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公开(公告)号：US20190177863A1
公开(公告)日：2019-06-13
申请号：US15841031
申请日：2017-12-13
Inventor： Mazen Mohamed KHALED , Ramadan Abdelmonem Geioushy , Khalid Alhooshani
Abstract: An electrode with a conductive substrate and an electrocatalyst comprising zinc oxide and copper oxide supported on a carbon nanomaterial, a method of fabricating the electrode, an electrochemical cell that utilizes the electrode as a working electrode, and a process for producing propanol from CO2 with the electrochemical cell. Various combinations of embodiments of the electrode and the method of fabricating thereof, the electrochemical cell, and the process for producing propanol from CO2 is provided.
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公开(公告)号：US12215025B1
公开(公告)日：2025-02-04
申请号：US18774551
申请日：2024-07-16
Inventor： Khalid Alhooshani , Mohammed Mosaad Awad , Ijaz Hussain
Abstract: A method for dry reformation of methane (DRM) includes introducing a H2-containing feed gas stream into a reactor, including a nickel-containing fibrous silica zinc oxide (Ni/FSZ) catalyst, passing the H2-containing feed gas stream through the reactor to contact the H2-containing feed gas stream with particles of the Ni/FSZ catalyst at a temperature of from 500 to 900 degrees Celsius (° C.) to form a reduced catalyst; terminating the introduction of the H2-containing feed gas stream and introducing and passing a mixed feed gas stream including CH4 and CO2 through the reactor to contact the mixed feed gas stream with the reduced catalyst at a temperature of from 500 to 1000° C. thereby converting at least a portion of the CH4 and CO2 to H2 and CO; and regenerating the Ni/FSZ catalyst particles to form a regenerated catalyst and producing a residue gas stream leaving the reactor.
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公开(公告)号：US11833485B2
公开(公告)日：2023-12-05
申请号：US17708582
申请日：2022-03-30
Inventor： Khalid Alhooshani , Abdulkadir Tanimu
CPC classification number: B01J20/3255 , B01J20/103 , B01J20/28061 , B01J20/28071 , B01J20/28073 , B01J20/28083 , B01J20/3236 , B01J2220/46
Abstract: A functionalized silica sorbent is described. The sorbent comprises mesoporous silica nanoparticles having a surface functionalized with a conjugated system comprising an azole and a phenyl. The surface may be functionalized by a Cu-catalyzed click reaction. The nanoparticles have an average particle size of 10-80 nm, and may be used to adsorb phenolic contaminants from aqueous solutions.
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公开(公告)号：US11630089B2
公开(公告)日：2023-04-18
申请号：US16255192
申请日：2019-01-23
Inventor： Khalid Alhooshani , Shehzada Muhammad Sajid Jilani
IPC: G01N1/40 , G01N30/08 , B01J20/06 , B01J20/22 , B01J20/28 , B01J20/32 , B01J20/34 , G01N33/18 , G01N30/00
Abstract: Yttria containing hybrid organic-inorganic sol-gels may be used in coatings for capillary microextraction, optionally hyphenated to online HPLC analysis. The sol-gel reaction mixture can use an yttrium trialkoxyalkoxide, such as yttrium trimethoxyethoxide, and a [bis(hydroxyalkyl)-amino-alkyl]-terminated polydialkyl/arylsiloxane, such as [bis(hydroxyethyl)-amine] (BHEA)-terminated polydimethylsiloxane, that can undergo hydrolysis and polycondensation, to form coating materials. Capillaries coated with such sol-gels can have improved extraction efficiency compared, e.g., to pure yttria-based coatings. The CME-HPLC can analyze water samples containing analytes of varied polarity, with excellent extraction of amides, phenols, alcohols, ketones, aldehydes, and polyaromatic hydrocarbons and detection limits ranging from 0.18 to 7.35 ng/mL (S/N=3). Such capillaries can exhibit solvent stability at pH 0 to 14, RSD % between 0.6 to 6.8% (n=3), at a preparative reproducibility RSD between 4.1 and 9.9%.
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Patent Agency Ranking
5.发明授权Method of determining phenoxy herbicides in water samples by phase transfer microextraction with simultaneous derivatization and gas-chromatography mass-spectrometry analysis 有权通过相转移微萃取法同时进行衍生化和气相色谱质谱分析，测定水样中苯氧基除草剂的方法公开(公告)号：US09316629B2
公开(公告)日：2016-04-19
申请号：US14031658
申请日：2013-09-19
Inventor： Abdulmumin A. Nuhu , Chanbasha Basheer , Khalid Alhooshani , Abdul Rahman Al-Arfaj
CPC classification number: G01N33/1826 , G01N30/7206 , G01N2030/067
Abstract: A method for determining the concentration of a phenoxy herbicide in an aqueous sample, by simultaneously phase-transfer catalyst extracting and alkylating an aqueous sample comprising a phenoxy herbicide to form a sample composition, and measuring an amount of the alkylated phenoxy herbicide in the sample composition. The method includes controlling factors such as pH of the aqueous matrix, temperature, extraction duration, type and amount of derivation reagents, and type and amount of phase transfer catalyst.
Abstract translation: 一种用于通过同时相转移催化剂萃取和烷基化包含苯氧基除草剂的含水样品以形成样品组合物并测量样品组合物中烷基化苯氧基除草剂的量来测定水性样品中苯氧基除草剂浓度的方法 。 该方法包括控制诸如水基质的pH，温度，萃取持续时间，衍生试剂的类型和数量以及相转移催化剂的类型和量的因素。
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6.发明申请公开(公告)号：US20150079692A1
公开(公告)日：2015-03-19
申请号：US14031658
申请日：2013-09-19
Inventor： Abdulmumin A NUHU , Chanbasha Basheer , Khalid Alhooshani , Abdul Rahman Al-Arfaj
IPC: G01N33/18
CPC classification number: G01N33/1826 , G01N30/7206 , G01N2030/067
Abstract: A method for determining the concentration of a phenoxy herbicide in an aqueous sample, by simultaneously phase-transfer catalyst extracting and alkylating an aqueous sample comprising a phenoxy herbicide to form a sample composition, and measuring an amount of the alkylated phenoxy herbicide in the sample composition. The method includes controlling factors such as pH of the aqueous matrix, temperature, extraction duration, type and amount of derivation reagents, and type and amount of phase transfer catalyst.
Abstract translation: 一种用于通过同时相转移催化剂萃取和烷基化包含苯氧基除草剂的含水样品以形成样品组合物并测量样品组合物中烷基化苯氧基除草剂的量来测定水性样品中苯氧基除草剂浓度的方法 。 该方法包括控制诸如水基质的pH，温度，萃取持续时间，衍生试剂的类型和数量以及相转移催化剂的类型和量的因素。
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公开(公告)号：US11305259B2
公开(公告)日：2022-04-19
申请号：US16296480
申请日：2019-03-08
Inventor： Khalid Alhooshani , Abdulkadir Tanimu
Abstract: A functionalized silica sorbent is described. The sorbent comprises mesoporous silica nanoparticles having a surface functionalized with a conjugated system comprising an azole and a phenyl. The surface may be functionalized by a Cu-catalyzed click reaction. The nanoparticles have an average particle size of 10-80 nm, and may be used to adsorb phenolic contaminants from aqueous solutions.
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8.发明申请公开(公告)号：US20200282380A1
公开(公告)日：2020-09-10
申请号：US16296480
申请日：2019-03-08
Inventor： Khalid Alhooshani , Abdulkadir Tanimu
Abstract: A functionalized silica sorbent is described. The sorbent comprises mesoporous silica nanoparticles having a surface functionalized with a conjugated system comprising an azole and a phenyl. The surface may be functionalized by a Cu-catalyzed click reaction. The nanoparticles have an average particle size of 10-80 nm, and may be used to adsorb phenolic contaminants from aqueous solutions.
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公开(公告)号：US10537883B2
公开(公告)日：2020-01-21
申请号：US15715688
申请日：2017-09-26
Inventor： Khalid Alhooshani , Saheed Adewale Ganiyu
Abstract: A single-pot method of producing a hydrodesulfurization catalyst by hydrothermally treating a hydrothermal precursor that includes a silica source, a structural directing surfactant, an aqueous acid solution, and metal precursors that contain active catalyst materials is provided. The hydrodesulfurization catalyst includes a catalyst support having SBA-15 and preferably titanium, wherein the active catalyst materials are homogenously deposited on the catalyst support. Various embodiments of said method and the hydrodesulfurization catalyst are also provided.
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