺通过重结晶纯化，以这种方式从烟酸和烟酸盐中释放出来。 作为溶剂，使用含有2-甲基丙醇-1的水。 重结晶发生在约7至10之间的pH。
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公开(公告)号：US4447614A
公开(公告)日：1984-05-08
申请号：US288187
申请日：1981-07-29
IPC分类号： C07D213/82 , C07D213/81 , C07D211/72 , C07D211/84 , C07D213/56
CPC分类号： C07D213/81
摘要： Crude nicotinamide is purified by a recrystallization and thereby is particularly freed from nicotinic acid and salts of nicotinic acid. As solvent there is used 2-methylpropanol-1 containing water. The warm solution after dissolving the crude nicotinamide is treated with ion exchangers.
摘要翻译： 粗烟酰胺通过重结晶纯化，特别是从烟酸和烟酸盐中脱除。 作为溶剂，使用含有2-甲基丙醇-1的水。 溶解粗烟酰胺后的温热溶液用离子交换剂处理。
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公开(公告)号：US4171445A
公开(公告)日：1979-10-16
申请号：US622488
申请日：1975-10-15
申请人： Helmut Beschke , Heinz Friedrich , Gerd Schreyer
发明人： Helmut Beschke , Heinz Friedrich , Gerd Schreyer
IPC分类号： C07D213/12
CPC分类号： C07D213/12
摘要： Pyridine and 3-methyl pyridine are prepared by reacting acrolein with ammonia in the gas phase on a catalyst in a fluidized bed. The acrolein and ammonia are introduced separately in gaseous form into the reactor.
摘要翻译： 吡啶和3-甲基吡啶通过在气相中的丙烯醛与氨在流化床中的催化剂上反应来制备。 将丙烯醛和氨分别以气态引入反应器。
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公开(公告)号：US4139536A
公开(公告)日：1979-02-13
申请号：US676197
申请日：1976-04-12
IPC分类号： C07D213/82 , C07D213/81 , C07D213/56
CPC分类号： C07D213/81
摘要： Nicotinamide is recovered from the reaction mixture resulting from the hydrolysis of nicotinonitrile at elevated temperature by converting the nicotinamide into a melt while removing the solvent.
摘要翻译： 通过将烟酰胺转化成熔体同时除去溶剂，从高温下烟腈腈水解得到的反应混合物中回收烟酰胺。
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公开(公告)号：US4314064A
公开(公告)日：1982-02-02
申请号：US192038
申请日：1980-09-29
IPC分类号： C07D213/82 , C07D213/81 , C07D213/56
CPC分类号： C07D213/81
摘要： Nicotinamide is prepared from nicotinonitrile by hydrolysis at 120.degree. to 200.degree. C. employing alkali hydroxide.
摘要翻译： 使用碱金属氢氧化物，在120〜200℃水解由烟腈制得烟酰胺。
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7.发明授权Animal feed additive based on fermentation broth, a process for its production and its use 失效基于发酵液的动物饲料添加剂，其生产和使用的过程
公开(公告)号：US5622710A
公开(公告)日：1997-04-22
申请号：US518222
申请日：1995-08-23
申请人： Wolfram Binder , Franz-Ludwig Dahm , Ulrich Hertz , Heinz Friedrich , Hermann Lotter , Wolfgang Hohn , Dieter Greissinger , Wolfgang Polzer
发明人： Wolfram Binder , Franz-Ludwig Dahm , Ulrich Hertz , Heinz Friedrich , Hermann Lotter , Wolfgang Hohn , Dieter Greissinger , Wolfgang Polzer
CPC分类号： A23K20/142 , A23K10/12 , A23K40/10 , A23K40/20
摘要： An animal feed additive comprising stable pellets is produced by pelletizing from a fermentation broth containing an animal feed additive with at least 33% by weight of the fermentation products present. The pellets can be produced particularly effectively by pelletizing providing they are built up from at least 30% by weight of fine particles of which at least 70% by weight are smaller than 100 .mu.m in size. The biomass may be completely present, partly present or not present at all in the pellets.
摘要翻译： 包含稳定颗粒的动物饲料添加剂通过从含有至少33重量％存在的发酵产物的动物饲料添加剂的发酵液中造粒而产生。 颗粒可以通过造粒而特别有效地生产，只要它们由至少70重量％至少70重量％的小于100μm的细小颗粒构成。 生物质可以完全存在，部分存在或完全不存在于颗粒中。
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公开(公告)号：US4496729A
公开(公告)日：1985-01-29
申请号：US511574
申请日：1983-07-07
CPC分类号： C07D241/24 , B01J21/16 , B01J23/22 , B01J23/34 , B01J23/84 , B01J35/10 , B01J35/1014 , B01J35/1038 , B01J35/1066 , B01J35/1071
摘要： For the catalytic reaction of 2-methylpyrazine with ammonia and oxygen to form 2-cyanopyrazine there are used compounds of the elements antimony, vanadium, and oxygen and at least one of the elements iron, copper, titanium, cobalt, manganese, and nickel, whereby the atomic ratio of antimony to vanadium is greater than 1 and which contain besides these compounds a lattice layer silicate and a highly dispersed silica. These catalysts are very selective and result in high yields and high space-time-yields.
摘要翻译： 对于2-甲基吡嗪与氨和氧的形成2-氰基吡嗪的催化反应，使用元素锑，钒和氧以及铁，铜，钛，钴，锰和镍中的至少一种元素， 由此锑与钒的原子比大于1，除了这些化合物外，还含有晶格层硅酸盐和高度分散的二氧化硅。 这些催化剂是非常有选择性的并且导致高产率和高的空时产率。
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公开(公告)号：US4169951A
公开(公告)日：1979-10-02
申请号：US830982
申请日：1977-09-06
申请人： Helmut Beschke , Heinz Friedrich
发明人： Helmut Beschke , Heinz Friedrich
IPC分类号： C07D213/12 , C07D213/22 , C07D213/02 , C07D213/08
CPC分类号： C07D213/22 , C07D213/12
摘要： Pyridines substituted in the 2- and 3-positions by aromatic or heteroaromatic groups are prepared by reacting an aromatic or heteroaromatic substituted ketone which has at least one reactive methylene group adjacent to the keto group with an aliphatic oxo compound having a carbon to carbon ethylenic double bond on the carbon atom adjacent to the oxo group and ammonia in the presence of a dehydrating and dehydrogenating catalyst at a temperature of about 250.degree. to 550.degree. C.
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公开(公告)号：US4163854A
公开(公告)日：1979-08-07
申请号：US871979
申请日：1978-01-24
申请人： Helmut Beschke , Heinz Friedrich
发明人： Helmut Beschke , Heinz Friedrich
IPC分类号： C07D213/09 , B01J21/00 , C07B61/00 , C07D213/12
CPC分类号： C07D213/12
摘要： 3-Methyl pyridine is produced by the catalytic reaction of acrolein and propionaldehyde with ammonia in the gas phase. There is used as the catalyst a highly dispersed aluminum silicate containing 3 to 30 weight percent aluminum oxide, a BET surface area of 200 to 800 m.sup.2 /g, a pore volume of 0.4 to 1.0 cm.sup.3 /g and a pore diameter of 20 to 100.times.10.sup.-8 cm.
摘要翻译： 3-甲基吡啶通过丙烯醛和丙醛与氨在气相中的催化反应而产生。 使用含有3〜30重量％的氧化铝，BET表面积为200〜800m 2 / g，孔体积为0.4〜1.0cm 3 / g，孔径为20〜100×10 6的高度分散的硅酸铝作为催化剂 -8厘米。
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