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    Tetrakisazo compound and a polarizing film containing the same
    2.
    发明授权
    Tetrakisazo compound and a polarizing film containing the same 失效
    四唑偶氮化合物和含有它们的偏光膜

    公开(公告)号：US5659020A

    公开(公告)日：1997-08-19

    申请号：US527557

    申请日：1995-09-13

    申请人： Kazuya Ogino ,  Kaneo Yokoyama ,  Narutoshi Hayashi ,  Takashi Omura

    发明人： Kazuya Ogino ,  Kaneo Yokoyama ,  Narutoshi Hayashi ,  Takashi Omura

    IPC分类号： C09B31/30 ,  C09B45/28 ,  G02B5/30 ,  C09B33/26

    CPC分类号： G02B5/3033 ,  C09B31/30 ,  C09B45/28

    摘要： A tetrakisazo compound of the formulae: ##STR1## wherein Q.sup.1 represents a phenyl or naphthyl group, Q.sup.2 represents a phenyl which is substituted by at least one substituent selected from a hydroxy group and an amino group, and R.sup.1, R.sup.2, R.sup.3 and R.sup.4 each independently represents a hydrogen atom, a hydroxy group, a lower alkyl group, a lower alkoxy group or a substituted or unsubstituted amino group, or a salt thereof, and a polarizing film which comprises the tetrakisazo compound or a salt thereof and which may further comprise other organic dyes.

    摘要翻译： 下式的四偶氮化合物：Q表示由至少一个选自羟基和氨基的取代基取代的苯基，R 1，R 2，R 3和R 4各自独立地表示氢 原子，羟基，低级烷基，低级烷氧基或取代或未取代的氨基或其盐，以及包含四偶氮化合物或其盐并可以进一步包含其它有机染料的偏振膜。

    Dye containing polarizing film
    3.
    发明授权
    Dye containing polarizing film 失效
    含偏光膜的染料

    公开(公告)号：US06235064B1

    公开(公告)日：2001-05-22

    申请号：US08249736

    申请日：1994-05-26

    申请人： Kazuya Ogino ,  Narutoshi Hayashi ,  Setsuko Yamamoto ,  Takashi Omura

    发明人： Kazuya Ogino ,  Narutoshi Hayashi ,  Setsuko Yamamoto ,  Takashi Omura

    IPC分类号： D06P700

    CPC分类号： G02B5/3033 ,  C09B67/0059

    摘要： A dye-containing polarizing film having neutral color which comprises at least one disazo dye represented by the formula (I) in the form of the free acid wherein Me is a transition metal selected from copper, nickel, zinc and iron, A1 is phenyl or naphthyl which may be substituted or substituted. B1 is 1-naphthol or 2-naphthol residue which may be unsubstituted or substituted and in which its hydroxy group is adjacent to the azo group and is linked with the transition metal Me to form the complex, and R1 is a lower alkoxy; and at least two of other specific dyes, and the film causes no light to break through the film at dark state within the visible radiation wavelength region and is excellent in the polarizing activities as well as the durability to water and heat.

    摘要翻译： 含有中性色素的含染料的偏光膜包含至少一种以式（I）表示的游离酸形式的二偶氮染料，其中Me是选自铜，镍，锌和铁的过渡金属，A1是苯基或萘基 其可以被取代或取代。 B1是可以是未取代或取代的1-萘酚或2-萘酚残基，其中羟基与偶氮基相邻，并与过渡金属Me连接形成络合物，R1是低级烷氧基; 和其他特定染料中的至少两种，并且该膜不会在可见光辐射波长区域内的黑暗状态下导致光线穿透膜，并且极化活性以及对水和热的耐久性优异。

    Dye containing polarizing film
    4.
    发明授权
    Dye containing polarizing film 失效
    含偏光膜的染料

    公开(公告)号：US5609796A

    公开(公告)日：1997-03-11

    申请号：US322620

    申请日：1994-10-13

    申请人： Setsuko Yamamoto ,  Kazuya Ogino ,  Narutohsi Hayashi ,  Takashi Omura

    发明人： Setsuko Yamamoto ,  Kazuya Ogino ,  Narutohsi Hayashi ,  Takashi Omura

    IPC分类号： C09B43/10 ,  C09B45/24 ,  C09K19/60 ,  G02B5/30 ,  F21V9/14

    CPC分类号： C09B45/24 ,  C09B43/10 ,  G02B5/3033

    摘要： A dye-containing polarizing film which comprises at least one dye selected from:dye represented by the following formula(1):Q1--N.dbd.N--Q2--X--Q3--N.dbd.N--Q4 (1)wherein Q1 and Q4 are phenyl or naphthyl group, Q2 and Q3 are phenylen group, X is azo or azoxy, and dye represented by the following formula(2): ##STR1## wherein Me is a transition metal selected from copper, nickel, zinc and iron, Q5 and Q6 are 1-naphthol or 2-naphthol residue, Y is azo or azoxy, R1 and R2 are hydrogen, lower alkyl, lower alkoxy or sulfo. The polarizing film exhibits polarizing activities not smaller than those of a iodine containing polarizing film, has excellent durability and does not cause light to break through the film by using several types of the specific dye in combination.

    摘要翻译： 含有选自下述式（1）表示的染料的至少一种染料的染料偏振膜：Q1-N = N-Q2-X-Q3-N = N-Q4（1）其中Q1和Q4为 苯基或萘基，Q2和Q3是亚苯基，X是偶氮或偶氮基，以及由下式（2）表示的染料：其中Me是选自铜，镍，锌和铁的过渡金属 ，Q5和Q6是1-萘酚或2-萘酚残基，Y是偶氮或氮氧基，R1和R2是氢，低级烷基，低级烷氧基或磺基。 偏振膜具有不低于含碘偏光膜的偏振活性，具有优异的耐久性，并且通过组合使用几种特定染料不会使光破裂。

    Disazo dyes having aminobenzoylamino group
    5.
    发明授权
    Disazo dyes having aminobenzoylamino group 失效
    具有氨基苯甲酰氨基的双偶氮染料

    公开(公告)号：US5480977A

    公开(公告)日：1996-01-02

    申请号：US134942

    申请日：1993-10-13

    申请人： Kazuya Ogino ,  Narutoshi Hayashi ,  Takashi Omura

    发明人： Kazuya Ogino ,  Narutoshi Hayashi ,  Takashi Omura

    IPC分类号： C09B45/24 ,  C09B45/28 ,  C09B45/32 ,  G02B1/08 ,  G02B5/30 ,  F21V9/14

    CPC分类号： G02B5/3033 ,  C09B45/24

    摘要： The invention is directed to a novel disazo compound represented by the formula (I) ##STR1## wherein Q is a substituted or unsubstituted phenyl or naphthyl group; Me is copper, nickel, zinc or iron; and Z is hydrogen, lower alkyl, lower alkoxyl, sulfo, or substituted or unsubstituted amino; and also to a polarizing film having said disazo compound incorporated into a polarizing film base. The polarizing film exhibits high polarizing activities comparable to those of an iodine-containing polarizing film, and also has excellent durability.

    摘要翻译： 本发明涉及由式（I）表示的新型双偶氮化合物，其中Q是取代或未取代的苯基或萘基; 我是铜，镍，锌或铁; Z为氢，低级烷基，低级烷氧基，磺基或取代或未取代的氨基; 并且还涉及一种偏振膜，其具有并入偏振膜基底中的所述双偶氮化合物。 偏光膜具有与含碘偏光膜相当的高偏振活性，并且也具有优异的耐久性。

    Metallized formazan compounds having two fiber reactive groups linked by n-alkyl-containing group
    6.
    发明授权
    Metallized formazan compounds having two fiber reactive groups linked by n-alkyl-containing group 失效
    具有由含有n-烷基的基团连接的两个纤维反应性基团的金属化的甲an化合物

    公开(公告)号：US4935500A

    公开(公告)日：1990-06-19

    申请号：US513663

    申请日：1983-07-14

    申请人： Takashi Omura ,  Katsumasa Otake ,  Kaneo Yokoyama ,  Yasuo Tezuka

    发明人： Takashi Omura ,  Katsumasa Otake ,  Kaneo Yokoyama ,  Yasuo Tezuka

    IPC分类号： C09B50/00 ,  C09B62/44 ,  C09B62/503 ,  D06P1/382 ,  D06P1/384

    CPC分类号： C09B62/4407

    摘要： A reactive metal formazan blue dye represented by a free acid of the formula, ##STR1## wherein A.sub.1 and A.sub.2 are independently a substituted or unsubstituted phenylene or naphthylene group, B is a straight or branched alkyl or alkenyl group, a phenyl group, a naphthyl group or a heterocyclic group, the alkyl, alkenyl, phenyl, napthyl and heterocyclic group being substituted or unsubstituted, Me is an ion of metal identified by an atomic number of 27 to 29, X is --O-- or ##STR2## Y is a halogen atom, Z is a group capable of imparting water solubility, each of l, m and n is 0 or an integer of 1 to 3, provided that the sum of l, m and n is from 1 to 4, D is a substituted or unsubstituted phenylene or naphthylene group, R is a substituted or unsubstituted lower alkyl group, and Q is --SO.sub.2 CH.dbd.CH.sub.2 or --SO.sub.2 CH.sub.2 CH.sub.2 L in which L is a group capable of being splitted by the action of alkali, which is useful for dyeing hydroxy- or amido-containing fiber materials with good build-up and level-dyeing properties to obtain a dyed product of deep blue color having excellent fastness, particularly against light, perspiration-light and chlorine.

    摘要翻译： 由下式游离酸代表的活性金属甲an蓝染料，其中A1和A2独立地是取代或未取代的亚苯基或亚萘基，B是直链或支链烷基或烯基，苯基，萘基 基团或杂环基团，烷基，烯基，苯基，萘基和杂环基团是取代或未取代的，Me是由原子序数27至29鉴定的金属离子，X是-O-或Y是 卤素原子，Z是能够赋予水溶性的基团，l，m和n各自为0或1〜3的整数，条件是l，m和n的和为1〜4，D为取代基 或未取代的亚苯基或亚萘基，R是取代或未取代的低级烷基，Q是-SO 2 CH = CH 2或-SO 2 CH 2 CH 2 L，其中L是能够通过碱的作用而分裂的基团，其可用于染色羟基 - 或含酰胺的纤维材料，具有良好的积聚和水平染色性能 以获得具有优异坚牢度，特别是针对光，汗水和氯的深蓝色的染色产品。

    Tetraskisazo compound and ink containing the compound
    7.
    发明授权
    Tetraskisazo compound and ink containing the compound 失效
    四丁基偶氮化合物和含有该化合物的油墨

    公开(公告)号：US5530105A

    公开(公告)日：1996-06-25

    申请号：US313458

    申请日：1994-09-27

    申请人： Satoshi Yamazaki ,  Hideo Kawashita ,  Koji Aburada ,  Kazuya Ogino ,  Yuriko Tamura ,  Takashi Omura

    发明人： Satoshi Yamazaki ,  Hideo Kawashita ,  Koji Aburada ,  Kazuya Ogino ,  Yuriko Tamura ,  Takashi Omura

    IPC分类号： C09B35/62 ,  C09D11/02

    CPC分类号： C09D11/328 ,  C09B35/62

    摘要： A tetrakisazo compound represented by the following formula (1) in the free acid form: ##STR1## wherein Q.sub.1 and Q.sub.2 independently represent phenylene or naphthylene group which may be optionally substituted, R.sub.4, R.sub.5 and R.sub.6 independently represent a hydrogen atom, a halogen atom, a hydroxy group, a sulfonic acid group or an amino, alkyl, alkoxy, carbamoyl or sulfamoyl group which may be optionally substituted, m is 0 or 1 and n is 1 or 2, and an ink which comprises the tetrakisazo compound. The ink exhibit excellent properties for ink jet printing.

    摘要翻译： 由下式（1）表示的游离酸形式的四偶氮化合物：其中Q1和Q2独立地表示可任意取代的亚苯基或亚萘基，R4，R5和R6独立地表示 表示氢原子，卤素原子，羟基，磺酸基或氨基，可以任意取代的烷基，烷氧基，氨基甲酰基或氨磺酰基，m为0或1，n为1或2， 其包含四偶氮化合物。 该油墨具有出色的喷墨印刷性能。

    Trisazo compound imparting black color, method for dyeing by using it and ink containing it
    9.
    发明授权
    Trisazo compound imparting black color, method for dyeing by using it and ink containing it 失效
    赋予黑色的Trisazo化合物，使用它的染色方法和含有它的油墨

    公开(公告)号：US5489671A

    公开(公告)日：1996-02-06

    申请号：US313642

    申请日：1994-09-27

    申请人： Kazuya Ogino ,  Yuriko Tamura ,  Takashi Omura ,  Mahito Fujita ,  Hideo Kawashita ,  Koji Aburada

    发明人： Kazuya Ogino ,  Yuriko Tamura ,  Takashi Omura ,  Mahito Fujita ,  Hideo Kawashita ,  Koji Aburada

    IPC分类号： C09B35/46 ,  C09D11/00 ,  C09D11/02 ,  D21H21/28

    CPC分类号： C09D11/328 ,  C09B35/465 ,  Y10S8/918 ,  Y10S8/919

    摘要： A trisazo compound represented by the following formula (1) in the free acid form: ##STR1## wherein Q' is phenylene group, Q.sup.2 is phenyl or naphtyl group, one of the A and B is a hydroxy group and the other is an amino group, K is 1 or 2, one of m and n is 1 and the other is 0, X and Y independently of one another are each --OR.sup.1, --SR.sup.2, --NR.sup.3 R.sup.4 or ##STR2## wherein R.sup.1, R.sup.2, R.sup.3 and R.sup.4 independently of one another are each a hydrogen atom, an alkyl, phenyl or naphthyl group; r is 1 or 2; and Z is --CH.sub.2 --, --O--, --SO.sub.2 -- or --NR.sup.5 -- wherein R.sup.5 is a hydrogen atom or C.sub.1 -C.sub.4 alkyl group;a method for dyeing fiber material, paper or leather by using the trisazo compound;and an ink which contains the trisazo compound and which is excellent in storage stability and can give a clear black printed image having excellent water resistance and light fastness.

    摘要翻译： 由游离酸形式的下式（1）表示的三偶氮化合物：（1）苯基或萘基，A和B之一是羟基，另一个是氨基，K是1或 如图2所示，m和n之一为1且另一个为0，X和Y彼此独立地为-OR 1，-SR 2，-NR 3 R 4或者其中R 1，R 2，R 3和R 4各自独立地为 氢原子，烷基，苯基或萘基; r为1或2; 且Z为-CH 2 - ， - O - ， - SO 2 - 或-NR 5 - ，其中R 5为氢原子或C 1 -C 4烷基; 通过使用三偶氮化合物对纤维材料，纸或皮革进行染色的方法; 和含有三偶氮化合物的油墨，其保存稳定性优异，能够得到清晰的黑色印刷图像，其耐水性和耐光性优异。

    Fast atom bombardment source, fast atom beam emission method, and surface modification apparatus
    10.
    发明申请
    Fast atom bombardment source, fast atom beam emission method, and surface modification apparatus 有权
    快原子轰击源，快原子束发射法和表面改性装置

    公开(公告)号：US20070284539A1

    公开(公告)日：2007-12-13

    申请号：US11790611

    申请日：2007-04-26

    申请人： Takashi Omura ,  Shinji Ishitani ,  Naoki Suzuki

    发明人： Takashi Omura ,  Shinji Ishitani ,  Naoki Suzuki

    IPC分类号： H01J27/02

    CPC分类号： H05H3/02 ,  G21K5/02 ,  G21K5/04

    摘要： A positive electrode drive unit enables a positive electrode to be repeatedly rotated about the center of the positive electrode to vary a distance between the positive electrode and an atom emission unit. A control unit receives input data which is set to obtain a desired atom density distribution by displacement of the positive electrode, and the control unit outputs a drive control signal for displacing the positive electrode to the positive electrode drive unit. The positive electrode drive unit is stopped during running by the control unit, or a drive speed of the positive electrode drive unit is changed by the control unit. Therefore, a residence time of each attitude is changed in the positive electrode to vary the atom density per unit time.

    摘要翻译： 正极驱动单元能够使正极围绕正极的中心反复旋转，以改变正极和原子发射单元之间的距离。 控制单元接收输入数据，其被设置为通过正极的位移获得期望的原子密度分布，并且控制单元输出用于将正电极移位到正电极驱动单元的驱动控制信号。 正极驱动单元在由控制单元运行期间停止，或者通过控制单元改变正极驱动单元的驱动速度。 因此，在正极中改变每个姿态的停留时间，以改变每单位时间的原子密度。