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    Process for recovering resorcinol and hydroquinone in mixture
    1.
    发明授权
    Process for recovering resorcinol and hydroquinone in mixture 失效
    在混合物中回收间苯二酚和氢醌的方法

    公开(公告)号：US3969420A

    公开(公告)日：1976-07-13

    申请号：US375920

    申请日：1973-07-02

    申请人： Hideaki Suda ,  Iwao Dohgane ,  Takashi Chinuki ,  Kenji Tanimoto ,  Hirokazu Hosaka ,  Yukimichi Nakao ,  Yuji Ueda ,  Seiya Imada ,  Hideki Yanagihara ,  Kunihiko Tanaka

    发明人： Hideaki Suda ,  Iwao Dohgane ,  Takashi Chinuki ,  Kenji Tanimoto ,  Hirokazu Hosaka ,  Yukimichi Nakao ,  Yuji Ueda ,  Seiya Imada ,  Hideki Yanagihara ,  Kunihiko Tanaka

    IPC分类号： C07C27/00 ,  C07C37/72 ,  C07C37/84 ,  C07C39/08 ,  C07C67/00 ,  C07C37/24

    CPC分类号： C07C37/72 ,  C07C37/685 ,  C07C37/84

    摘要： Resorcinol and hydroquinone are recovered in mixture at a high purity from a solution containing resorcinol and hydroquinone, especially, a solution resulting from cleavage of oxidation products of isopropylbenzene and successive distillation of the cleavage product thereby to remove lower and higher boiling components therefrom, by adding 0.5 to 20 parts by weight of at least one solvent selected from aromatic hydrocarbons, aromatic hydrocarbons having lower alkyl substituent groups, and aliphatic hydrocarbons having 7 to 10 carbon atoms to one part by weight of said solution, if necessary, together with 1 to 30% by weight of at least one compound selected from ketones having 3 to 10 carbon atoms, alcohols having 1 to 5 carbon atoms and aliphatic esters having 3 to 5 carbon atoms, based on the weight of the organic solvent, dissolving the solution into the organic solvent by heating, separating a mixture of resorcinol and hydroquinone as a solid phase from the organic solvent layer after slow cooling, and recovering the solid phase as a product. The resorcinol and hydroquinone in the organic solvent layer are further recovered through extraction with water. When water is used together with the organic solvent from the beginning of extraction, the resorcinol and hydrocarbon are obtained in an aqueous layer.

    摘要翻译： 间苯二酚和氢醌以高纯度从含有间苯二酚和氢醌的溶液中回收，特别是从裂解异丙苯的氧化产物产生的溶液，并连续蒸馏裂解产物，从而通过加入从其中除去较低沸点和较高沸点的组分 0.5至20重量份的至少一种选自芳族烃，具有低级烷基取代基的芳族烃和具有7至10个碳原子的脂族烃的溶剂相对于所述溶液的1重量份，如果需要，连同1至30个 至少一种选自具有3至10个碳原子的化合物，具有1至5个碳原子的醇和3至5个碳原子的脂肪族酯的化合物，基于有机溶剂的重量，将该溶液溶解在有机溶剂中 溶剂，从有机溶剂层af分离作为固相的间苯二酚和氢醌的混合物 缓慢冷却，并回收作为产品的固相。 有机溶剂层中的间苯二酚和氢醌通过水提取进一步回收。 当水从开始开始与有机溶剂一起使用时，在水层中获得间苯二酚和烃。

    Method for extraction of dihydroperoxide
    6.
    发明授权
    Method for extraction of dihydroperoxide 失效
    二氢过氧化物提取方法

    公开(公告)号：US4059637A

    公开(公告)日：1977-11-22

    申请号：US607020

    申请日：1975-08-22

    申请人： Hirokazu Hosaka ,  Kenji Tanimoto ,  Hiromichi Okabe ,  Kunthiko Tanaka ,  Yuji Ueda ,  Iwao Dohgane

    发明人： Hirokazu Hosaka ,  Kenji Tanimoto ,  Hiromichi Okabe ,  Kunthiko Tanaka ,  Yuji Ueda ,  Iwao Dohgane

    IPC分类号： C07C409/12 ,  C07C67/00 ,  C07C407/00 ,  C07C179/02

    CPC分类号： C07C407/003

    摘要： A method for extracting a dihydroperoxide of a dialkylbenzene of the formula, ##STR1## wherein each R.sub.1, R.sub.2, R.sub.3 and R.sub.4 is independently a lower alkyl group, from an aqueous alkali solution of the said dihydroperoxide with at least one organic solvent selected from the group consisting of C.sub.4 -C.sub.10 ketones, C.sub.4 -C.sub.10 ethers and C.sub.4 -C.sub.8 alcohols, which comprises extracting the dihydroperoxide by a countercurrent multi-stage extraction at a temperature between 0.degree. and 85.degree. C with a temperature gradient, the aqueous alkali solution being fed to the lower temperature zone, the organic solvent being fed to the higher temperature zone, and each aqueous alkali solution and organic solvent being fed countercurrently, whereby the dihydroperoxide is obtained in the form of organic solvent solution from the lower temperature zone.

    摘要翻译： 一种提取下式的二烷基苯的二氢过氧化物的方法，其中每个R 1，R 2，R 3和R 4各自为低级烷基，所述二氢过氧化物的碱性水溶液与至少一种选自以下的有机溶剂 其包括C4-C10酮，C4-C10醚和C4-C8醇，其包括在0℃至85℃之间的温度梯度下通过逆流多级萃取萃取二氢过氧化物，碱水溶液为 进料到较低温度区域，将有机溶剂进料到较高温度区域，并将每种碱性水溶液和有机溶剂逆流进料，由此从低温区获得有机溶剂溶液形式的二氢过氧化物。

    Process for producing alkylnaphthalenes
    8.
    发明授权
    Process for producing alkylnaphthalenes 失效
    制备烷基萘的方法

    公开(公告)号：US3985819A

    公开(公告)日：1976-10-12

    申请号：US513188

    申请日：1974-10-08

    申请人： Katsumi Kobayashi ,  Iwao Dohgane ,  Hiromichi Okabe ,  Kenji Tanimoto

    发明人： Katsumi Kobayashi ,  Iwao Dohgane ,  Hiromichi Okabe ,  Kenji Tanimoto

    IPC分类号： C07C2/68 ,  C07C2/70 ,  C07C3/56 ,  C07C15/24

    CPC分类号： C07C2/68 ,  C07C2/70 ,  C07C2527/11 ,  C07C2527/126

    摘要： A process for producing alkylnaphthalenes by alkylating naphthalene with an olefin having 2 to 4 carbon atoms, which comprises (1) introducing the olefin into a solution of crude naphthalene containing thianaphthene as an impurity in a solvent having a boiling point sufficiently different from the boiling point of the naphthalene and alkylnaphthalenes produced that the solvent is separable by distillation in the presence of (i) an aluminum chloride complex consisting of (a) aluminum chloride, (b) hydrogen chloride and (c) an alkylated benzene or naphthalene, or (ii) a solid aluminum chloride which is dissolved into the reaction solution by adding gaseous hydrogen chloride simultaneously with or prior to the introducing of the olefin, (2) aging the reaction solution, and (3) recovering the resulting alkylnaphthalenes, whereby alkylnaphthalenes, containing as monoalkylnaphthalenes a predominant amount of a .beta.-monoalkylnaphthalene, are obtained in a high yield.

    摘要翻译： 通过用具有2〜4个碳原子的烯烃烷基化萘来制造烷基萘的方法，其包括：（1）将烯烃作为杂质引入到具有与沸点充分不同的沸点的溶剂中作为杂质， 的萘和烷基萘产生溶剂在（i）由（a）氯化铝，（b）氯化氢和（c）烷基化的苯或萘组成的氯化铝络合物存在下蒸馏分离，或（ii） ）固体氯化铝，其通过在引入烯烃的同时或之前加入气态氯化氢而溶解到反应溶液中，（2）使反应溶液老化，和（3）回收所得的烷基萘，由此烷基萘含有 以高产率获得主要量的β-单烷基萘的单烷基萘。

    Process for producing .beta.-isopropyl-naphthalene hydroperoxide
    9.
    发明授权
    Process for producing .beta.-isopropyl-naphthalene hydroperoxide 失效
    制备{62-异丙基萘氢过氧化物的方法

    公开(公告)号：US4049720A

    公开(公告)日：1977-09-20

    申请号：US551812

    申请日：1975-02-21

    申请人： Hirokazu Hosaka ,  Kenji Tanimoto ,  Hiroshi Yamachika

    发明人： Hirokazu Hosaka ,  Kenji Tanimoto ,  Hiroshi Yamachika

    IPC分类号： C07C409/02 ,  C07C67/00 ,  C07C407/00 ,  C07C409/08 ,  C07C179/02

    CPC分类号： C07C409/08 ,  C07C407/00 ,  Y02P20/582

    摘要： A process for the continuous production of .beta.-isopropylnaphthalene hydroperoxide comprising oxidizing an isopropylnaphthalene mixture containing .alpha.- and .beta.-isopropylnaphthalene isomers with molecular oxygen or a molecular oxygen containing gas in an oxidation zone and recycling unreacted ispropylnaphthalene recoverd after the oxidation to the oxidation zone, in which the oxidation is carried out by controlling the .alpha.-isopropylnaphthalene content in the isopropylnaphthalene mixture continuously fed to the oxidation zone to about 15% by weight or less.

    摘要翻译： 连续生产β-异丙基氢过氧化物的方法，包括在氧化区中氧化含有α-和β-异丙基萘异构体的异丙基萘混合物与分子氧或含分子氧的气体，并将氧化后的未反应的异丙基萘回收至氧化区， 其中氧化通过将连续进料至氧化区的异丙基萘混合物中的α-异丙基萘含量控制在约15重量％以下来进行。

    Refrigeration apparatus
    10.
    发明授权
    Refrigeration apparatus 失效
    制冷装置

    公开(公告)号：US07752864B2

    公开(公告)日：2010-07-13

    申请号：US11659121

    申请日：2005-08-01

    申请人： Masaaki Takegami ,  Takeo Ueno ,  Kenji Tanimoto ,  Satoru Sakae

    发明人： Masaaki Takegami ,  Takeo Ueno ,  Kenji Tanimoto ,  Satoru Sakae

    IPC分类号： F25B13/00

    CPC分类号： F25B13/00 ,  F25B2313/0231

    摘要： A refrigeration apparatus (1) is provided with a refrigerant circuit (1E) along which are connected a compressor (2), an outdoor heat exchanger (4), an expansion mechanism, an indoor heat exchanger (41) for providing room air conditioning, and a cooling heat exchanger (45, 51) for providing storage compartment cooling. The refrigerant circuit (1E) includes a discharge side three way switch valve (101) for varying the flow rate of a portion of the refrigerant which is discharged out of the compressor (2) and then distributed to the indoor heat exchanger (41) and the outdoor heat exchanger (4) during a heat recovery operation mode in which the indoor heat exchanger (41) and the outdoor heat exchanger (4) operate as condensers. As a result of such arrangement, even when the amount of heat obtained in the cooling heat exchanger (45, 51) exceeds the amount of heat required in the indoor heat exchanger (41), surplus heat is discharged without excessive decrease in the discharge pressure of the compressor (2).

    摘要翻译： 制冷装置（1）具备：制冷剂回路（1E），连接有压缩机（2），室外热交换器（4），膨胀机构，室内空调用的室内热交换器（41） 以及用于提供储藏室冷却的冷却热交换器（45,51）。 制冷剂回路（1E）包括排出侧三通切换阀（101），用于改变从压缩机（2）排出的一部分制冷剂的流量，然后分配到室内热交换器（41）和 在室内热交换器（41）和室外热交换器（4）作为冷凝器运转的热回收运转模式中的室外热交换器（4）。 作为这种结构的结果，即使在冷却热交换器（45,51）中获得的热量超过室内热交换器（41）所需的热量的情况下，也可以排出多余的热量而不会使排出压力过度降低 的压缩机（2）。