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    Intermediate Product Comprised of a Mixture of Organic Carbonates and Carbamates and a Method for Its Manufacture
    1.
    发明申请
    Intermediate Product Comprised of a Mixture of Organic Carbonates and Carbamates and a Method for Its Manufacture 审中-公开
    由有机碳酸盐和氨基甲酸酯混合物组成的中间体产品及其制造方法

    公开(公告)号：US20070252106A1

    公开(公告)日：2007-11-01

    申请号：US10571997

    申请日：2004-07-16

    申请人： Henning Buchold ,  Jurgen Eberhardt ,  Ulrich Wagner ,  Hans-Jorg Wolk

    发明人： Henning Buchold ,  Jurgen Eberhardt ,  Ulrich Wagner ,  Hans-Jorg Wolk

    IPC分类号： C07C69/96 ,  C07C271/12 ,  C07D323/00 ,  C08G65/333 ,  C07C68/00

    CPC分类号： C08G65/324 ,  C07C68/00 ,  C07C69/96 ,  C07D323/00 ,  C08G65/325 ,  C08L71/02 ,  C08L2666/04

    摘要： The invention relates to an intermediate product based on the organic carbonates and carbamates mixture and method for the production thereof. The inventive method consists in reacting a carbamide, a substituted carbamide, a carbamic acid salt or ester or one of the N-substituted derivatives thereof in a glycol polyalkylene, polyol polyester or a polyol polyether of general formula (I), wherein R is a linear or branched alkylene group having from 2 to 12 carbon atoms and n is a number ranging from 1 to 20, or in a totally or partly hydrolysed polyvinyl alcohol of general formula (II), wherein R′ is an alkyl, aryl or acyl group having from 1 to 12 carbon atoms p and q are numbers ranging from 1 to 20, or dissolving in the mixture of said compounds with an alkaline catalyst promoting the ammonia separation. The thus free ammonia or an amine produced by the reaction mixture is removed by a stripping gas.

    摘要翻译： 本发明涉及一种基于有机碳酸酯和氨基甲酸酯混合物的中间产物及其生产方法。 本发明的方法在于使脲，取代的脲，氨基甲酸盐或其N-取代的衍生物之一或其中一个在通式（I）的二醇聚亚烷基，多元醇多酯或多元醇多元醇中反应，其中R为 具有2至12个碳原子且n为1至20的数的直链或支链亚烷基，或在通式（II）的全部或部分水解的聚乙烯醇中，其中R'为烷基，芳基或酰基 具有1至12个碳原子的p和q为1至20的数，或者将所述化合物的混合物与促进氨分离的碱性催化剂溶解。 由游离氨或由反应混合物产生的胺通过汽提气体除去。

    Method for the production of organic carbonates
    2.
    发明申请
    Method for the production of organic carbonates 失效
    生产有机碳酸酯的方法

    公开(公告)号：US20070082985A1

    公开(公告)日：2007-04-12

    申请号：US10571476

    申请日：2004-07-16

    申请人： Henning Buchold ,  Jurgen Eberhardt ,  Ulrich Wagner ,  Hans-Jorg Wolk

    发明人： Henning Buchold ,  Jurgen Eberhardt ,  Ulrich Wagner ,  Hans-Jorg Wolk

    IPC分类号： C08K5/49

    CPC分类号： C07C68/00 ,  C07C69/96

    摘要： The invention relates to a method for the production of monomer organic carbonates, wherein urea, substituted urea, a salt or an ester of carbamide acid or one of the N-substituted derivatives thereof is reacted in a first step in a polyalkylene glycol, a polyester-polyol or a polyether-polyol of general formula (I), wherein R represents a linear or branched alkylene group having 2-12 carbon atoms and n is a number between (2) and (20), or in a completely or partially hydrolysed polyvinyl alcohol of general formula (II) wherein R′ represents an alkyl group, an aryl group or an acyl group having 1-12 carbon atoms, p and q are numbers between 1 and 20, or in mixtures of said compounds in the presence of a catalyst facilitating the separation of ammonia in order to form a mixture containing carbonates and carbamates, the ammonia becomes free or the amine is removed form the reaction mixture by means of a strip gas. In a second reaction step (transesterification), the mixture containing the carbonates and carbamates is reacted with a monomer alcohol or a phenol whereby monomer carbonates are formed and polymer polyalcohols of formulae (I) or (II) are reformed. HO—RnOH  (I)

    摘要翻译： 本发明涉及一种制备单体有机碳酸酯的方法，其中脲，取代的脲，脲或其中的一种或多种N-取代的衍生物的脲或其酯之一在第一步骤中在聚亚烷基二醇，聚酯 - 多元醇或通式（I）的聚醚多元醇，其中R表示具有2-12个碳原子的直链或支链亚烷基，n是（2）和（20）之间的数，或者在完全或部分水解的 通式（II）的聚乙烯醇，其中R'表示烷基，芳基或具有1-12个碳原子的酰基，p和q是1至20之间的数字，或所述化合物在存在下的 促进氨分离以形成含有碳酸酯和氨基甲酸酯的混合物的催化剂，氨变得游离，或者通过带状气体从反应混合物中除去胺。 在第二反应步骤（酯交换）中，将含有碳酸酯和氨基甲酸酯的混合物与单体醇或苯酚反应，由此形成单体碳酸酯，并且将式（I）或（II）的聚合物多元醇重整。 <？in-line-formula description =“In-line Formulas”end =“lead”？> H OR OH（I）<？in-line-formula description =“In-line Formulas”end =“tail”？>

    Method for the production of organic carbonates
    3.
    发明申请
    Method for the production of organic carbonates 失效
    生产有机碳酸酯的方法

    公开(公告)号：US20070203322A1

    公开(公告)日：2007-08-30

    申请号：US10571479

    申请日：2004-07-16

    申请人： Honning Buchold ,  Jurgen Eberhardt ,  Ulrich Wagner ,  Hans-Jorg Wolk

    发明人： Honning Buchold ,  Jurgen Eberhardt ,  Ulrich Wagner ,  Hans-Jorg Wolk

    IPC分类号： C08G64/00

    CPC分类号： C07C68/06 ,  C07C68/00 ,  C07C69/96

    摘要： The invention relates to a method for the production of monomer organic carbonates from a mixture of organic carbonates and carbamates which are obtained by reacting urea, substituted urea, a salt or ester of carbamide acid or one of the N-substituted derivatives thereof with a polyalkylene glycol, polyester-polyol or a polyether-polyol of general formula (I), wherein R represents a linear or branched alkylene group having 2-12 carbon atoms and n represents a number between 2 and 20, or with a completely or partially hydrolysed polyvinyl alcohol of general formula (II), wherein R′ represents an alkyl group, an aryl group or an acyl group having 1-12 carbon atoms, p and q represent a number between 120, or with mixtures of said compounds in the presence of a catalyst facilitating the separation of ammonia and the ammonia becomes free or the amine is removed from the reaction mixture by means of a strip gas, whereby said mixture is reacted m with an alcohol or a phenol whereby monomer carbonates are formed and polymer polyalcohols of formulae (I) or (II) are reformed.

    摘要翻译： 本发明涉及一种由有机碳酸酯和氨基甲酸酯的混合物制备单体有机碳酸酯的方法，其通过使脲，取代的脲，脲酰胺酸的盐或酯或其N-取代的衍生物之一与聚亚烷基 乙二醇，聚酯多元醇或通式（I）的聚醚多元醇，其中R表示具有2-12个碳原子的直链或支链亚烷基，n表示2至20的数，或具有完全或部分水解的聚乙烯 通式（II）的醇，其中R'表示烷基，芳基或具有1-12个碳原子的酰基，p和q表示120之间的数，或与所述化合物在存在下的 促进氨分离的催化剂变得游离，或者通过带状气体从反应混合物中除去胺，由此所述混合物与醇或酚反应，由此单体ca 形成波长形成物，将式（I）或（II）的聚合物多元醇重整。