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1.发明授权Intact method of evaluating unit cells in a fuel cell stack and a device using the same 有权评价燃料电池堆中的单体电池的完整方法和使用其的装置公开(公告)号：US09496573B2
公开(公告)日：2016-11-15
申请号：US13353443
申请日：2012-01-19
申请人： Jong Hyun Jang , Kug-Seung Lee , Hyoung-Juhn Kim , Eun Ae Cho , Soo-Kil Kim , Dirk Henkensmeier , Suk-Woo Nam , Tae Hoon Lim
发明人： Jong Hyun Jang , Kug-Seung Lee , Hyoung-Juhn Kim , Eun Ae Cho , Soo-Kil Kim , Dirk Henkensmeier , Suk-Woo Nam , Tae Hoon Lim
IPC分类号： H01M8/04828 , H01M8/04
CPC分类号： H01M8/0491 , H01M8/04552 , Y02E60/50
摘要： Disclosed are a method and an apparatus for an intact evaluation of the unit cells in a fuel cell stack. Since the degradation of the unit cells can be detected intactly, i.e. without disassembly of the stack, the time required for the detection and analysis thereof can be greatly reduced.
摘要翻译： 公开了一种用于完整评估燃料电池堆中的单元电池的方法和装置。 由于能够完整地检测单元电池的劣化，即不进行堆叠的拆卸，所以能够大幅降低检测和分析所需的时间。
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2.发明授权Branched multiblock polybenzimidazole-benzamide copolymer and method for preparing the same, electrolyte membrane and paste/gel prepared therefrom 有权支化多嵌段聚苯并咪唑 - 苯甲酰胺共聚物及其制备方法，由其制备的电解质膜和糊剂/凝胶公开(公告)号：US07632591B2
公开(公告)日：2009-12-15
申请号：US11593471
申请日：2006-11-07
申请人： Jung-hye Won , Yong-su Park , Chong-kyu Shin , Jae-hyuk Chang , Bong-keun Lee , Dirk Henkensmeier
发明人： Jung-hye Won , Yong-su Park , Chong-kyu Shin , Jae-hyuk Chang , Bong-keun Lee , Dirk Henkensmeier
IPC分类号： H01M8/10
CPC分类号： C08G73/18 , B01D71/56 , B01D71/62 , B01D71/80 , B01D71/82 , C08G73/22 , C08J5/2256 , C08J2365/02 , C08J2379/04 , C08J2379/06 , C08J2387/00 , H01M8/103 , H01M8/1048
摘要： A branched multiblock polybenzimidazole-benzamide copolymer, specifically, one consisting of a repeating unit represented by Formula 1, and a method for preparing the same; an electrolyte membrane using the branched multiblock copolymer, a consistent electrolyte paste/gel and a method for preparing the same; a membrane-electrode assembly (MEA) using the electrolyte membrane and the consistent electrolyte paste/gel and a method for preparing the same; and a fuel cell prepared from the membrane-electrode assembly. The electrolyte membrane according to the present invention has high hydrogen ion conductivity over a wide temperature range, and excellent physical properties such as mechanical properties, chemical resistance and thermal stability. Deterioration of the membrane properties is effectively controlled by phosphoric acid doping and high hydrogen ion conductivity is realized even with a low phosphoric acid doping level. This consistent electrolyte paste/gel may be useful in improving the operating performance of a fuel cell by coating the electrolyte uniformly.
摘要翻译： 支链多嵌段聚苯并咪唑 - 苯甲酰胺共聚物及其制备方法，特别是由式1表示的重复单元构成的共聚物。 使用支链多嵌段共聚物的电解质膜，一致的电解质糊剂/凝胶及其制备方法; 使用电解质膜和一致的电解质糊剂/凝胶的膜 - 电极组件（MEA）及其制备方法; 以及由所述膜 - 电极组件制备的燃料电池。 根据本发明的电解质膜在宽的温度范围内具有高的氢离子传导性，并且具有优异的物理性能如机械性能，耐化学性和热稳定性。 通过磷酸掺杂有效地控制膜性能的劣化，即使在低磷酸掺杂水平下也实现了高的氢离子传导性。 这种一致的电解质糊剂/凝胶可以通过均匀地涂覆电解质来改善燃料电池的操作性能。
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3.发明申请METHOD FOR PREPARING AN ENHANCED PROTON EXCHANGE MEMBRANE AND ENHANCED PROTON EXCHANGE MEMBRANE 有权制备增强型原子交换膜和增强型原子交换膜的方法公开(公告)号：US20110294035A1
公开(公告)日：2011-12-01
申请号：US13147060
申请日：2010-02-01
CPC分类号： C08J5/2243 , C08J2325/08 , C08J2333/20 , H01M8/0289 , H01M8/1023 , H01M8/1039 , H01M8/1044 , H01M8/1088 , Y02E60/521 , Y02P70/56
摘要： A novel approach based on the increase of the intrinsic oxidative stability of uncrosslinked membranes is addressed. The co-grafting of styrene with methacrylonitrile (MAN), which possesses a protected α-position and strong dipolar pendant nitrile group, onto 25 μm ETFE base film is disclosed. Styrene/MAN co-grafted membranes were compared to styrene based membrane in durability tests in single H2/O2 fuel cells. The incorporation of MAN improves the chemical stability dramatically. The membrane preparation based on the copolymerization of styrene and MAN shows encouraging results and offers the opportunity of tuning the MAN and crosslinker content to enhance the oxidative stability of the resulting fuel cell membranes.
摘要翻译： 解决了基于未交联膜的固有氧化稳定性增加的新方法。 公开了将苯乙烯与具有保护的α位和强偶极侧基腈基的甲基丙烯腈（MAN）共同接枝到25μmETFE基膜上。 在单个H 2 / O 2燃料电池的耐久性试验中，将苯乙烯/ MAN共接枝膜与苯乙烯基膜进行比较。 MAN的并入显着提高了化学稳定性。 基于苯乙烯和MAN的共聚合膜制备显示出令人鼓舞的结果，并提供调谐MAN和交联剂含量以提高所得燃料电池膜的氧化稳定性的机会。
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公开(公告)号：US08372894B2
公开(公告)日：2013-02-12
申请号：US13119068
申请日：2009-02-23
申请人： Dirk Henkensmeier
发明人： Dirk Henkensmeier
CPC分类号： C08F259/08 , C08F255/00 , C08F255/02 , C08F291/00 , C08L51/003 , C08L51/06 , C08L2666/02
摘要： A method for producing a graft polymer comprises the steps of: a) irradiating a base polymer with an electron beam or a source of γ-radiation, b) contacting a grafting solution with the base polymer, wherein the grafting solution contains at least one oxygen scavenger and at least one graft monomer selected from the group consisting of styrene and styrene derivatives, and c) graft polymerizing the mixture of the base polymer and the grafting solution obtained in step b).
摘要翻译： 制备接枝聚合物的方法包括以下步骤：a）用电子束或γ-辐射源照射基础聚合物，b）使接枝溶液与基础聚合物接触，其中接枝溶液含有至少一种氧 清除剂和至少一种选自苯乙烯和苯乙烯衍生物的接枝单体，和c）将步骤b）中获得的基础聚合物和接枝溶液的混合物接枝聚合。
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5.发明授权Method for preparing an enhanced proton exchange membrane and enhanced proton exchange membrane 有权制备增强质子交换膜和增强质子交换膜的方法公开(公告)号：US08951694B2
公开(公告)日：2015-02-10
申请号：US13147060
申请日：2010-02-01
CPC分类号： C08J5/2243 , C08J2325/08 , C08J2333/20 , H01M8/0289 , H01M8/1023 , H01M8/1039 , H01M8/1044 , H01M8/1088 , Y02E60/521 , Y02P70/56
摘要： A novel approach based on the increase of the intrinsic oxidative stability of uncrosslinked membranes is addressed. The co-grafting of styrene with methacrylonitrile (MAN), which possesses a protected α-position and strong dipolar pendant nitrile group, onto 25 μm ETFE base film is disclosed. Styrene/MAN co-grafted membranes were compared to styrene based membrane in durability tests in single H2/O2 fuel cells. The incorporation of MAN improves the chemical stability dramatically. The membrane preparation based on the copolymerization of styrene and MAN shows encouraging results and offers the opportunity of tuning the MAN and crosslinker content to enhance the oxidative stability of the resulting fuel cell membranes.
摘要翻译： 解决了基于未交联膜的固有氧化稳定性增加的新方法。 公开了将苯乙烯与具有保护的α位和强偶极侧基腈基的甲基丙烯腈（MAN）共同接枝到25μmETFE基膜上。 在单个H 2 / O 2燃料电池的耐久性试验中，将苯乙烯/ MAN共接枝膜与苯乙烯基膜进行比较。 MAN的并入显着提高了化学稳定性。 基于苯乙烯和MAN的共聚合膜制备显示出令人鼓舞的结果，并提供调谐MAN和交联剂含量以提高所得燃料电池膜的氧化稳定性的机会。
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公开(公告)号：US20110245365A1
公开(公告)日：2011-10-06
申请号：US13119068
申请日：2009-02-23
申请人： Dirk Henkensmeier
发明人： Dirk Henkensmeier
CPC分类号： C08F259/08 , C08F255/00 , C08F255/02 , C08F291/00 , C08L51/003 , C08L51/06 , C08L2666/02
摘要： A method for producing a graft polymer comprises the steps of: a) irradiating a base polymer with an electron beam or a source of γ-radiation, b) contacting a grafting solution with the base polymer, wherein the grafting solution contains at least one oxygen scavenger and at least one graft monomer selected from the group consisting of styrene and styrene derivatives, and c) graft polymerizing the mixture of the base polymer and the grafting solution obtained in step b).
摘要翻译： 制备接枝聚合物的方法包括以下步骤：a）用电子束或γ-辐射源照射基础聚合物，b）使接枝溶液与基础聚合物接触，其中接枝溶液含有至少一种氧 清除剂和至少一种选自苯乙烯和苯乙烯衍生物的接枝单体，和c）将步骤b）中获得的基础聚合物和接枝溶液的混合物接枝聚合。
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7.发明申请Branched multiblock polybenzimidazole-benzamide copolymer and method for preparing the same, electrolyte membrane and paste/gel prepared therefrom 有权支化多嵌段聚苯并咪唑 - 苯甲酰胺共聚物及其制备方法，由其制备的电解质膜和糊剂/凝胶公开(公告)号：US20070111075A1
公开(公告)日：2007-05-17
申请号：US11593471
申请日：2006-11-07
申请人： Jung-hye Won , Yong-su Park , Chong-kyu Shin , Jae-hyuk Chang , Bong-keun Lee , Dirk Henkensmeier
发明人： Jung-hye Won , Yong-su Park , Chong-kyu Shin , Jae-hyuk Chang , Bong-keun Lee , Dirk Henkensmeier
CPC分类号： C08G73/18 , B01D71/56 , B01D71/62 , B01D71/80 , B01D71/82 , C08G73/22 , C08J5/2256 , C08J2365/02 , C08J2379/04 , C08J2379/06 , C08J2387/00 , H01M8/103 , H01M8/1048
摘要： A branched multiblock polybenzimidazole-benzamide copolymer, specifically, one consisting of a repeating unit represented by Formula 1, and a method for preparing the same; an electrolyte membrane using the branched multiblock copolymer, a consistent electrolyte paste/gel and a method for preparing the same; a membrane-electrode assembly (MEA) using the electrolyte membrane and the consistent electrolyte paste/gel and a method for preparing the same; and a fuel cell prepared from the membrane-electrode assembly. The electrolyte membrane according to the present invention has high hydrogen ion conductivity over a wide temperature range, and excellent physical properties such as mechanical properties, chemical resistance and thermal stability. Deterioration of the membrane properties is effectively controlled by phosphoric acid doping and high hydrogen ion conductivity is realized even with a low phosphoric acid doping level. This consistent electrolyte paste/gel may be useful in improving the operating performance of a fuel cell by coating the electrolyte uniformly.
摘要翻译： 支链多嵌段聚苯并咪唑 - 苯甲酰胺共聚物及其制备方法，特别是由式1表示的重复单元构成的共聚物。 使用支链多嵌段共聚物的电解质膜，一致的电解质糊剂/凝胶及其制备方法; 使用电解质膜和一致的电解质糊剂/凝胶的膜 - 电极组件（MEA）及其制备方法; 以及由所述膜 - 电极组件制备的燃料电池。 根据本发明的电解质膜在宽的温度范围内具有高的氢离子传导性，并且具有优异的物理性能如机械性能，耐化学性和热稳定性。 通过磷酸掺杂有效地控制膜性能的劣化，即使在低磷酸掺杂水平下也实现了高的氢离子传导性。 这种一致的电解质糊剂/凝胶可以通过均匀地涂覆电解质来改善燃料电池的操作性能。
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