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公开(公告)号：US5804634A
公开(公告)日：1998-09-08
申请号：US763071
申请日：1996-12-10
CPC分类号： C08L67/00
摘要： Disclosed herein is a liquid crystalline resin compound which includes about 100 pbw of liquid crystalline resin and about 5-200 pbw of inorganic filler, the liquid crystalline resin being composed of about 99.5-50 wt % of partially aromatic liquid crystalline polyester resin and about 0.5-50 wt % of wholly aromatic liquid crystalline polyester resin, and the inorganic filler having an average aspect ratio in the range of 3 to 25. Also disclosed is a molded article of liquid crystalline resin obtained by molding from the liquid crystalline resin compound. The resin compound is superior in flowability and the molded article has good mechanical properties, especially balanced rigidity and toughness.
摘要翻译： 本文公开了一种液晶树脂化合物，其包含约100pbw的液晶树脂和约5-200pbw的无机填料，液晶树脂由约99.5-50wt％的部分芳族液晶聚酯树脂和约0.5 -50重量％的全芳族液晶聚酯树脂，以及平均长径比在3〜25的范围内的无机填料。还公开了通过从液晶树脂化合物成型得到的液晶树脂的成型体。 树脂化合物的流动性优异，成型体具有良好的机械性能，特别是刚性和韧性平衡。
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公开(公告)号：US5980777A
公开(公告)日：1999-11-09
申请号：US998377
申请日：1997-12-24
申请人： Hideyuki Umetsu , Yoshiki Makabe , Toshihide Inoue
发明人： Hideyuki Umetsu , Yoshiki Makabe , Toshihide Inoue
摘要： A liquid crystalline resin which comprises at least one kind of liquid crystalline polymer selected from liquid crystalline polyester and liquid crystalline polyester amide, both forming an anisotropic molten phase, and an inorganic phosphorus compound, said liquid crystalline resin having an absorbance of 0.5 or less at 380 nm when measured over an optical path length of 10 mm in a 0.5 wt % solution in a 1:1 mixed solvent of pentafluorophenol and chloroform (by weight). It is useful as engineering plastics because of improved color, heat resistance, and hydrolytic resistance.
摘要翻译： 一种液晶树脂，其包含至少一种选自液晶聚酯和液晶聚酯酰胺的液晶聚合物，两者都形成各向异性熔融相和无机磷化合物，所述液晶树脂的吸光度为0.5以下，吸光度为 在0.5重量％的五氟苯酚和氯仿的混合溶剂（重量比）的溶液中在10mm的光程长度上测量时为380nm。 由于改善了颜色，耐热性和耐水解性，因此可用作工程塑料。
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公开(公告)号：US6075114A
公开(公告)日：2000-06-13
申请号：US91435
申请日：1998-06-29
申请人： Hideyuki Umetsu , Yoshiki Makabe , Toshihide Inoue
发明人： Hideyuki Umetsu , Yoshiki Makabe , Toshihide Inoue
CPC分类号： C08K3/32 , C08K3/02 , C08K2003/026
摘要： A liquid-crystalline resin composition comprising 100 parts by weight of a semi-aromatic liquid-crystalline polyester and/or a semi-aromatic liquid-crystalline polyester-amide, from 0.001 to 5 parts by weight of at least one or more compounds selected from phosphorous acid, hypophosphorous acid and their salts, and from 0.01 to 10 parts by weight of red phosphorus has good flame retardancy, low anisotropy, good heat resistance and good hydrolysis resistance, and is useful as engineering plastic.
摘要翻译： PCT No.PCT / JP98 / 01747 Sec。 371日期1998年6月29日第 102（e）日期1998年6月29日PCT提交1998年4月16日PCT公布。 公开号WO98 / 49232 日期1998年11月5日一种液晶树脂组合物，其包含100重量份的半芳族液晶聚酯和/或半芳族液晶聚酯 - 酰胺，0.001至5重量份的至少一种 或更多选自亚磷酸，次磷酸及其盐的化合物和0.01至10重量份的红磷具有良好的阻燃性，低各向异性，良好的耐热性和良好的耐水解性，并且可用作工程塑料。
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4.发明授权Liquid crystalline polyester composition and metal composite molded product using the same 有权液晶聚酯组合物和使用其的金属复合成型制品公开(公告)号：US09085672B2
公开(公告)日：2015-07-21
申请号：US14009535
申请日：2011-12-14
CPC分类号： C08K3/34 , C08K3/346 , C08K7/14 , C09K19/3809 , C08L67/03
摘要： A liquid crystalline polyester composition contains 100 parts by weight of a liquid crystalline polyester (A) and 10 to 100 parts by weight of a mica (B), wherein a rate in number of mica with a ratio (d1/d2) of a long diameter (d1) to a short diameter (d2) that is greater than 2.0, to an entire content of the mica (B) contained in the liquid crystalline polyester composition is not higher than 20%.
摘要翻译： 液晶聚酯组合物包含100重量份的液晶聚酯（A）和10至100重量份的云母（B），其中云母数量的比率（d1 / d2）为长 对于液晶聚酯组合物中含有的云母（B）的全部含量，直径（d1）至大于2.0的短径（d2）不大于20％。
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5.发明授权公开(公告)号：US08916673B2
公开(公告)日：2014-12-23
申请号：US13996815
申请日：2011-12-19
CPC分类号： B01J19/02 , B01J19/0066 , B01J19/18 , B01J2219/00029 , B01J2219/0006 , B01J2219/00094 , B01J2219/00182 , B01J2219/00189 , B01J2219/0236 , C08G63/605 , C08G63/785
摘要： The present invention provides a process for producing a liquid crystalline polyester resin, wherein an acetylation reaction and an oligomerization reaction of raw materials are carried out in an acetylation reaction vessel, and then a deacetylation polycondensation of a liquid after the oligomerization reaction is carried out in a polycondensation reaction vessel, wherein the acetylation reaction vessel used is a vessel having an inner wall surface composed of an alloy containing 50% by mass or more of Ni and 10% by mass or more of Mo; and the inner wall surface of the acetylation reaction vessel is divided into three or more band-like zones arrayed in the height direction of the vessel, and the oligomerization reaction is carried out while maintaining the temperatures of each band-like zone in a particular relationship.
摘要翻译： 本发明提供一种液晶聚酯树脂的制造方法，其中在乙酰化反应容器中进行原料的乙酰化反应和低聚反应，然后在低聚反应后进行液体的脱乙酰基缩聚 缩聚反应容器，其中使用的乙酰化反应容器是具有由含有50质量％以上的Ni和10质量％以上的Mo的合金构成的内壁面的容器， 并将乙酰化反应容器的内壁表面分成在容器的高度方向排列的三个以上的带状区域，在保持各带状区域的温度为特定关系的同时进行低聚反应 。
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6.发明授权公开(公告)号：US08784683B2
公开(公告)日：2014-07-22
申请号：US13637738
申请日：2011-12-14
IPC分类号： C09K19/52 , C09K19/54 , G02F1/13 , C09K19/02 , C09K19/00 , B29B7/00 , B29C45/00 , C08F283/00 , C08G63/91 , C08L67/00 , B60C1/00 , C08K3/04
摘要： A liquid crystalline polyester composition contains at least 100 parts by weight of liquid crystalline polyester having different structural units and 10 to 100 parts by weight of glass fiber, wherein the glass fiber has a weight-average fiber length (Mw) of 200 to 500 μm, and content of specific glass fiber having fiber length of not less than 1500 μm is 0.1 to 5.0 percent by weight to a total amount of the glass fiber.
摘要翻译： 液晶聚酯组合物含有至少100重量份具有不同结构单元的液晶聚酯和10至100重量份玻璃纤维，其中玻璃纤维的重均纤维长度（Mw）为200-500μm ，纤维长度不小于1500μm的特定玻璃纤维的含量相对于玻璃纤维的总量为0.1〜5.0重量％。
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7.发明授权公开(公告)号：US08778222B2
公开(公告)日：2014-07-15
申请号：US13637742
申请日：2011-12-14
IPC分类号： C09K19/52 , C09K19/54 , C09K19/02 , C09K19/00 , C08F283/00 , C08G63/91 , C08L67/00 , B60C1/00 , C08K3/04
CPC分类号： C08J5/043 , B29C47/0021 , C08J2367/03 , C08K7/14 , Y10T428/10 , C08L67/03
摘要： A liquid crystalline polyester composition contains at least 100 parts by weight of liquid crystalline polyester and 10 to 100 parts by weight of glass fiber, wherein the glass fiber has a weight-average fiber length of 30 to 100 μm, and content of specific glass fiber having fiber length of 300 to 500 μm is 0.1 to 5 percent by weight to a total amount of the glass fiber.
摘要翻译： 液晶聚酯组合物含有至少100重量份液晶聚酯和10-100重量份玻璃纤维，其中玻璃纤维的重均纤维长度为30-100微米，特定玻璃纤维的含量 纤维长度为300〜500μm，相对于玻璃纤维的总量为0.1〜5重量％。
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8.发明申请LIQUID CRYSTALLINE POLYESTER COMPOSITION AND METAL COMPOSITE MOLDED PRODUCT USING THE SAME 有权液晶聚合物组合物和使用其的金属复合材料成型产品公开(公告)号：US20140022502A1
公开(公告)日：2014-01-23
申请号：US14009535
申请日：2011-12-14
IPC分类号： C08K3/34
CPC分类号： C08K3/34 , C08K3/346 , C08K7/14 , C09K19/3809 , C08L67/03
摘要： A liquid crystalline polyester composition contains 100 parts by weight of a liquid crystalline polyester (A) and 10 to 100 parts by weight of a mica (B), wherein a rate in number of mica with a ratio (d1/d2) of a long diameter (d1) to a short diameter (d2) that is greater than 2.0, to an entire content of the mica (B) contained in the liquid crystalline polyester composition is not higher than 20%.
摘要翻译： 液晶聚酯组合物包含100重量份的液晶聚酯（A）和10至100重量份的云母（B），其中云母数量的比率（d1 / d2）为长 对于液晶聚酯组合物中含有的云母（B）的全部含量，直径（d1）至大于2.0的短径（d2）不大于20％。
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9.发明授权公开(公告)号：US08440780B2
公开(公告)日：2013-05-14
申请号：US13617677
申请日：2012-09-14
CPC分类号： C08G63/605 , C08G63/78 , C09K19/3809
摘要： A wholly aromatic liquid crystalline polyester contains 2.0 to 15.0 mole percent of a hydroquinone-derived structural unit relative to a total amount of structural units. The wholly aromatic liquid crystalline polyester has sum of an amount (a) of terminal hydroxyl group and an amount (b) of terminal acetyl group in a range of 50 to 350 equivalents/(g·10−6), and has a ratio [(a)+(b)]/(c) of the sum of the amount (a) of terminal hydroxyl group and the amount (b) of terminal acetyl group to an amount (c) of terminal carboxyl group in a range of 1.05 to 2.00.
摘要翻译： 全芳族液晶聚酯相对于结构单元的总量含有2.0〜15.0摩尔％的氢醌衍生的结构单元。 全芳香族液晶聚酯具有末端羟基的量（a）和末端乙酰基的量（b）在50〜350当量/（g·10 -6）的范围内的总和， （a）末端羟基的量（a）和末端乙酰基的量（b）与末端羧基量（c）之和的总和的（a）+（b）] /（c） 至2.00。
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10.发明申请公开(公告)号：US20130015400A1
公开(公告)日：2013-01-17
申请号：US13637738
申请日：2011-12-14
摘要： A liquid crystalline polyester composition contains at least 100 parts by weight of liquid crystalline polyester having different structural units and 10 to 100 parts by weight of glass fiber, wherein the glass fiber has a weight-average fiber length (Mw) of 200 to 500 μm, and content of specific glass fiber having fiber length of not less than 1500 μm is 0.1 to 5.0 percent by weight to a total amount of the glass fiber.
摘要翻译： 液晶聚酯组合物含有至少100重量份具有不同结构单元的液晶聚酯和10至100重量份玻璃纤维，其中玻璃纤维的重均纤维长度（Mw）为200-500μm ，纤维长度不小于1500μm的特定玻璃纤维的含量相对于玻璃纤维的总量为0.1〜5.0重量％。
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