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公开(公告)号：US6114499A
公开(公告)日：2000-09-05
申请号：US295218
申请日：1999-04-21
申请人： Peter M. Kazmaier , Karen A. Moffat , Marko D. Saban , Richard P. N. Veregin , Michael K. Georges , Gordon K. Hamer , Toyofumi Inoue , Stephan V. Drappel
发明人： Peter M. Kazmaier , Karen A. Moffat , Marko D. Saban , Richard P. N. Veregin , Michael K. Georges , Gordon K. Hamer , Toyofumi Inoue , Stephan V. Drappel
IPC分类号： C08F2/00 , C08F257/02 , C08F265/04 , C08F279/00 , C08F279/02 , C08F283/01 , C08F287/00 , C08F291/00 , C08F293/00 , C08G83/00 , C08L51/00 , G03G9/087 , G03G9/13 , C08J3/20
CPC分类号： C08G83/003 , C08F257/02 , C08F265/04 , C08F279/00 , C08F279/02 , C08F283/01 , C08F287/00 , C08F291/00 , C08F293/005 , C08L51/003 , G03G9/08791 , G03G9/133 , Y10S430/166
摘要： A process for the preparation of branched thermoplastic resins comprising: heating a mixture of an unsaturated resin, a free radical initiator, and a stable free radical agent; adding to the heated mixture at least on polymerizable monomer; and cooling the mixture, wherein the resulting product is a branched thermoplastic resin with arms or branches comprised of polymerized monomer with substantially uniform length and narrow polydispersity.
摘要翻译： 一种制备支化热塑性树脂的方法，包括：加热不饱和树脂，自由基引发剂和稳定的自由基剂的混合物; 至少在可聚合单体上加热至加热的混合物; 并冷却混合物，其中所得产物是具有臂或分枝的支链热塑性树脂，其具有基本上均匀的长度和窄的多分散性的聚合单体。
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2.发明授权Stable free radical polymerization process and thermoplastic materials produced therefrom 失效稳定的自由基聚合方法和由其制备的热塑性材料
公开(公告)号：US5449724A
公开(公告)日：1995-09-12
申请号：US358561
申请日：1994-12-14
申请人： Karen A. Moffat , Marko D. Saban , Richard P. N. Veregin , Michael K. Georges , Gordon K. Hamer , Peter M. Kazmaier
发明人： Karen A. Moffat , Marko D. Saban , Richard P. N. Veregin , Michael K. Georges , Gordon K. Hamer , Peter M. Kazmaier
CPC分类号： C08F10/02
摘要： A free radical polymerization process for the preparation of a thermoplastic resin includes heating a mixture comprised of a free radical initiator, a stable free radical agent, and ethylene at a temperature of from about 40.degree. C. to about 500.degree. C. and at a pressure of from about 500 to about 5,000 bar to form a thermoplastic resin. The thermoplastic resin has a molecular weight distribution of from about 1.0 to about 2.0.
摘要翻译： 用于制备热塑性树脂的自由基聚合方法包括在约40℃至约500℃的温度下加热由自由基引发剂，稳定的自由基试剂和乙烯组成的混合物， 压力为约500至约5,000巴，以形成热塑性树脂。 热塑性树脂的分子量分布为约1.0至约2.0。
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公开(公告)号：US5412047A
公开(公告)日：1995-05-02
申请号：US242490
申请日：1994-05-13
申请人： Michael K. Georges , Marko D. Saban , Peter M. Kazmaier , Richard P. N. Veregin , Gordon K. Hamer , Karen A. Moffat
发明人： Michael K. Georges , Marko D. Saban , Peter M. Kazmaier , Richard P. N. Veregin , Gordon K. Hamer , Karen A. Moffat
摘要： A polymerization process for the preparation of homopolymeric acrylate containing thermoplastic resin or resins comprising heating a mixture comprised of a free radical initiator, an oxo nitroxide stable free radical agent, at least one polymerizable acrylate monomer compound, and optionally a solvent, to form a homopolymeric acrylate containing thermoplastic resin or resins with a high monomer to polymer conversion and a narrow polydispersity.
摘要翻译： 一种用于制备含丙烯酸酯的热塑性树脂或树脂的聚合方法，包括加热由自由基引发剂，氧代氮氧化物稳定的自由基，至少一种可聚合丙烯酸酯单体化合物和任选的溶剂组成的混合物，以形成均聚物 丙烯酸酯含有热塑性树脂或具有高单体与聚合物转化率和窄多分散性的树脂。
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公开(公告)号：US5773510A
公开(公告)日：1998-06-30
申请号：US413645
申请日：1995-03-30
申请人： Peter M. Kazmaier , Karen A. Moffat , Marko D. Saban , Richard P. N. Veregin , Michael K. Georges , Gordon K. Hamer , Toyofumi Inoue , Stephan V. Drappel
发明人： Peter M. Kazmaier , Karen A. Moffat , Marko D. Saban , Richard P. N. Veregin , Michael K. Georges , Gordon K. Hamer , Toyofumi Inoue , Stephan V. Drappel
IPC分类号： C08F2/00 , C08F257/02 , C08F265/04 , C08F279/00 , C08F279/02 , C08F283/01 , C08F287/00 , C08F291/00 , C08F293/00 , C08G83/00 , C08L51/00 , G03G9/087 , G03G9/13
CPC分类号： C08G83/003 , C08F257/02 , C08F265/04 , C08F279/00 , C08F279/02 , C08F283/01 , C08F287/00 , C08F291/00 , C08F293/005 , C08L51/003 , G03G9/08791 , G03G9/133 , Y10S430/166
摘要： A process for the preparation of branched thermoplastic resins comprising: heating a mixture of an unsaturated resin, a free radical initiator, and a stable free radical agent; adding to the heated mixture at least on polymerizable monomer; and cooling the mixture, wherein the resulting product is a branched thermoplastic resin with arms or branches comprised of polymerized monomer with substantially uniform length and narrow polydispersity.
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公开(公告)号：US5919861A
公开(公告)日：1999-07-06
申请号：US895443
申请日：1997-07-16
申请人： Peter M. Kazmaier , Karen A. Moffat , Marko D. Saban , Richard P. N. Veregin , Michael K. Georges , Gordon K. Hamer
发明人： Peter M. Kazmaier , Karen A. Moffat , Marko D. Saban , Richard P. N. Veregin , Michael K. Georges , Gordon K. Hamer
IPC分类号： C08F2/00 , C08F257/02 , C08F265/04 , C08F279/00 , C08F279/02 , C08F283/01 , C08F287/00 , C08F291/00 , C08F293/00 , C08G83/00 , C08L51/00 , G03G9/087 , G03G9/13
CPC分类号： C08G83/003 , C08F257/02 , C08F265/04 , C08F279/00 , C08F279/02 , C08F283/01 , C08F287/00 , C08F291/00 , C08F293/005 , C08L51/003 , G03G9/08791 , G03G9/133 , Y10S430/166
摘要： A process for the preparation of branched thermoplastic resins comprising: heating a mixture of an unsaturated resin, a free radical initiator, and a stable free radical agent; adding to the heated mixture at least on polymerizable monomer; and cooling the mixture, wherein the resulting product is a branched thermoplastic resin with arms or branches comprised of polymerized monomer with substantially uniform length and narrow polydispersity.
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6.发明授权Processes for preparing telechelic, branched and star thermoplastic resin polymers 失效制备遥爪，支链和星形热塑性树脂聚合物的方法
公开(公告)号：US5723511A
公开(公告)日：1998-03-03
申请号：US664702
申请日：1996-06-17
申请人： Peter M. Kazmaier , Barkev Keoshkerian , Karen A. Moffat , Michael K. Georges , Gordon K. Hamer , Richard P. N. Veregin
发明人： Peter M. Kazmaier , Barkev Keoshkerian , Karen A. Moffat , Michael K. Georges , Gordon K. Hamer , Richard P. N. Veregin
IPC分类号： C08F2/50 , C08F4/00 , C08F4/32 , C08F285/00 , C08F291/00 , C08F293/00 , C08F257/02 , C08F265/06 , C08F287/00
CPC分类号： C08F4/00 , C08F291/00 , C08F293/00 , Y10S522/904 , Y10S525/901 , Y10S525/941
摘要： A process for the preparation of branched thermoplastic resins comprising: heating a mixture of a free radical initiator, at least one first free radical reactive monomer, at least one free radical reactive branching agent compound, and at least one stable free radical agent, to produce a linear or unbranched polymer product with a free radical initator fragment at one end and a covalently bonded stable free radical agent at the other end of the polymerized chain of monomers; and irradiating the unbranched polymer product in the presence of a reactive compound selected from the group consisting of a free radical reactive monomer, a branching agent compound, and mixtures thereof to form a branched polymeric product.
摘要翻译： 一种制备支化热塑性树脂的方法，包括：加热自由基引发剂，至少一种第一自由基反应性单体，至少一种自由基反应性支化剂化合物和至少一种稳定的自由基试剂的混合物，以产生 在一端具有自由基引发剂片段的线性或非支化聚合物产物和在聚合链单体链的另一端的共价键合的稳定自由基试剂; 并且在选自自由基反应性单体，支化剂化合物及其混合物的反应性化合物存在下照射非支化聚合物产物以形成支化聚合物产物。
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公开(公告)号：US06320007B1
公开(公告)日：2001-11-20
申请号：US08345371
申请日：1994-11-18
申请人： Peter M. Kazmaier , Michael K. Georges , Richard P. N. Veregin , Barkev Keoshkerian , Gordon K. Hamer , Karen A. Moffat , Marko Saban
发明人： Peter M. Kazmaier , Michael K. Georges , Richard P. N. Veregin , Barkev Keoshkerian , Gordon K. Hamer , Karen A. Moffat , Marko Saban
IPC分类号： C08F200
CPC分类号： C08F4/00
摘要： A free radical polymerization process for the preparation of a thermoplastic resin or resins includes the in situ formation of a stable free radical agent from a precursor material in a reactor vessel, introducing a free radical initiator and at least one polymerizable monomer compound into the reactor vessel, and heating a mixture of the free radical initiator, the stable free radical agent, and the polymerizable monomer compound(s) in the reactor vessel to form a thermoplastic resin.
摘要翻译： 用于制备热塑性树脂或树脂的自由基聚合方法包括从反应器容器中的前体材料原位形成稳定的自由基试剂，将自由基引发剂和至少一种可聚合单体化合物引入反应器容器 ，并在反应器容器中加热自由基引发剂，稳定自由基和可聚合单体化合物的混合物以形成热塑性树脂。
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公开(公告)号：US5728747A
公开(公告)日：1998-03-17
申请号：US700328
申请日：1996-08-08
申请人： Peter M. Kazmaier , Barkev Keoshkerian , Rafik O. Loutfy , Karen A. Moffat , Michael K. Georges , Gordon K. Hamer , Richard P. N. Veregin
发明人： Peter M. Kazmaier , Barkev Keoshkerian , Rafik O. Loutfy , Karen A. Moffat , Michael K. Georges , Gordon K. Hamer , Richard P. N. Veregin
IPC分类号： C08F2/00 , C08F2/48 , C08F4/00 , C08F293/00 , C08F2/50
CPC分类号： C08F4/00 , C08F293/00
摘要： A free radical polymerization process for the preparation of polymer comprising: a first heating and photoinitiating with ultraviolet light of a mixture comprised of a stable free radical agent, and at least one polymerizable monomer compound; optionally cooling said mixture; a second heating of said mixture at a temperature of from about 100.degree. C. to about 160.degree. C.; isolating the polymer product formed; and optionally washing and drying said polymer.
摘要翻译： 一种用于制备聚合物的自由基聚合方法，包括：用由稳定的自由基试剂和至少一种可聚合单体化合物组成的混合物的紫外光进行第一次加热和光引发; 任选地冷却所述混合物; 所述混合物在约100℃至约160℃的温度下进行第二次加热。 分离形成的聚合物产物; 并任选地洗涤和干燥所述聚合物。
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公开(公告)号：US5817824A
公开(公告)日：1998-10-06
申请号：US905266
申请日：1997-08-01
IPC分类号： C07D211/94
CPC分类号： C07D211/94
摘要： A process for the preparation of 4-oxo-2,2,6,6-tetramethyl-1-piperidinyloxy which comprises the reaction of triacetone amine in the presence of a catalyst and a peroxide.
摘要翻译： 一种制备4-氧代-2,2,6,6-四甲基-1-哌啶基氧基的方法，其包括三丙酮胺在催化剂和过氧化物存在下的反应。
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10.发明授权Process for producing telechelic, branched and star thermoplastic resin polymers 失效生产遥爪，支链和星形热塑性树脂聚合物的方法
公开(公告)号：US5498679A
公开(公告)日：1996-03-12
申请号：US413753
申请日：1995-03-30
摘要： A free radical polymerization process for the preparation of a thermoplastic resin or resins includes heating a mixture of a multifunctional nitroxide compound and at least one polymerizable monomer compound to form a thermoplastic resin or resins; cooling the mixture; and optionally isolating and washing and drying the thermoplastic resin. A multifunctional nitroxide compound for use in the reaction is formed from a stable free radical agent and a compound having one or more halide functional groups. The free radical polymerization process may be used to prepare telechelic, branched and star polymers.
摘要翻译： 用于制备热塑性树脂或树脂的自由基聚合方法包括加热多官能氮氧化合物和至少一种可聚合单体化合物的混合物以形成热塑性树脂或树脂; 冷却混合物; 并且可选地分离和洗涤和干燥热塑性树脂。 用于反应的多官能氮氧化合物由稳定的自由基剂和具有一个或多个卤化物官能团的化合物形成。 自由基聚合方法可用于制备遥爪，支链和星形聚合物。
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