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    Combatting insects and acarids with certain O-methyl/ethyl-S-propyl/butyl-O-phenyl-thiophosphates and -dithiophosphates
    4.
    发明授权
    Combatting insects and acarids with certain O-methyl/ethyl-S-propyl/butyl-O-phenyl-thiophosphates and -dithiophosphates 失效
    用某些O-甲基/乙基-S-丙基/丁基-O-苯基 - 硫代磷酸酯和二硫代磷酸酯来防治昆虫和螨

    公开(公告)号：US4017612A

    公开(公告)日：1977-04-12

    申请号：US578960

    申请日：1975-05-19

    申请人： Ernst Beriger ,  Manfred Boger ,  Jozef Drabek ,  Odd Kristiansen

    发明人： Ernst Beriger ,  Manfred Boger ,  Jozef Drabek ,  Odd Kristiansen

    IPC分类号： A01N57/10 ,  C07F9/18 ,  A01N9/36

    CPC分类号： A01N57/10 ,  C07F9/18

    摘要： Thiophosphoric and dithiophosphoric acid esters of the formula ##STR1## wherein R.sub.1 represents methyl or ethyl, R.sub.2 represents n-propyl, isobutyl or sec, butyl, R.sub.3 and R.sub.4 each represents chlorine, bromine, methyl or ethyl, R.sub.5 represents--OCOCH.sub.3, --O--C.sub.3 --C.sub.5 --alkenyl, --O--C.sub.3 --C.sub.5 --alkinyl, --O--C.sub.1 --C.sub.4 --alkylene-O--C.sub.1 --C.sub.4 --alkyl, --O--CH.sub.2 --CCl=CH.sub.2, --O--CH.sub.2 --CH=CHCl, ##STR2## --S--C.sub.3 --C.sub.5 --alkenyl, SCN, --CH.sub.2 --CCl=CH.sub.2, --CH.sub.2 CH=CHCl, --CHO, ##STR3## ##STR4## AND X represents oxygen or sulphur, processes for their manufacture and their use in pest control.

    摘要翻译： 其中R 1表示甲基或乙基，R 2表示正丙基，异丁基或仲丁基，R 3和R 4各自表示氯，溴，甲基或乙基，R 5表示-OCOCH 3，-O -C 3 -C 5 - 烯基，-O-C 3 -C 5 - 炔基，-O-C 1 -C 4亚烷基-O-C 1 -C 4烷基，-O-CH 2 -CCl = CH 2，-O-CH 2 -CH = CHCl ，图像-S-C3-C5-烯基，SCN，-CH2-CCl = CH2，-CH2CH = CHCl，-CHO，

    O-methyl/ethyl-S-propyl/butyl-O-phenyl thiphosphates and dithiophosphates having a thioether group on the phenyl ring
    5.
    发明授权
    O-methyl/ethyl-S-propyl/butyl-O-phenyl thiphosphates and dithiophosphates having a thioether group on the phenyl ring 失效
    在苯环上具有硫醚基的O-甲基/乙基-S-丙基/丁基-O-邻苯二磷酸酯和二硫代磷酸酯

    公开(公告)号：US3991141A

    公开(公告)日：1976-11-09

    申请号：US534591

    申请日：1974-12-20

    申请人： Ernst Beriger ,  Manfred Boger ,  Jozef Drabek ,  Odd Kristiansen

    发明人： Ernst Beriger ,  Manfred Boger ,  Jozef Drabek ,  Odd Kristiansen

    IPC分类号： A01N57/10 ,  C07F9/18 ,  C07F9/12

    CPC分类号： C07F9/18 ,  A01N57/10

    摘要： Thiophosphoric and dithiophosphoric acid esters of the formula ##SPC1##Wherein R.sub.1 represents methyl or ethyl, R.sub.2 represents n-propyl, isobutyl or sec, butyl, R.sub.3 and R.sub.4 each represents chlorine, bromine, methyl or ethyl, R.sub.5 represents--OCOCH.sub.3, --O--C.sub.3 --C.sub.5 -alkenyl, --O--C.sub.3 --C.sub.5 -alkinyl, --O--C.sub.1 --C.sub.4 -alkylene-O--C.sub.1 --C.sub.4 -alkyl, --O--CH.sub.2 --CCl=CH.sub.2, --O--CH.sub.2 --CH=CHCl, ##EQU1##--S--C.sub.3 --C.sub.5 -alkenyl, SCN, --CH.sub.2 --CCl=CH.sub.2, --CH.sub.2 CH=CHCl, --CHO, ##SPC2##--CH=N--C.sub.1 --C.sub.4 -alkyl, --CH=N--NH--C.sub.1 --C.sub.4 -alkyl or X represents oxygen or sulphur, processes for their manufacture and their use in pest control.

    摘要翻译： 式II的硫代磷酸和二硫代磷酸酯，其中R1表示甲基或乙基，R2表示正丙基，异丁基或仲丁基，R 3和R 4各自表示氯，溴，甲基或乙基，R 5表示-OCOCH 3，-O-C 3 - C5-烯基，-O-C3-C5-炔基，-O-C1-C4-亚烷基-O-C1-C4-烷基，-O-CH2-CCl = CH2，-O-CH2-CH = CHCl，-SCH2 -S-C 3 -C 5 - 烯基，SCN，-CH 2 -CCl = CH 2，-CH 2 CH = CHCl，-CHO，O -CH ANGLE，O -CH = N-C 1 -C 4烷基，-CH = C 1 -C 4 - 烷基或C 1 -C 4 - 烷基-CH = NN ANGLE和C 1 -C 4 - 烷基X代表氧或硫，其制备方法及其在害虫防治中的应用。

    O-methyl/ethyl-s-propyl/butyl-o-phenyl thiophosphates and dithiophosphates having an ether group or the phenyl ring
    6.
    发明授权
    O-methyl/ethyl-s-propyl/butyl-o-phenyl thiophosphates and dithiophosphates having an ether group or the phenyl ring 失效
    具有醚基或苯环的O-甲基/乙基 - 正丙基/丁基邻苯基硫代磷酸酯和二硫代磷酸酯

    公开(公告)号：US3943202A

    公开(公告)日：1976-03-09

    申请号：US534594

    申请日：1974-12-20

    申请人： Ernst Beriger ,  Manfred Boger ,  Jozef Drabek ,  Odd Kristiansen

    发明人： Ernst Beriger ,  Manfred Boger ,  Jozef Drabek ,  Odd Kristiansen

    IPC分类号： A01N57/10 ,  C07F9/18 ,  C07F9/12

    CPC分类号： A01N57/10 ,  C07F9/18

    摘要： Thiophosphoric and dithiophosphoric acid esters of the formula ##SPC1##Wherein R.sub.1 represents methyl or ethyl, R.sub.2 represents n-propyl, isobutyl or sec, butyl, R.sub.3 and R.sub.4 each represents chlorine, bromine, methyl or ethyl, R.sub.5 represents ##EQU1## X represents oxygen or sulphur, processes for their manufacture and their use in pest control.

    摘要翻译： 式II的硫代磷酸和二硫代磷酸酯，其中R1表示甲基或乙基，R2表示正丙基，异丁基或仲丁基，R 3和R 4各自表示氯，溴，甲基或乙基，R 5表示-OCOCH 3，-O-C 3 - C5-烯基，-O-C3-C5-炔基，-O-C1-C4-亚烷基-O-C1-C4-烷基，-O-CH2-CCl = CH2，-O-CH2-CH = CHCl，-SCH2 -S-C 3 -C 5 - 烯基，SCN，-CH 2 -CCl = CH 2，O -CH 2 CH = CHCl，-CHO，-CHOGLE，O O-CH 3 O-CH 3 -CHO | CH- ，O-CH 3 O-CH 3 | O-CH 3 O - -CH ANGLE |，-CH-角ANGLE，O-CH 3 O - S - OC 1 -C 4 - 烷基|，-CH ANGLE，-C ANGLE | S-OC 1 -C 4 - 烷基CH 3 SC 1 -C 4 - 烷基S- -CH ANGLE，-CH ANGLE |，SC 1 -C 4 - 烷基S- O-S- -CH ANGLE |，-CH角度，S- S- - CH 3 S-C 2 H 5 -CHORGLE |，-CH ANGLE |，S- S- -CH = N-C 1 -C 4 - 烷基，-CH = N-NH-C 1 -C 4 - 烷基或C 1 -C 4烷基 -CH = NN ANGLE C 1 -C 4 - 烷基，X代表氧或硫，它们的制备过程及其在害虫防治中的应用。

    O-methyl/ethyl-s-propyl/butyl-o-phenyl thiophosphates and dithiophosphates having an o-heterocyclic group or the phenyl ring
    7.
    发明授权
    O-methyl/ethyl-s-propyl/butyl-o-phenyl thiophosphates and dithiophosphates having an o-heterocyclic group or the phenyl ring 失效
    O-甲基/乙基 - 正丙基/丁基邻苯基硫代磷酸酯和具有o-杂环基团或苯环的二硫代磷酸酯

    公开(公告)号：US3935233A

    公开(公告)日：1976-01-27

    申请号：US534933

    申请日：1974-12-20

    申请人： Ernst Beriger ,  Manfred Boger ,  Jozef Drabek ,  Odd Kristiansen

    发明人： Ernst Beriger ,  Manfred Boger ,  Jozef Drabek ,  Odd Kristiansen

    IPC分类号： A01N57/10 ,  C07F9/18 ,  C07D319/06 ,  A01N9/28

    CPC分类号： C07F9/18 ,  A01N57/10 ,  Y10S514/949

    摘要： Thiophosphoric and dithiophosphoric acid esters of the formula ##SPC1##Wherein R.sub.1 represents methyl or ethyl, R.sub.2 represents n-propyl, isobutyl or sec, butyl, R.sub.3 and R.sub.4 each represents chlorine, bromine, methyl or ethyl, R.sub.5 represents ##EQU1## AND X represents oxygen or sulphur, processes for their manufacture and their use in pest control.

    摘要翻译： 式II的硫代磷酸和二硫代磷酸酯，其中R1表示甲基或乙基，R2表示正丙基，异丁基或仲丁基，R 3和R 4各自表示氯，溴，甲基或乙基，R 5表示-OCOCH 3，-O-C 3 - C5-烯基，-O-C3-C5-炔基，-O-C1-C4-亚烷基-O-C1-C4-烷基，-O-CH2-CCl = CH2，-O-CH2-CH = CHCl，-S -C 3 -C 5 - 烯基，SCN，-CH 2 -CCl = CH 2，O -CH 2 CH = CHCl，-CHO，-CHOGLE，OO-CH 3 O-CH 3 -CHOGLE |，-CH ANGLE |，O- CH 3 O-CH 3 | O-CH 3 O--CH ANGLE |，-CH-角ANGLE，O-CH 3 O-OC 1 -C 4 - 烷基-S -CH-，-C ANGLE |，OC 1 -C 4 - 烷基-S- C 1 -C 4烷基-S -CH-CH 2，-CH 2，-CH 2，-CH 2，-CH 2，-CH 2， SS--CH = N-C 1 -C 4 - 烷基-CH = N-NH-C 1 -C 4 - 烷基或C 1 -C 4烷基-CH = NN ANGLE C 1 -C 4烷基，X代表氧或硫， 制造及其在病虫害防治中的应用。

    Substituted thioureas, isothioureas and carbodiimides
    10.
    发明授权
    Substituted thioureas, isothioureas and carbodiimides 失效
    取代硫脲，异硫脲和碳二亚胺

    公开(公告)号：US4888348A

    公开(公告)日：1989-12-19

    申请号：US91157

    申请日：1987-08-28

    申请人： Josef Ehrenfreund ,  Manfred Boger ,  Odd Kristiansen ,  Jozef Drabek ,  Haukur Kristinsson

    发明人： Josef Ehrenfreund ,  Manfred Boger ,  Odd Kristiansen ,  Jozef Drabek ,  Haukur Kristinsson

    IPC分类号： A01N47/30 ,  A01N47/32 ,  A01N47/40 ,  A01N47/42 ,  C07D207/34 ,  C07D209/32 ,  C07D231/20 ,  C07D233/70 ,  C07D235/26 ,  C07D249/12 ,  C07D257/04 ,  C07D263/38 ,  C07D263/58 ,  C07D271/10 ,  C07D271/113 ,  C07D277/20 ,  C07D277/34 ,  C07D277/68 ,  C07D285/08 ,  C07D285/12 ,  C07D285/13 ,  C07D307/58 ,  C07D333/32 ,  C07D333/34

    CPC分类号： C07D271/113 ,  A01N47/30 ,  A01N47/32 ,  A01N47/40 ,  A01N47/42 ,  C07D233/70 ,  C07D249/12 ,  C07D277/34 ,  C07D277/68 ,  C07D285/08 ,  C07D285/13

    摘要： The invention relates to novel substituted phenylthioureas, phenylisothioureas and phenylcarbodiimides of formula I ##STR1## wherein Z is ##STR2## or --N.dbd.C.dbd.N--; R.sub.1 is C.sub.1 -C.sub.12 alkyl, C.sub.3 -C.sub.10 alkenyl, C.sub.3 -C.sub.10 alkynyl, C.sub.3 -C.sub.8 cycloalkyl, C.sub.1 -C.sub.3 alkyl substituted by 1 or 2 C.sub.3 -C.sub.6 cycloalkyl radicals, or is alkoxyalkyl containing a total of 3 to 10 carbon atoms, halogen-substituted C.sub.1 -C.sub.12 alkyl, polycyclic C.sub.7 -C.sub.10 cycloalkyl, or phenyl(C.sub.1 -C.sub.5)alkyl which may be substituted in the phenyl moiety by 1 or 2 identical or different members selected from the group consisting of halogen, methoxy, ethoxy and C.sub.1 -C.sub.5 alkyl,R.sub.2 is hydrogen or C.sub.1 -C.sub.5 alkyl,R.sub.3 is C.sub.1 -C.sub.5 alkyl or C.sub.3 -C.sub.6 cycloalkyl,R.sub.4 is hydrogen or C.sub.1 -C.sub.4 alkyl,R.sub.5 is a 5-membered heterocyclic radical containing 1 to 4 hetero atoms selected from the group consisting of N, O and S, which radical may be substituted at the carbon or nitrogen atoms by 1 to 3 of the substituents R.sub.6, R.sub.7 and R.sub.8, or is a 5-membered heterocyclic radical which may be fused with benzene nuclei and which contains 1 or 2 hetero atoms selected from the group consisting of N, O and S and can be substituted at the carbon or nitrogen atoms by 1 to 3 of the substituents R.sub.6, R.sub.7 and R.sub.8,R.sub.6 and R.sub.7 are each independently of the other hydrogen, halogen, C.sub.1 -C.sub.4 alkyl, halogen-substituted C.sub.1 -C.sub.4 alkyl, C.sub.1 -C.sub.4 alkoxy; halogen-substituted C.sub.1 -C.sub.4 alkoxy, phenyl, or C.sub.1 -C.sub.4 alkylthio,R.sub.8 is hydrogen or C.sub.1 -C.sub.4 alkyl, andR.sub.9 is C.sub.1 -C.sub.5 alkyl, C.sub.2 -C.sub.5 alkenyl, C.sub.3 -C.sub.4 alkynyl, alkoxyalkyl containing a total of 10 carbon atoms, or alkylthioalkyl containing a total of 10 carbon atomsand to the salts thereof with acids and bases. The invention further relates to the preparation of these compounds and to the use thereof in pest control, and to novel intermediates.

    摘要翻译： 本发明涉及式I的新的取代的苯基硫脲，苯基异硫脲和苯基碳二亚胺其中Z是或-N = C = N-; R 1是C 1 -C 12烷基，C 3 -C 10烯基，C 3 -C 10炔基，C 3 -C 8环烷基，被1或2个C 3 -C 6环烷基取代的C 1 -C 3烷基，或者是含有总共3至10个碳原子的烷氧基烷基，卤素取代的C 1 -C 12烷基 ，多环C 7 -C 10环烷基或可在苯基部分被1或2个选自卤素，甲氧基，乙氧基和C 1 -C 5烷基的相同或不同的成员取代的苯基（C 1 -C 5）烷基，R 2为氢或 C 1 -C 5烷基，R 3是C 1 -C 5烷基或C 3 -C 6环烷基，R 4是氢或C 1 -C 4烷基，R 5是含有1至4个选自N，O和S的杂原子的5元杂环基， 可以在碳原子或氮原子上被1至3个取代基R6，R7和R8取代，或者是可以与苯核稠合并且含有1或2个选自以下的杂原子的5元杂环基： 的N，O和S，并且可以在碳或氮原子上被1至3个取代 取代基R 6，R 7和R 8，R 6和R 7各自独立地为氢，卤素，C 1 -C 4烷基，卤素取代的C 1 -C 4烷基，C 1 -C 4烷氧基， 卤素取代的C1-C4烷氧基，苯基或C1-C4烷硫基，R8是氢或C1-C4烷基，R9是C1-C5烷基，C2-C5链烯基，C3-C4炔基，含有总共10个碳原子的烷氧基烷基，或含有 总共10个碳原子，并与其与酸和碱的盐反应。 本发明进一步涉及这些化合物的制备及其在病虫害防治中的应用，以及新颖的中间体。