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公开(公告)号：US4127644A
公开(公告)日：1978-11-28
申请号：US792445
申请日：1977-04-29
摘要： Hydrogen is produced from water by first reacting I.sub.2, SO.sub.2 and H.sub.2 O to make hydrogen iodide and sulfuric acid. A substantial molar excess of SO.sub.2 and I.sub.2 in the reaction zone creates a lighter sulfuric acid-bearing phase and a heavier polyiodic-acid-bearing phase. The heavier phase is separated, degassed and then contacted with phosphoric acid to permit distillation of HI of low water content and recovery of I.sub.2 as a separate fraction. Hydrogen is recovered from HI vapor, as by thermal decomposition.
摘要翻译： 通过首先使I2，SO2和H2O反应生成碘化氢和硫酸，从而产生氢。 在反应区域中相当大量的过量的SO 2和I 2产生较轻的含硫酸相和较重的含多碘酸的相。 将较重的相分离，脱气，然后与磷酸接触，以允许蒸馏低水含量的HI，并将I2作为分离馏分回收。 通过热分解从HI蒸气中回收氢。
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公开(公告)号：US5038046A
公开(公告)日：1991-08-06
申请号：US550468
申请日：1990-07-10
CPC分类号： G21G4/08 , A61K51/1282 , A61K2121/00
摘要： A method and generator for preparing the radioisotope of lead, .sup.212 Pb, whereby .sup.228 Th, in a closed chamber, is allowed to decay to gaseous .sup.220 Rn which is then readily separated from the thorium and other decay products by diffusing the .sup.220 Rn gas into a second chamber, where it decays to .sup.212 Pb which can then be collected from the second chamber. The .sup.228 Th preferably is amorphous, such as thorium stearate. Collection of .sup.212 Pb occurs in a medium of high and open porosity into which the .sup.220 Rn diffuses so that the decay products recoil into the medium. The .sup.212 Pb can be recovered from this medium by dissolving the medium or by reacting it with an antibody-chelating complex solution to entrap it in the antibody-chelating complex.
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公开(公告)号：US4150094A
公开(公告)日：1979-04-17
申请号：US865949
申请日：1977-12-30
申请人： Karol J. Mysels , John H. Norman
发明人： Karol J. Mysels , John H. Norman
摘要： A continuous reaction is carried out between gaseous SO.sub.2, I.sub.2 and liquid H.sub.2 O in a substantially vertical reaction zone. H.sub.2 O plus I.sub.2 in a substantial excess are supplied to an upper location at preselected rates. SO.sub.2 is injected into the zone at a lower location, and a desired temperature is maintained at an intermediate location where the reaction proceeds to produce sulfuric acid and hydrogen iodide. The reaction products are removed from a location near the bottom at a rate proportional to the preselected rates to cause a continuous downward flow within the reaction zone. The SO.sub.2 flow rate assures that substantially all of the SO.sub.2 either reacts or is absorbed by the downward traveling nongaseous reactants.
摘要翻译： 在基本上垂直的反应区中，在气态SO 2，I 2和液体H 2 O之间进行连续反应。 大量过量的H 2 O加上I2以预选速率供应到上部位置。 在较低的位置将SO 2注入该区域，并且在反应进行以产生硫酸和碘化氢的中间位置保持所需的温度。 反应产物以与预选速率成比例的速率从靠近底部的位置移除，以引起反应区内的连续向下流动。 SO 2流量确保基本上所有的SO 2都反应或被向下移动的非气态反应物吸收。
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公开(公告)号：US4855162A
公开(公告)日：1989-08-08
申请号：US74635
申请日：1987-07-17
IPC分类号： B01D67/00 , B01D71/36 , B01D71/68 , B05D7/02 , C08J3/03 , C08J7/04 , C08J9/42 , D06M13/02 , D06M13/188 , D06M15/256
CPC分类号： B01D67/0088 , B05D7/02 , C08J3/03 , C08J7/047 , C08J2327/18 , C08J2427/00
摘要： Adherent, PTFE coatings on polymer surfaces can be produced at temperatures well below the sintering temperature of PTFE, by contacting the surface with a dilute dispersion of PTFE particles and heating the surface to its softening point (in the vicinity of its glass transition temperature) to dry it and to cause the individual particles to become embedded in and surrounded by the polymer.
摘要翻译： 聚合物表面上的粘附的PTFE涂层可以在远低于PTFE的烧结温度的温度下生产，通过使PTFE表面与PTFE颗粒的稀释分散体接触并将表面加热到其软化点（在其玻璃化转变温度附近）至 干燥并使单个颗粒嵌入聚合物并被聚合物包围。
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公开(公告)号：US4073834A
公开(公告)日：1978-02-14
申请号：US555688
申请日：1975-03-05
申请人： Karol J. Mysels
发明人： Karol J. Mysels
CPC分类号： G21C21/02 , Y10S376/901
摘要： A nuclear fuel element is fabricated from a porous graphite block containing a plurality of open coolant passageways and a plurality of fuel chambers uniformly located therebetween. The fuel chambers are filled with nuclear fuel material and closed. The entire porous block is then impregnated with a liquid carbonizable impregnant which penetrates through the septa and into each of the fuel chambers, wherein it is cured and then carbonized in situ. The resulting carbon residue integrally binds the nuclear fuel material to the fuel chamber walls of the porous graphite block and provides excellent heat transfer from the fuel to the walls of the open passageways from which the heat is extracted by the coolant.
摘要翻译： 核燃料元件由含有多个开放冷却剂通道的多孔石墨块和均匀地位于其间的多个燃料室制成。 燃料室充满核燃料并关闭。 然后将整个多孔块浸渍在渗透通过隔片并进入每个燃料室的液体碳化浸渍剂中，其中其被固化，然后原位碳化。 所得碳残余物将核燃料材料整体地结合到多孔石墨块的燃料室壁上，并且提供从燃料到冷却剂从其中提取热量的开放通道的壁的良好热传递。
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公开(公告)号：US4040902A
公开(公告)日：1977-08-09
申请号：US564773
申请日：1975-04-03
申请人： Karol J. Mysels
发明人： Karol J. Mysels
CPC分类号： G21C19/205
摘要： A method for axially shuffling fuel elements in a nuclear reactor is disclosed wherein column vacancies are created in a manner to allow substantially lateral transfer of a selected number of fuel elements from another adjacent column to a vacated column, the remaining fuel elements of the partially transferred column are removed and discarded whereby to create a new column vacancy, fresh fuel elements are added to the transferred fuel elements to establish a full new column of fuel elements and continuing such shuffling throughout the entire active core of the reactor.
摘要翻译： 公开了一种用于在核反应堆中轴向改组燃料元件的方法，其中柱空位以使得选定数量的燃料元件从另一相邻塔基本上横向转移到空出的塔的方式产生，剩余的燃料元件被部分转移 柱被移除并丢弃，由此产生新的柱空位，将新鲜的燃料元素添加到转移的燃料元件中，以建立全新的燃料元素柱并且在反应器的整个活性核心上继续进行洗牌。
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7.发明授权Method of extracting iodine from liquid mixtures of iodine, water and hydrogen iodide 失效从碘，水和碘化氢的液体混合物中提取碘的方法
公开(公告)号：US4176169A
公开(公告)日：1979-11-27
申请号：US921435
申请日：1978-07-03
申请人： Karol J. Mysels
发明人： Karol J. Mysels
CPC分类号： C01B7/14
摘要： The components of a liquid mixture consisting essentially of HI, water and at least about 50 w/o iodine are separated in a countercurrent extraction zone by treating with phosphoric acid containing at least about 90 w/o H.sub.3 PO.sub.4. The bottom stream from the extraction zone is substantially completely molten iodine, and the overhead stream contains water, HI, H.sub.3 PO.sub.4 and a small fraction of the amount of original iodine.When the water and HI are present in near-azeotropic proportions, there is particular advantage in feeding the overhead stream to an extractive distillation zone wherein it is treated with additional concentrated phosphoric acid to create an anhydrous HI vapor stream and bottoms which contain at least about 85 w/o H.sub.3 PO.sub.4. Concentration of these bottoms provides phosphoric acid infeed for both the countercurrent extraction zone and for the extractive distillation zone.
摘要翻译： 基本上由HI，水和至少约50w / o碘组成的液体混合物的组分通过用含有至少约90w / oH 3 PO 4的磷酸处理在逆流提取区中分离。 来自提取区的底部流基本上是完全熔融的碘，并且塔顶馏出物流含有水，HI，H 3 PO 4和少量的原始碘。 当水和HI以近似共沸的比例存在时，将塔顶物流进料到萃取蒸馏区有特别的优点，其中用另外的浓磷酸处理以产生无水的HI蒸气流和含有至少约 85 w / o H3PO4。 这些底部的浓度为逆流萃取区和萃取蒸馏区提供磷酸进料。
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公开(公告)号：US4432875A
公开(公告)日：1984-02-21
申请号：US268403
申请日：1981-05-29
CPC分类号： B01D67/0088 , B01D67/0093
摘要： Semi-permeable, porous membranes useful as filtration and reverse osmosis membranes can have or can consist of a porous layer of a hydrophobic polymer rendered hydrophilic at its surface by the presence of a surfactant containing both hydrophobic and hydrophilic groups, the surfactant being bonded to the polymer. Such a membrane may be made by quenching a previously made dry membrane in a solution of the surfactant and then banking the membrane. Such a membrane may also be made by contacting a membrane manufactured by quenching a dope of the hydrophobic polymer with such a solution of the surfactant prior to the membrance being dried after being formed by quenching. Such a membrane can also be made by forming a dope of the hydrophobic polymer and the surfactant and then quenching the dope to form the membrane, this quenching serving to contact the membrane with the surfactant as it is being formed.
摘要翻译： 可用作过滤和反渗透膜的半透性多孔膜可以具有或可以由疏水性聚合物的多孔层组成，所述疏水性聚合物通过存在包含疏水基和亲水基团的表面活性剂在表面具有亲水性，所述表面活性剂结合到 聚合物。 这样的膜可以通过将先前制成的干膜在表面活性剂的溶液中淬灭并然后使膜沉积来制备。 这样的膜也可以通过在通过骤冷形成膜之前将通过猝灭疏水性聚合物的掺杂物的膜与这种表面活性剂的溶液接触而制成。 这样的膜也可以通过形成疏水性聚合物和表面活性剂的掺杂物，然后淬灭涂料以形成膜，这种淬火用于在形成膜时与表面活性剂接触。
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公开(公告)号：US4164382A
公开(公告)日：1979-08-14
申请号：US819363
申请日：1977-07-27
申请人： Karol J. Mysels
发明人： Karol J. Mysels
CPC分类号： F03D3/04 , Y02E10/74 , Y10S415/907
摘要： A wind driven power apparatus for converting wind to mechanical energy is disclosed which includes a fixed axis turbine supported centrally of a fixed air guide defining a plurality of horizontal air passages disposed circumferentially of the turbine and each being adapted to receive an air stream therein coming from a limited range of wind directions and effect accelerated air flow toward the turbine. In one embodiment, an air guide block is disposed circumferentially of the turbine and is rotatable about the axis of the turbine to direct accelerated air flow to the turbine from the windwardly facing ones of the air passages, while in alternative embodiments means are provided for selectively closing off the air passages so that accelerated air flow from selected air passages is directed to the turbine.
摘要翻译： 公开了一种用于将风转换成机械能的风力发电设备，其包括固定轴承涡轮机，其被固定在空气导向器的中心，所述固定轴承涡轮限定了沿涡轮机周向布置的多个水平空气通道，并且每个空气通道适于接纳来自 有限的风向范围和影响加速气流向涡轮。 在一个实施例中，空气引导块设置在涡轮机的周向并且可绕涡轮机的轴线旋转，以将加速的空气流从风向面对的空气通道引导到涡轮机，而在替代实施例中， 关闭空气通道，使得来自选定的空气通道的加速气流被引导到涡轮。
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公开(公告)号：US4413074A
公开(公告)日：1983-11-01
申请号：US342068
申请日：1982-01-25
IPC分类号： B01D67/00 , C08J7/04 , C08L1/28 , B05D5/00 , C08F253/00
CPC分类号： B01D67/0088 , B01D67/0093 , C08J7/047 , B01D2323/30 , C08J2401/00
摘要： A hydrophilic surface can be provided on a hydrophobic polymer surface by contacting the hydrophobic surface with a solution of a hydroxyalkyl cellulose and a perfluorocarbon surfactant in water or a mixture of water and one or more aliphatic alcohols so as to form a layer of the solution on the hydrophobic surface and then heating the surface coated with the layer so as to remove the solvent, so as to form a bond between the cellulose and the hydrophobic surface. This results in the formation of a hydrophilic surface coating a layer on the hydrophobic surface. Hydrophilic surfaces as are created in this manner are primarily intended to be utilized on polysulfone surfaces in semipermeable membranes such as are utilized in micro- and ultra-filtration.
摘要翻译： 通过使疏水表面与羟烷基纤维素和全氟化碳表面活性剂在水中或水与一种或多种脂族醇的混合物中的溶液接触，可以在疏水性聚合物表面上提供亲水表面，以形成溶液层 疏水表面，然后加热涂覆有该层的表面以除去溶剂，以便在纤维素和疏水性表面之间形成结合。 这导致在疏水性表面上形成涂覆一层的亲水性表面。 以这种方式产生的亲水性表面主要用于半透膜中的聚砜表面，例如用于微量和超滤。
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