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    Process for preparing pure cyclododecanone
    1.
    发明授权
    Process for preparing pure cyclododecanone 有权
    制备纯环十二酮的方法

    公开(公告)号：US08188320B2

    公开(公告)日：2012-05-29

    申请号：US12694815

    申请日：2010-01-27

    申请人： Joaquim Henrique Teles ,  Beatrice Röβler-Feigel ,  Alexander Hauk ,  Anton Meier ,  Christian Müller ,  Michael Schelper ,  Tanja Kirchner ,  Susanne Szeschkus ,  Rolf Pinkos ,  Gerd-Dieter Tebben

    发明人： Joaquim Henrique Teles ,  Beatrice Röβler-Feigel ,  Alexander Hauk ,  Anton Meier ,  Christian Müller ,  Michael Schelper ,  Tanja Kirchner ,  Susanne Szeschkus ,  Rolf Pinkos ,  Gerd-Dieter Tebben

    IPC分类号： C07C45/27

    CPC分类号： C07C45/82 ,  C07C45/28 ,  C07C45/62 ,  C07C2601/20 ,  C07C49/607 ,  C07C49/413

    摘要： The present invention relates to a process for preparing at least one cyclic compound with Z cycles and 7 to 16 carbon atoms with a keto group, at least comprising the stages: (a1) oxidation of a composition (A), at least comprising one cyclic olefin with Z cycles and 7 to 16 carbon atoms and at least two C—C double bonds, by means of dinitrogen monoxide to give a composition (A1), (a2) separating off the at least one cyclic olefin with Z cycles and 7 to 16 carbon atoms with at least two C—C double bonds from the composition (A1) in order to obtain a composition (A2), and (b) distillative treatment of the composition (A2) from step (a2) in order to obtain a composition (B), comprising the at least one cyclic compound with Z cycles and 7 to 16 carbon atoms with a keto group and less than 1.0% by weight of the at least one compound with Z−1 cycles and 7 to 16 carbon atoms with at least one aldehyde group, where Z can be 1, 2, 3 or 4.

    摘要翻译： 本发明涉及一种制备具有Z环和至少具有7至16个碳原子的酮基的至少一种环状化合物的方法，至少包括以下步骤：（a1）组合物（A）的氧化，至少包含一个环状 烯烃，Z循环和7至16个碳原子和至少两个C-C双键，借助于一氧化二氮，得到组合物（A1），（a2）以Z循环分离至少一种环状烯烃， 16个碳原子与来自组合物（A1）的至少两个C-C双键，以获得组合物（A2），和（b）从步骤（a2）中的组合物（A2）的蒸馏处理，以获得 组合物（B），其包含至少一种Z循环的环状化合物和具有酮基的7至16个碳原子和小于1.0重量％的至少一种具有Z-1循环和7至16个碳原子的化合物， 至少一个醛基，其中Z可以是1,2,3或4个。

    PROCESS FOR PREPARING PURE CYCLODODECANONE
    2.
    发明申请
    PROCESS FOR PREPARING PURE CYCLODODECANONE 有权
    制备纯环己酮的方法

    公开(公告)号：US20100191018A1

    公开(公告)日：2010-07-29

    申请号：US12694815

    申请日：2010-01-27

    申请人： Joaquim Henrique Teles ,  Beatrice Rößler-Feigel ,  Alexander Hauk ,  Anton Meier ,  Christian Müller ,  Michael Schelper ,  Tanja Kirchner ,  Susanne Szeschkus ,  Rolf Pinkos ,  Gerd-Dieter Tebben

    发明人： Joaquim Henrique Teles ,  Beatrice Rößler-Feigel ,  Alexander Hauk ,  Anton Meier ,  Christian Müller ,  Michael Schelper ,  Tanja Kirchner ,  Susanne Szeschkus ,  Rolf Pinkos ,  Gerd-Dieter Tebben

    IPC分类号： C07C45/27

    CPC分类号： C07C45/82 ,  C07C45/28 ,  C07C45/62 ,  C07C2601/20 ,  C07C49/607 ,  C07C49/413

    摘要： The present invention relates to a process for preparing at least one cyclic compound with Z cycles and 7 to 16 carbon atoms with a keto group, at least comprising the stages: (a1) oxidation of a composition (A), at least comprising one cyclic olefin with Z cycles and 7 to 16 carbon atoms and at least two C—C double bonds, by means of dinitrogen monoxide to give a composition (A1), (a2) separating off the at least one cyclic olefin with Z cycles and 7 to 16 carbon atoms with at least two C—C double bonds from the composition (A1) in order to obtain a composition (A2), and (b) distillative treatment of the composition (A2) from step (a2) in order to obtain a composition (B), comprising the at least one cyclic compound with Z cycles and 7 to 16 carbon atoms with a keto group and less than 1.0% by weight of the at least one compound with Z−1 cycles and 7 to 16 carbon atoms with at least one aldehyde group, where Z can be 1, 2, 3 or 4.

    摘要翻译： 本发明涉及一种制备具有Z环和至少具有7至16个碳原子的酮基的至少一种环状化合物的方法，至少包括以下步骤：（a1）组合物（A）的氧化，至少包含一个环状 烯烃，Z循环和7至16个碳原子和至少两个C-C双键，借助于一氧化二氮，得到组合物（A1），（a2）以Z循环分离至少一种环状烯烃， 16个碳原子与来自组合物（A1）的至少两个C-C双键，以获得组合物（A2），和（b）从步骤（a2）中的组合物（A2）的蒸馏处理，以获得 组合物（B），其包含至少一种Z循环的环状化合物和具有酮基的7至16个碳原子和小于1.0重量％的至少一种具有Z-1循环和7至16个碳原子的化合物， 至少一个醛基，其中Z可以是1,2,3或4个。

    Process for the isolation of dodecatrienal and its use as aroma substance
    3.
    发明授权
    Process for the isolation of dodecatrienal and its use as aroma substance 有权
    分离十二碳三烯的方法及其作为芳香物质的用途

    公开(公告)号：US08212082B2

    公开(公告)日：2012-07-03

    申请号：US12694851

    申请日：2010-01-27

    申请人： Joaquim Henrique Teles ,  Beatrice Röβler-Feigel ,  Alexander Hauk ,  Christian Müller ,  Michael Schelper ,  Tanja Kirchner ,  Susanne Szeschkus

    发明人： Joaquim Henrique Teles ,  Beatrice Röβler-Feigel ,  Alexander Hauk ,  Christian Müller ,  Michael Schelper ,  Tanja Kirchner ,  Susanne Szeschkus

    IPC分类号： C07C45/28 ,  A61K8/35 ,  A61K47/08 ,  C11D3/50

    CPC分类号： C11B9/0015 ,  C07C45/28 ,  C07C45/62 ,  C07C45/82 ,  Y02P20/582 ,  C07C47/21 ,  C07C47/02

    摘要： The present invention relates to a process for preparing at least one compound with Z−1 cycles and 7 to 16 carbon atoms with at least one aldehyde group, at least comprising the stages: (a1) oxidation of a composition (A), at least comprising a cyclic olefin with Z cycles and 7 to 16 carbon atoms and at least two C—C double bonds, by means of dinitrogen monoxide to give a composition (A1), (a2) separating off the at least one cyclic olefin with Z cycles and 7 to 16 carbon atoms with at least two C—C double bonds from the composition (A1) from stage (a1) in order to obtain a composition (A2), (b1) separating off the at least one cyclic compound with Z cycles and 7 to 16 carbon atoms with a keto group from the composition (A2) from step (a2), in order to obtain a composition (B1), comprising at least 50% by weight of the at least one compound with Z−1 cycles and 7 to 16 carbon atoms with at least one aldehyde group and at least two C—C double bonds, where Z may be 1, 2, 3 or 4.

    摘要翻译： 本发明涉及至少一种具有Z-1个循环和7-16个碳原子的化合物与至少一个醛基的制备方法，至少包括以下步骤：（a1）组合物（A）的氧化，至少 包含具有Z循环和7至16个碳原子的环烯烃以及至少两个C-C双键的方法，借助于一氧化二氮，得到组合物（A1），（a2）以Z循环分离出至少一种环状烯烃 和从碳（a1）组合物（A1）至少具有两个C-C双键的碳原子数为7〜16的碳原子，以获得组合物（A2），（b1）以Z循环分离出至少一种环状化合物 和具有来自步骤（a2）的组合物（A2）的酮基的7至16个碳原子，以获得组合物（B1），其包含至少50重量％的至少一种Z-1循环的化合物 和具有至少一个醛基和至少两个C-C双键的7至16个碳原子，其中Z可以是1,2,3或4。

    PROCESS FOR THE ISOLATION OF DODECATRIENAL AND ITS USE AS AROMA SUBSTANCE
    4.
    发明申请
    PROCESS FOR THE ISOLATION OF DODECATRIENAL AND ITS USE AS AROMA SUBSTANCE 有权
    分离多糖的方法及其作为芳香物质的使用

    公开(公告)号：US20100190869A1

    公开(公告)日：2010-07-29

    申请号：US12694851

    申请日：2010-01-27

    申请人： Joaquim Henrique Teles ,  Beatrice Rößler-Feigel ,  Alexander Hauk ,  Christian Müller ,  Michael Schelper ,  Tanja Kirchner ,  Susanne Szeschkus

    发明人： Joaquim Henrique Teles ,  Beatrice Rößler-Feigel ,  Alexander Hauk ,  Christian Müller ,  Michael Schelper ,  Tanja Kirchner ,  Susanne Szeschkus

    IPC分类号： A61K8/35 ,  C07C45/28 ,  C11D3/50 ,  A61K47/08 ,  A61Q13/00

    CPC分类号： C11B9/0015 ,  C07C45/28 ,  C07C45/62 ,  C07C45/82 ,  Y02P20/582 ,  C07C47/21 ,  C07C47/02

    摘要： The present invention relates to a process for preparing at least one compound with Z−1 cycles and 7 to 16 carbon atoms with at least one aldehyde group, at least comprising the stages: (a1) oxidation of a composition (A), at least comprising a cyclic olefin with Z cycles and 7 to 16 carbon atoms and at least two C—C double bonds, by means of dinitrogen monoxide to give a composition (A1), (a2) separating off the at least one cyclic olefin with Z cycles and 7 to 16 carbon atoms with at least two C—C double bonds from the composition (A1) from stage (a1) in order to obtain a composition (A2), (b1) separating off the at least one cyclic compound with Z cycles and 7 to 16 carbon atoms with a keto group from the composition (A2) from step (a2), in order to obtain a composition (B1), comprising at least 50% by weight of the at least one compound with Z−1 cycles and 7 to 16 carbon atoms with at least one aldehyde group and at least two C—C double bonds, where Z may be 1, 2, 3 or 4.

    摘要翻译： 本发明涉及至少一种具有Z-1个循环和7-16个碳原子的化合物与至少一个醛基的制备方法，至少包括以下步骤：（a1）组合物（A）的氧化，至少 包含具有Z循环和7至16个碳原子的环烯烃以及至少两个C-C双键的方法，通过一氧化二氮来得到组合物（A1），（a2）以Z循环分离出至少一种环状烯烃 和从碳（a1）组合物（A1）至少具有两个C-C双键的碳原子数为7〜16的碳原子，以获得组合物（A2），（b1）以Z循环分离出至少一种环状化合物 和具有来自步骤（a2）的组合物（A2）的酮基的7至16个碳原子，以获得组合物（B1），其包含至少50重量％的至少一种Z-1循环的化合物 和具有至少一个醛基和至少两个C-C双键的7至16个碳原子，其中Z可以是1,2,3或4。

    Method for purifying cyclic ketones
    8.
    发明授权
    Method for purifying cyclic ketones 有权
    环酮纯化方法

    公开(公告)号：US07714171B2

    公开(公告)日：2010-05-11

    申请号：US12306807

    申请日：2007-06-27

    申请人： Rolf Pinkos ,  Gerd Tebben ,  Alexander Hauk ,  Christian Müller ,  Harald Rust

    发明人： Rolf Pinkos ,  Gerd Tebben ,  Alexander Hauk ,  Christian Müller ,  Harald Rust

    IPC分类号： C07C45/27

    CPC分类号： C07C45/85 ,  C07C45/33 ,  C07C45/34 ,  C07C45/58 ,  C07C45/62 ,  C07C45/80 ,  C07C45/81 ,  C07C45/82 ,  C07C49/413 ,  C07C49/607

    摘要： The present invention relates to a process for purifying a composition (I) comprising at least one cyclic ketone having from 7 to 16 carbon atoms, which comprises thermal treatment of the composition (I) with at least one acid and further purification by means of a process selected from the group consisting of distillation, extraction and crystallization, Furthermore, the present invention relates to a process for preparing cyclododecanone, which comprises such a purification, and the use of at least one acid for purifying a composition (I) comprising at least one cyclic ketone having from 7 to 16 carbon atoms by thermal treatment of the composition (I) with the acid.

    摘要翻译： 本发明涉及一种纯化包含至少一种具有7至16个碳原子的环酮的组合物（I）的方法，其包括用至少一种酸对组合物（I）进行热处理，并进一步通过 选自蒸馏，萃取和结晶的方法。此外，本发明涉及一种制备环十二烷酮的方法，其包括这种纯化，以及使用至少一种酸来纯化至少包含（I）的组合物 一种具有7-16个碳原子的环酮，通过组合物（I）与酸的热处理。

    METHOD FOR PURIFYING CYCLIC KETONES
    9.
    发明申请
    METHOD FOR PURIFYING CYCLIC KETONES 有权
    纯化循环克隆的方法

    公开(公告)号：US20090326277A1

    公开(公告)日：2009-12-31

    申请号：US12306807

    申请日：2007-06-27

    申请人： Rolf Pinkos ,  Gerd Tebben ,  Alexander Hauk ,  Christian Müller ,  Harald Rust

    发明人： Rolf Pinkos ,  Gerd Tebben ,  Alexander Hauk ,  Christian Müller ,  Harald Rust

    IPC分类号： C07C45/00

    CPC分类号： C07C45/85 ,  C07C45/33 ,  C07C45/34 ,  C07C45/58 ,  C07C45/62 ,  C07C45/80 ,  C07C45/81 ,  C07C45/82 ,  C07C49/413 ,  C07C49/607

    摘要： The present invention relates to a process for purifying a composition (I) comprising at least one cyclic ketone having from 7 to 16 carbon atoms, which comprises thermal treatment of the composition (I) with at least one acid and further purification by means of a process selected from the group consisting of distillation, extraction and crystallization, Furthermore, the present invention relates to a process for preparing cyclododecanone, which comprises such a purification, and the use of at least one acid for purifying a composition (I) comprising at least one cyclic ketone having from 7 to 16 carbon atoms by thermal treatment of the composition (I) with the acid.

    摘要翻译： 本发明涉及一种纯化包含至少一种具有7至16个碳原子的环酮的组合物（I）的方法，其包括用至少一种酸对组合物（I）进行热处理，并进一步通过 选自蒸馏，萃取和结晶的方法。此外，本发明涉及一种制备环十二烷酮的方法，其包括这种纯化，以及使用至少一种酸来纯化至少包含（I）的组合物 一种具有7-16个碳原子的环酮，通过组合物（I）与酸的热处理。