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    Method of Preparing Wholly Aromatic Polyester
    1.
    发明申请
    Method of Preparing Wholly Aromatic Polyester 审中-公开
    制备全芳族聚酯的方法

    公开(公告)号：US20090212451A1

    公开(公告)日：2009-08-27

    申请号：US12084441

    申请日：2006-11-01

    申请人： Mahn Jong Kim ,  Jong Hwa Yun ,  Youn Eung Lee ,  Tae Jun Ok ,  Sun Hwa Jang ,  Hyun Min Kim

    发明人： Mahn Jong Kim ,  Jong Hwa Yun ,  Youn Eung Lee ,  Tae Jun Ok ,  Sun Hwa Jang ,  Hyun Min Kim

    IPC分类号： B29B9/12 ,  C08G63/183 ,  C08L67/03 ,  C08K3/34 ,  C08K3/40 ,  C08K3/22 ,  B29B9/10

    CPC分类号： C08G63/785 ,  B01F7/00116 ,  B01F7/00175 ,  B01F7/00266 ,  B01F7/00291 ,  B01F7/00433 ,  B01J19/1806 ,  B01J2219/00779 ,  C08G63/133 ,  C08G63/605 ,  C08G63/80 ,  C08K3/013 ,  C08K7/00 ,  C08L67/00 ,  C08L2205/02

    摘要： The invention relates to a method of preparing wholly aromatic polyester including: mixing monomers, introducing the mixed monomers into a reactor having a rectangular or trapezoidal plate type stirring impeller, and polymerizing the introduced monomers through esterification with a power per unit volume of 10˜60 kW/m3, a length (L) to diameter (D) ratio of the stirring impeller is 1˜3:1, and a distance between the bottom of the reactor and a lower portion of the stirring impeller is 1/100˜ 1/15 times of the diameter (D); b) pulverizing the obtained polymer; and c) solid state polymerizing the pulverized polymer. The present invention also relates to a method of preparing wholly aromatic polyester having excellent heat resistant properties in which byproduct is effectively discharged by controlling a heating rate and reaction holding time between the weight loss initiating temperature and the melting point of a low molecular weight polymer generated in a melt polymerization in a solid state polymerization, adhesion does not occur, and discoloration due to heating does not occur.

    摘要翻译： 本发明涉及一种制备全芳族聚酯的方法，包括：将单体混合，将混合单体引入具有矩形或梯形板式搅拌叶轮的反应器中，并通过酯化每单位体积10〜60的功率聚合引入的单体 kW / m3，搅拌叶轮的长度（L）与直径（D）的比为1〜3:1，反应器底部与搅拌叶轮下部的距离为1/100〜1 / 15倍直径（D）; b）粉碎所得聚合物; 和c）固态聚合粉碎的聚合物。 本发明还涉及一种制备全芳香族聚酯的方法，其具有优异的耐热性能，其中通过控制生成的低分子量聚合物的重量损失起始温度和熔点之间的加热速率和反应保持时间来有效排出副产物 在固态聚合中的熔融聚合中，不会发生粘合，并且不会发生由于加热而变色。

    METHOD OF PREPARING WHOLLY AROMATIC LIQUID CRYSTALLINE POLYESTER RESIN AND RESIN PREPARED BY THE METHOD, AND COMPOUND INCLUDING THE RESIN
    2.
    发明申请
    METHOD OF PREPARING WHOLLY AROMATIC LIQUID CRYSTALLINE POLYESTER RESIN AND RESIN PREPARED BY THE METHOD, AND COMPOUND INCLUDING THE RESIN 审中-公开
    制备芳香族液晶聚酯树脂的方法和方法制备的树脂和包括树脂的化合物

    公开(公告)号：US20130331540A1

    公开(公告)日：2013-12-12

    申请号：US13984953

    申请日：2011-11-28

    申请人： Hyun Min Kim ,  Jong Hwa Yun ,  Mahn Jong Kim

    发明人： Hyun Min Kim ,  Jong Hwa Yun ,  Mahn Jong Kim

    IPC分类号： C08G63/78 ,  C08G63/60

    CPC分类号： C08G63/78 ,  C08G63/605

    摘要： Provided is a method of preparing a wholly aromatic liquid crystalline polyester resin and a wholly aromatic liquid crystalline polyester resin prepared by the method, and a compound of the wholly aromatic liquid crystalline polyester resin. The disclosed method of preparing the wholly aromatic liquid crystalline polyester resin includes a step (a first temperature increasing step) of increasing the temperature of a reaction mixture including at least one monomer at a first temperature increasing rate up to a first temperature; a step (an isothermal maintaining step) of maintaining the reaction mixture that passed through the first temperature increasing step at the first temperature for a first time; and a step (a second temperature increasing step) of increasing the temperature of the reaction mixture that passed through the isothermal maintaining step at a second temperature increasing rate.

    摘要翻译： 提供一种制备全芳族液晶聚酯树脂和通过该方法制备的全芳族液晶聚酯树脂的方法和全芳族液晶聚酯树脂的化合物。 所公开的制备全芳香族液晶聚酯树脂的方法包括以第一升温速率将包含至少一种单体的反应混合物的温度升至第一温度的步骤（第一升温步骤）; 将通过第一升温步骤的反应混合物在第一温度下保持第一次的步骤（等温保持步骤）; 和以第二升温速度提高通过等温保持步骤的反应混合物的温度的步骤（第二升温步骤）。

    PRODUCTION METHOD FOR A WHOLLY AROMATIC LIQUID CRYSTALLINE POLYESTER RESIN, A WHOLLY AROMATIC LIQUID CRYSTALLINE POLYESTER RESIN PRODUCED BY MEANS OF THE METHOD, AND A COMPOUND OF THE WHOLLY AROMATIC LIQUID CRYSTALLINE POLYESTER RESIN
    3.
    发明申请
    PRODUCTION METHOD FOR A WHOLLY AROMATIC LIQUID CRYSTALLINE POLYESTER RESIN, A WHOLLY AROMATIC LIQUID CRYSTALLINE POLYESTER RESIN PRODUCED BY MEANS OF THE METHOD, AND A COMPOUND OF THE WHOLLY AROMATIC LIQUID CRYSTALLINE POLYESTER RESIN 有权
    一种纯粹的芳香族液晶聚酯树脂的生产方法，该方法生产的一种纯粹的芳香族液晶聚酯树脂，以及一种芳香族液晶聚酯树脂的化合物

    公开(公告)号：US20130137845A1

    公开(公告)日：2013-05-30

    申请号：US13521618

    申请日：2011-01-12

    申请人： Hyun Min Kim ,  Jong Hwa Yun ,  Mahn Jong Kim

    发明人： Hyun Min Kim ,  Jong Hwa Yun ,  Mahn Jong Kim

    IPC分类号： C08G63/80

    CPC分类号： C08G63/80 ,  C08G63/605 ,  C08G63/78 ,  C09K19/3809

    摘要： Disclosed are a production method for a wholly aromatic liquid crystalline polyester resin, a wholly aromatic liquid crystalline polyester resin produced using the method, and a compound of the wholly aromatic liquid crystalline polyester resin. The disclosed production method for a wholly aromatic liquid crystalline polyester resin comprises the steps of synthesizing a wholly aromatic liquid crystalline polyester resin by synthesizing a wholly aromatic liquid crystalline polyester prepolymer by a condensation polymerization of a monomer and then reducing the pressure inside a reaction vessel containing the synthesized prepolymer at a predetermined internal pressure reduction rate of the reaction vessel.

    摘要翻译： 公开了全芳香族液晶聚酯树脂的制造方法，使用该方法制造的全芳香族液晶聚酯树脂和全芳香族液晶聚酯树脂的化合物。 所公开的全芳族液晶聚酯树脂的制造方法包括以下步骤：通过单体的缩聚合成全芳香族液晶聚酯预聚物，然后降低含有 所述合成的预聚物以所述反应容器的预定内压降低速率。