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    Imide nitrogen dibenzofurans polymers
    3.
    发明授权
    Imide nitrogen dibenzofurans polymers 失效
    酰亚胺氮二苯并呋喃聚合物

    公开(公告)号：US4138392A

    公开(公告)日：1979-02-06

    申请号：US798335

    申请日：1977-05-19

    申请人： Imre Puskas ,  Ellis K. Fields

    发明人： Imre Puskas ,  Ellis K. Fields

    IPC分类号： C07D307/91 ,  C07D491/14 ,  C07D493/14 ,  C08G73/10

    CPC分类号： C07D307/91 ,  C07D491/14 ,  C07D493/14 ,  C08G73/1085

    摘要： The present disclosure relates to a new composition of matter dibenzofuran-2,3,6,7,-tetracarboxylic acid dianhydride and polymers derived therefrom including polyamic acid or polyimide polymers formed from the reaction of the above dianhydride and a diamine. The claimed dianhydride finds use as an excellent cross-linking moiety. Condensation polymers derived from the dianhydride and diamines are useful in the production of films and fibers with good thermal stability.

    摘要翻译： 本公开涉及物质二苯并呋喃-2,3,6,7-四羧酸二酐和由其衍生的聚合物的新组合物，包括由上述二酐与二胺反应形成的聚酰胺酸或聚酰亚胺聚合物。 所要求的二酐可用作优异的交联部分。 衍生自二酐和二胺的缩合聚合物可用于制备具有良好热稳定性的薄膜和纤维。

    Alkenylation catalysts
    4.
    发明授权
    Alkenylation catalysts 失效
    烯化催化剂

    公开(公告)号：US4034052A

    公开(公告)日：1977-07-05

    申请号：US617368

    申请日：1975-09-29

    申请人： Imre Puskas

    发明人： Imre Puskas

    IPC分类号： C07C2/72 ,  C07C3/00

    CPC分类号： C07C2/72 ,  C07C2523/04 ,  C07C2531/02

    摘要： Unsaturated amines, primary and secondary saturated amines, N,N,N',N'-tetramethylethylenediamine, N,N,N',N'-tetramethyl-1,3-propanediamine, and ammonia cocatalysis with alkali metals for alkenylation of alkylaromatics having benzylic hydrogen with conjugated diolefins of 4-15 carbon atoms. Improved trans:cis product ratio and improved yield are produced by these nitrogen containing cocatalysts.

    摘要翻译： 不饱和胺，伯和仲饱和胺，N，N，N'，N'-四甲基乙二胺，N，N，N'，N'-四甲基-1,3-丙二胺和与碱金属进行氨共催化用于烷基芳族化合物的烯基化反应 具有4-15个碳原子的共轭二烯烃的苄基氢。 通过这些含氮助催化剂产生改进的反式：顺式产物比例和提高的产率。

    Tar reduction by inorganic halide for reaction of unsaturated anhydride and polybutene
    5.
    发明授权
    Tar reduction by inorganic halide for reaction of unsaturated anhydride and polybutene 失效
    用不饱和酸酐和聚丁烯反应的无机卤化物焦油还原

    公开(公告)号：US3935249A

    公开(公告)日：1976-01-27

    申请号：US358914

    申请日：1973-05-10

    申请人： Imre Puskas ,  John A. Cengel

    发明人： Imre Puskas ,  John A. Cengel

    IPC分类号： C07C51/567 ,  C08F8/46 ,  C07D307/60

    CPC分类号： C07C51/567 ,  C08F8/46

    摘要： Viscous polybutenes of number average molecular weight (M.sub.n) in the range of about 300 to about 3,000 have improved reactivity with intramolecular anhydrides of unsaturated aliphatic dicarboxylic acids when reacted in the presence of rather small amounts, i.e., 5 to 200 ppm, of inorganic halogen preferably chlorine and/or bromine containing compounds. Use of such halogen containing compounds in the addition reaction of polybutene with said unsaturated anhydrides can reduce formation of undesired tarry product resulting from polymerization and/or thermal decomposition of the unsaturated anhydrides.

    摘要翻译： 数均分子量（Mn）在约300至约3,000范围内的粘性聚丁烯在非常少量（即5至200ppm）的无机卤素的存在下反应时具有改善的不饱和脂族二羧酸的分子内酸酐的反应性 优选含氯和/或溴的化合物。 在聚丁烯与所述不饱和酸酐的加成反应中使用这种含卤素化合物可以减少由不饱和酸酐的聚合和/或热分解产生的不期望的焦油产物的形成。

    Method for manufacture of AMS-1B crystalline borosilicate molecular sieve with low sodium content
    6.
    发明授权
    Method for manufacture of AMS-1B crystalline borosilicate molecular sieve with low sodium content 失效
    低钠含量的AMS-1B结晶硼硅酸分子筛的制备方法

    公开(公告)号：US4514516A

    公开(公告)日：1985-04-30

    申请号：US528847

    申请日：1983-09-02

    申请人： Imre Puskas

    发明人： Imre Puskas

    IPC分类号： B01J29/86 ,  C01B35/10

    CPC分类号： B01J29/86 ,  C01B35/1009

    摘要： AMS-1B crystalline borosilicate molecular sieve is prepared by reacting under crystallization conditions an aqueous mixture containing sources for an oxide of silicon, an oxide of boron, a cation and a lower alkyl primary or secondary amine.

    摘要翻译： 通过在结晶条件下使含有硅氧化物，硼氧化物，阳离子和低级烷基伯胺或仲胺的含水混合物反应制备AMS-1B结晶硼硅酸盐分子筛。

    Process for manufacturing polyalkenyl succinic anhydrides
    9.
    发明授权
    Process for manufacturing polyalkenyl succinic anhydrides 失效
    制备聚链烯基琥珀酸酐的方法

    公开(公告)号：US4086251A

    公开(公告)日：1978-04-25

    申请号：US673707

    申请日：1976-04-05

    申请人： John A. Cengel ,  Imre Puskas

    发明人： John A. Cengel ,  Imre Puskas

    IPC分类号： C07C51/567 ,  C07C57/13 ,  C08F8/46 ,  C07D307/60

    CPC分类号： C07C51/567 ,  C07C57/13 ,  C08F8/46

    摘要： A process for producing alkenyl substituted anhydrides which comprises introducing one mole of polypropene or polybutene having a number average molecular weight of 200-3000, 0.8-5.0 moles of the anhydride of an unsaturated dicarboxylic acid and 5-200 ppm of an additive which suppresses the formation of tarry materials and undesirable reaction side products and/or improves yield, into a reaction zone, reacting said materials at a temperature from about 150.degree. C to about 300.degree. C to form the alkenyl anhydride, distilling off and condensing the unreacted anhydride from the reaction mixture, recovering the alkenyl substituted anhydride, and returning at least a portion of the recovered unreacted anhydride to a reaction zone for reaction with an alkenyl material.

    摘要翻译： 一种制备链烯基取代酐的方法，其包括将1摩尔数均分子量为200-3000的聚丙烯或聚丁烯，0.8-5.0摩尔不饱和二羧酸酐和5-200ppm的添加剂， 将焦油物质和不良反应副产物的形成和/或提高产率转化为反应区，使所述物质在约150℃至约300℃的温度下反应以形成烯基酸酐，蒸馏除去并将未反应的酸酐从 反应混合物，回收链烯基取代的酐，并将至少一部分回收的未反应的酸酐返回到反应区以与烯基材料反应。

    Process for the manufacture of 1,4-bis[2-(4'-carbomethoxystyrenyl)] benzene
    10.
    发明授权
    Process for the manufacture of 1,4-bis[2-(4'-carbomethoxystyrenyl)] benzene 失效
    制备1,4-双[2-（4'-甲磺酰基）]苯的方法

    公开(公告)号：US4537985A

    公开(公告)日：1985-08-27

    申请号：US514681

    申请日：1983-07-18

    申请人： Imre Puskas ,  Marshall Schmitt

    发明人： Imre Puskas ,  Marshall Schmitt

    IPC分类号： C07C67/00 ,  C07D217/04 ,  C07F9/54

    CPC分类号： C07D217/04 ,  C07C67/00 ,  C07F9/54

    摘要： A process for the manufacture of 1,4-bis[2-(4'-carbomethoxystyrenyl)] benzene is disclosed. This process comprises reacting, at a temperature of about 0.degree. C. to about 100.degree. C., in a highly polar anhydrous organic solvent or solvent mixture, or in liquid ammonia, a p-xylylene-bis-(trialkylphosphonium halide) or p-xylylene-bis-(triarylphosphonium halide) with 4-carbomethoxybenzaldehyde, initiated by the slow introduction of an organometallic compound or an inorganic base. Polyesters, such as polyethylene terephthalate, are copolymerized with about 5 to about 20 parts per million of 1,4-bis[2-(4'-carbomethoxystyrenyl)] benzene. 1,4-bis[2-(4'-carbomethoxystyrenyl)] benzene is useful to provide permanent whiteness to polyesters and polyamides and other synthetic or natural polymers. Polyesters are useful for the manufacture of fibers, films, and related industrial products.

    摘要翻译： 公开了制备1,4-双[2-（4'-甲磺酰基）]苯的方法。 该方法包括在约0℃至约100℃的温度下，在高极性无水有机溶剂或溶剂混合物中或在液氨中，将对二甲苯基 - 双 - （三烷基卤化鏻）或p （三芳基鏻卤化物）与4-甲酯基苯甲醛反应，由缓慢引入有机金属化合物或无机碱引发。 诸如聚对苯二甲酸乙二醇酯的聚酯与每百万份1,4-双[2-（4'-甲磺酰基甲苯基）]苯约5至约20份共聚。 1,4-双[2-（4'-甲酯基甲苯基）]苯可用于为聚酯和聚酰胺以及其它合成或天然聚合物提供永久白度。 聚酯可用于制造纤维，薄膜和相关工业产品。