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公开(公告)号：US20170096438A1
公开(公告)日：2017-04-06
申请号：US15294920
申请日：2016-10-17
申请人： Henkel AG & Co. KGaA
发明人： David Briers , Johann Klein , Esteban Mejia , Udo Kragl , Ralf Dunekake , Marleen Winterberg , Jens Baumgard
IPC分类号： C07F7/21
CPC分类号： C07F7/21
摘要： The present invention relates to a method for preparing functionalized cyclosiloxanes of Formula I, wherein R, R1, R2, m, n1 and n2 are as defined herein, comprising reacting (i) a cyclosiloxane of Formula II with (ii) a substituted acetylene of Formula III in the presence of a hydrosilylation catalyst. The invention further relates to methods for preparing biscyclosiloxanes by reacting the vinyl cyclosiloxanes obtained according to the described methods and the (bis)cyclosiloxanes obtainable according to the described methods.
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公开(公告)号：US08969457B2
公开(公告)日：2015-03-03
申请号：US13798598
申请日：2013-03-13
申请人： Henkel AG & Co. KGaA
发明人： David Briers
CPC分类号： C09D163/00 , C08G59/68 , C08G65/105 , C08G65/18 , C08L63/00 , C08L2312/06
摘要： The present invention relates to a curable composition, which comprises a) at least one radiation-curable resin, b) at least one specific anti-oxidant and c) at least one photoinitiator salt. The invention further relates to a cured product made from the curable composition. The curable compositions and/or the cured products thereof are particularly suitable as laminating adhesives, sealants, and/or encapsulants for electronic or optoelectronic devices.
摘要翻译： 本发明涉及可固化组合物，其包含a）至少一种辐射固化树脂，b）至少一种特定的抗氧化剂和c）至少一种光引发剂盐。 本发明还涉及由可固化组合物制成的固化产物。 可固化组合物和/或其固化产物特别适用于电子或光电器件的层压粘合剂，密封剂和/或密封剂。
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公开(公告)号：US11326027B2
公开(公告)日：2022-05-10
申请号：US16441451
申请日：2019-06-14
申请人： Henkel AG & Co. KGaA
发明人： Marleen Winterberg , Marta Woznicka , Annika Dietrich , Esteban Mejia , Udo Kragl , Christina Despotopoulou , Ralf Dunekake , David Briers , Johann Klein , Henrik Lund
IPC分类号： C08G77/46 , C08G77/16 , C07F7/08 , C08G77/08 , C08G77/388 , C08G77/14 , C08G65/336
摘要： A method for producing a hydroxyl-functionalized polysiloxane having secondary or tertiary hydroxyl groups, said method comprising the steps of: i) reacting a hydroxyalkyl allyl ether having a secondary or tertiary alcohol group with a siloxane under anhydrous conditions and under transition metal catalysis, said hydroxylalkyl allyl ether conforming to Formula (I) wherein n is 0, 1, 2, 3, 4 or 5, preferably 0; m is 1, 2, 3, 4 or 5, preferably 1; spacer group A is constituted by a covalent bond or a C1-C20 alkylene group; R1 is hydrogen, a C1-C8 alkyl group, a C3-C10 cycloalkyl group, a C6-C18 aryl group or an aralkyl group; Ra, Rb, Rc, Rd, R2, R3, R4 and R5 may be the same or different and each is independently selected from hydrogen, a C1-C8 alkyl group, a C6-C18 aryl group or a C6-C18 aralkyl group, with the proviso that at least one of R3 and R4 is not hydrogen; and said siloxane conforming to Formula (II) wherein m is 1, 2, 3, 4 or 5, preferably 1; R6, R7, R8 and R9 may be the same or different and each represent a C1-C8 alkyl group, a C3-C10 cycloalkyl group, a C6-C18 aryl group or a C6-C18 aralkyl group; and ii) in the presence of the reaction product of step i), performing a ring opening polymerization of at least one cyclic siloxane monomer.
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公开(公告)号：US20190322808A1
公开(公告)日：2019-10-24
申请号：US16441451
申请日：2019-06-14
申请人： Henkel AG & Co. KGaA
发明人： Marleen Winterberg , Marta Woznicka , Annika Dietrich , Esteban Mejia , Udo Kragl , Christina Despotopoulou , Ralf Dunekake , David Briers , Johann Klein , Henrik Lund
摘要： A method for producing a hydroxyl-functionalized polysiloxane having secondary or tertiary hydroxyl groups, said method comprising the steps of: i) reacting a hydroxyalkyl allyl ether having a secondary or tertiary alcohol group with a siloxane under anhydrous conditions and under transition metal catalysis, said hydroxylalkyl allyl ether conforming to Formula (I) wherein n is 0, 1, 2, 3, 4 or 5, preferably 0; m is 1, 2, 3, 4 or 5, preferably 1; spacer group A is constituted by a covalent bond or a C1-C20 alkylene group; R1 is hydrogen, a C1-C8 alkyl group, a C3-C10 cycloalkyl group, a C6-C18 aryl group or an aralkyl group; Ra, Rb, Rc, Rd, R2, R3, R4 and R5 may be the same or different and each is independently selected from hydrogen, a C1-C8 alkyl group, a C6-C18 aryl group or a C6-C18 aralkyl group, with the proviso that at least one of R3 and R4 is not hydrogen; and said siloxane conforming to Formula (II) wherein m is 1, 2, 3, 4 or 5, preferably 1; R6, R7, R8 and R9 may be the same or different and each represent a C1-C8 alkyl group, a C3-C10 cycloalkyl group, a C6-C18 aryl group or a C6-C18 aralkyl group; and ii) in the presence of the reaction product of step i), performing a ring opening polymerization of at least one cyclic siloxane monomer.
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公开(公告)号：US20190031812A1
公开(公告)日：2019-01-31
申请号：US16152599
申请日：2018-10-05
申请人： Henkel AG & Co. KGaA
发明人： Ralf Baetzgen , Jan-Erik Damke , David Briers , Johann Klein
摘要： A silylated polyurethane obtainable by a process comprising the following steps: (a) reacting at least one polyol with at least one triisocyanate to form a hydroxyl-terminated polyurethane prepolymer, and (b) reacting said polyurethane prepolymer with at least one isocyanatosilane of the formula (1): OCN—R—Si—(X)m(R1)3-m, wherein m is 0, 1 or 2, each R1 is independently from each other a hydroxyl group, an alkoxy group having 1 to 10 carbon atoms, an acyloxy group having 1 to 10 carbon atoms, or —OCH(R2)COOR3, wherein R2 is hydrogen or an alkyl group having 1 to 4 carbon atoms and R3 is a straight-chain or branched alkyl group having 1 to 8 carbon atoms, each X is independently from each other and optionally substituted hydrocarbon group having 1 to 10 carbon atoms, which can be interrupted by at least one heteroatom, and R is a difunctional organic group, to endcap the hydroxyl groups on said prepolymer with said isocyanatosilane. The silylated polyurethanes are suitable for use in a preparation as an adhesive, sealant, or coating agent.
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公开(公告)号：US20130187144A1
公开(公告)日：2013-07-25
申请号：US13798598
申请日：2013-03-13
申请人： Henkel AG & Co. KGaA
发明人： David Briers
IPC分类号： H01L51/00 , C09D163/00 , G03F7/00 , H01L21/00
CPC分类号： C09D163/00 , C08G59/68 , C08G65/105 , C08G65/18 , C08L63/00 , C08L2312/06
摘要： The present invention relates to a curable composition, which comprises a) at least one radiation-curable resin, b) at least one specific anti-oxidant and c) at least one photoinitiator salt. The invention further relates to a cured product made from the curable composition. The curable compositions and/or the cured products thereof are particularly suitable as laminating adhesives, sealants, and/or encapsulants for electronic or optoelectronic devices.
摘要翻译： 本发明涉及可固化组合物，其包含a）至少一种辐射固化树脂，b）至少一种特定的抗氧化剂和c）至少一种光引发剂盐。 本发明还涉及由可固化组合物制成的固化产物。 可固化组合物和/或其固化产物特别适用于电子或光电器件的层压粘合剂，密封剂和/或密封剂。
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公开(公告)号：US10118984B2
公开(公告)日：2018-11-06
申请号：US15697499
申请日：2017-09-07
申请人： Henkel AG & Co. KGaA
发明人： Ralf Bätzgen , Jan-Erik Damke , David Briers , Johann Klein
摘要： A silylated polyurethane obtainable by a process comprising the following steps: (a) reacting at least one polyol with at least one triisocyanate to form a hydroxyl-terminated polyurethane prepolymer, and (b) reacting said polyurethane prepolymer with at least one isocyanatosilane of the formula (1): OCN—R—Si—(X)m(R1)3−m, wherein m is 0, 1 or 2, each R1 is independently from each other a hydroxyl group, an alkoxy group having 1 to 10 carbon atoms, an acyloxy group having 1 to 10 carbon atoms, or —OCH(R2)COOR3, wherein R2 is hydrogen or an alkyl group having 1 to 4 carbon atoms and R3 is a straight-chain or branched alkyl group having 1 to 8 carbon atoms, each X is independently from each other and optionally substituted hydrocarbon group having 1 to 10 carbon atoms, which can be interrupted by at least one heteroatom, and R is a difunctional organic group, to endcap the hydroxyl groups on said prepolymer with said isocyanatosilane. The silylated polyurethanes are suitable for use in a preparation as an adhesive, sealant, or coating agent.
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公开(公告)号：US10059728B2
公开(公告)日：2018-08-28
申请号：US15294920
申请日：2016-10-17
申请人： Henkel AG & Co. KGaA
发明人： David Briers , Johann Klein , Esteban Mejia , Udo Kragl , Ralf Dunekake , Marleen Winterberg , Jens Baumgard
CPC分类号： C07F7/21
摘要： The present invention relates to a method for preparing functionalized cyclosiloxanes of Formula I, wherein R, R1, R2, m, n1 and n2 are as defined herein, comprising reacting (i) a cyclosiloxane of Formula II with (ii) a substituted acetylene of Formula III in the presence of a hydrosilylation catalyst. The invention further relates to methods for preparing biscyclosiloxanes by reacting the vinyl cyclosiloxanes obtained according to the described methods and the (bis)cyclosiloxanes obtainable according to the described methods.
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公开(公告)号：US20170362371A1
公开(公告)日：2017-12-21
申请号：US15697499
申请日：2017-09-07
申请人： Henkel AG & Co. KGaA
发明人： Ralf Bätzgen , Jan-Erik Damke , David Briers , Johann Klein
CPC分类号： C08G18/10 , C08G18/227 , C08G18/4825 , C08G18/718 , C08G18/792
摘要： A silylated polyurethane obtainable by a process comprising the following steps: (a) reacting at least one polyol with at least one triisocyanate to form a hydroxyl-terminated polyurethane prepolymer, and (b) reacting said polyurethane prepolymer with at least one isocyanatosilane of the formula (1): OCN—R—Si—(X)m(R1)3-m, wherein m is 0, 1 or 2, each R1 is independently from each other a hydroxyl group, an alkoxy group having 1 to 10 carbon atoms, an acyloxy group having 1 to 10 carbon atoms, or —OCH(R2)COOR3, wherein R2 is hydrogen or an alkyl group having 1 to 4 carbon atoms and R3 is a straight-chain or branched alkyl group having 1 to 8 carbon atoms, each X is independently from each other and optionally substituted hydrocarbon group having 1 to 10 carbon atoms, which can be interrupted by at least one heteroatom, and R is a difunctional organic group, to endcap the hydroxyl groups on said prepolymer with said isocyanatosilane. The silylated polyurethanes are suitable for use in a preparation as an adhesive, sealant, or coating agent.
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