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1.发明授权Strengthened glass substrates with glass frits and methods for making the same 有权用玻璃料加强玻璃基板和制作相同的方法公开(公告)号：US09346708B2
公开(公告)日：2016-05-24
申请号：US13464493
申请日：2012-05-04
CPC分类号： C03C8/08 , C03C3/17 , C03C3/19 , C03C3/21 , C03C4/02 , C03C4/18 , C03C17/04 , C03C2204/00 , C03C2207/00 , Y10T428/24942 , Y10T428/315
摘要： Strengthened glass substrates with glass fits and methods for forming the same are disclosed. According to one embodiment, a method for forming a glass frit on a glass substrate may include providing a glass substrate comprising a compressive stress layer extending from a surface of the glass substrate into a thickness of the glass substrate, the compressive stress having a depth of layer DOL and an initial compressive stress CSi. A glass frit composition may be deposited on at least a portion of the surface of the glass substrate. Thereafter, the glass substrate and the glass frit composition are heated in a furnace to sinter the glass fit composition and bond the glass frit composition to the glass substrate, wherein, after heating, the glass substrate has a fired compressive stress CSf which is greater than or equal to 0.70*CSi.
摘要翻译： 公开了使用玻璃配合的加强玻璃基板及其形成方法。 根据一个实施例，在玻璃基板上形成玻璃料的方法可以包括提供一种玻璃基板，其包括从玻璃基板的表面延伸到玻璃基板的厚度的压缩应力层，压缩应力的深度为 层DOL和初始压应力CSi。 可以在玻璃基板的表面的至少一部分上沉积玻璃料组合物。 然后，将玻璃基板和玻璃料组合物在炉中加热烧结玻璃配合组合物，并将玻璃料组合物粘合到玻璃基板上，其中，在加热之后，玻璃基板的烧制压缩应力CSf大于 或等于0.70 * CSi。
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2.发明申请STRENGTHENED GLASS SUBSTRATES WITH GLASS FRITS AND METHODS FOR MAKING THE SAME 有权具有玻璃纤维的加强玻璃基材及其制造方法公开(公告)号：US20130295353A1
公开(公告)日：2013-11-07
申请号：US13464493
申请日：2012-05-04
IPC分类号： C03C17/04
CPC分类号： C03C8/08 , C03C3/17 , C03C3/19 , C03C3/21 , C03C4/02 , C03C4/18 , C03C17/04 , C03C2204/00 , C03C2207/00 , Y10T428/24942 , Y10T428/315
摘要： Strengthened glass substrates with glass fits and methods for forming the same are disclosed. According to one embodiment, a method for forming a glass frit on a glass substrate may include providing a glass substrate comprising a compressive stress layer extending from a surface of the glass substrate into a thickness of the glass substrate, the compressive stress having a depth of layer DOL and an initial compressive stress CSi. A glass frit composition may be deposited on at least a portion of the surface of the glass substrate. Thereafter, the glass substrate and the glass frit composition are heated in a furnace to sinter the glass fit composition and bond the glass frit composition to the glass substrate, wherein, after heating, the glass substrate has a fired compressive stress CSf which is greater than or equal to 0.70*CSi.
摘要翻译： 公开了使用玻璃配合的加强玻璃基板及其形成方法。 根据一个实施例，在玻璃基板上形成玻璃料的方法可以包括提供一种玻璃基板，其包括从玻璃基板的表面延伸到玻璃基板的厚度的压缩应力层，压缩应力的深度为 层DOL和初始压应力CSi。 可以在玻璃基板的表面的至少一部分上沉积玻璃料组合物。 然后，将玻璃基板和玻璃料组合物在炉内加热烧结玻璃配合组合物并将玻璃料组合物粘合到玻璃基板上，其中，在加热之后，玻璃基板的烧制压缩应力CSf大于 或等于0.70 * CSi。
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3.发明申请ANTIMONY-FREE GLASS, ANTIMONY-FREE FRIT AND A GLASS PACKAGE THAT IS HERMETICALLY SEALED WITH THE FRIT 有权无反光玻璃，无反光玻璃和玻璃包裹，与玻璃幕墙密封公开(公告)号：US20120222450A1
公开(公告)日：2012-09-06
申请号：US13473204
申请日：2012-05-16
IPC分类号： C03B23/203 , C03C8/08
摘要： An antimony-free glass suitable for use in a frit for producing a hermetically sealed glass package is described. The hermetically sealed glass package, such as an OLED display device, is manufactured by providing a first glass substrate plate and a second glass substrate plate and depositing the antimony-free frit onto the first substrate plate. OLEDs may be deposited on the second glass substrate plate. An irradiation source (e.g., laser, infrared light) is then used to heat the frit which melts and forms a hermetic seal that connects the first glass substrate plate to the second glass substrate plate and also protects the OLEDs. The antimony-free glass has excellent aqueous durability, good flow, low glass transition temperature and low coefficient of thermal expansion.
摘要翻译： 描述适用于玻璃料生产密封玻璃包装的无锑玻璃。 通过提供第一玻璃基板和第二玻璃基板并将无锑玻璃料沉积到第一基板上来制造密封玻璃封装，例如OLED显示装置。 OLED可以沉积在第二玻璃基板上。 然后使用照射源（例如，激光，红外光）来加热熔融物并且形成将第一玻璃衬底板连接到第二玻璃衬底板并且还保护OLED的气密密封件。 无锑玻璃具有优异的水性耐久性，良好的流动性，低的玻璃化转变温度和低的热膨胀系数。
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4.发明授权公开(公告)号：US08198203B2
公开(公告)日：2012-06-12
申请号：US12622569
申请日：2009-11-20
摘要： An antimony-free glass suitable for use in a frit for producing a hermetically sealed glass package is described. The hermetically sealed glass package, such as an OLED display device, is manufactured by providing a first glass substrate plate and a second glass substrate plate and depositing the antimony-free frit onto the first substrate plate. OLEDs may be deposited on the second glass substrate plate. An irradiation source (e.g., laser, infrared light) is then used to heat the frit which melts and forms a hermetic seal that connects the first glass substrate plate to the second glass substrate plate and also protects the OLEDs. The antimony-free glass has excellent aqueous durability, good flow, low glass transition temperature and low coefficient of thermal expansion.
摘要翻译： 描述适用于玻璃料生产密封玻璃包装的无锑玻璃。 通过提供第一玻璃基板和第二玻璃基板并将无锑玻璃料沉积到第一基板上来制造密封玻璃封装，例如OLED显示装置。 OLED可以沉积在第二玻璃基板上。 然后使用照射源（例如，激光，红外光）来加热熔融物并且形成将第一玻璃衬底板连接到第二玻璃衬底板并且还保护OLED的气密密封件。 无锑玻璃具有优异的水性耐久性，良好的流动性，低的玻璃化转变温度和低的热膨胀系数。
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5.发明授权公开(公告)号：US08434328B2
公开(公告)日：2013-05-07
申请号：US13473204
申请日：2012-05-16
摘要： An antimony-free glass suitable for use in a frit for producing a hermetically sealed glass package is described. The hermetically sealed glass package, such as an OLED display device, is manufactured by providing a first glass substrate plate and a second glass substrate plate and depositing the antimony-free frit onto the first substrate plate. OLEDs may be deposited on the second glass substrate plate. An irradiation source (e.g., laser, infrared light) is then used to heat the frit which melts and forms a hermetic seal that connects the first glass substrate plate to the second glass substrate plate and also protects the OLEDs. The antimony-free glass has excellent aqueous durability, good flow, low glass transition temperature and low coefficient of thermal expansion.
摘要翻译： 描述适用于玻璃料生产密封玻璃包装的无锑玻璃。 通过提供第一玻璃基板和第二玻璃基板并将无锑玻璃料沉积到第一基板上来制造密封玻璃封装，例如OLED显示装置。 OLED可以沉积在第二玻璃基板上。 然后使用照射源（例如，激光，红外光）来加热熔融物并且形成将第一玻璃衬底板连接到第二玻璃衬底板并且还保护OLED的气密密封件。 无锑玻璃具有优异的水性耐久性，良好的流动性，低的玻璃化转变温度和低的热膨胀系数。
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公开(公告)号：US20100095705A1
公开(公告)日：2010-04-22
申请号：US12504276
申请日：2009-07-16
申请人： Robert S. Burkhalter , Lisa A. Lamberson , Robert M. Morena , Shyamala Shanmugam , Charlene M. Smith
发明人： Robert S. Burkhalter , Lisa A. Lamberson , Robert M. Morena , Shyamala Shanmugam , Charlene M. Smith
摘要： A dry glass-based fit, and methods of making a dry glass fit are disclosed. In one embodiment a dry glass frit comprises vanadium, phosphorous and a metal halide. The halide may be, for example, fluorine or chlorine. In another embodiment, a method of producing a dry glass frit comprises calcining a batch material for the frit, then melting the batch material in an inert atmosphere, such as a nitrogen atmosphere. In still another embodiment, a method of producing a dry glass frit comprises calcining a batch material for the frit, then melting the batch material in an air atmosphere, such as a nitrogen atmosphere
摘要翻译： 公开了基于干玻璃的配合以及制备干玻璃配合的方法。 在一个实施方案中，干玻璃料包含钒，磷和金属卤化物。 卤化物可以是例如氟或氯。 在另一个实施方案中，制备干玻璃料的方法包括煅烧用于玻璃料的批料，然后在惰性气氛如氮气气氛中熔化批料。 在另一个实施方案中，制备干玻璃料的方法包括煅烧用于玻璃料的批料，然后在空气气氛例如氮气氛中熔化批料
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7.发明申请ANTIMONY-FREE GLASS, ANTIMONY-FREE FRIT AND A GLASS PACKAGE THAT IS HERMETICALLY SEALED WITH THE FRIT 有权无反光玻璃，无反光玻璃和玻璃包裹，与玻璃幕墙密封公开(公告)号：US20110091668A1
公开(公告)日：2011-04-21
申请号：US12622569
申请日：2009-11-20
摘要： An antimony-free glass suitable for use in a frit for producing a hermetically sealed glass package is described. The hermetically sealed glass package, such as an OLED display device, is manufactured by providing a first glass substrate plate and a second glass substrate plate and depositing the antimony-free frit onto the first substrate plate. OLEDs may be deposited on the second glass substrate plate. An irradiation source (e.g., laser, infrared light) is then used to heat the frit which melts and forms a hermetic seal that connects the first glass substrate plate to the second glass substrate plate and also protects the OLEDs. The antimony-free glass has excellent aqueous durability, good flow, low glass transition temperature and low coefficient of thermal expansion.
摘要翻译： 描述适用于玻璃料生产密封玻璃包装的无锑玻璃。 通过提供第一玻璃基板和第二玻璃基板并将无锑玻璃料沉积到第一基板上来制造密封玻璃封装，例如OLED显示装置。 OLED可以沉积在第二玻璃基板上。 然后使用照射源（例如，激光，红外光）来加热熔融物并且形成将第一玻璃衬底板连接到第二玻璃衬底板并且还保护OLED的气密密封件。 无锑玻璃具有优异的水性耐久性，良好的流动性，低的玻璃化转变温度和低的热膨胀系数。
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8.发明授权Lead-free frits for plasma displays and other glass devices utilizing glass sealing materials 失效用于等离子体显示器和其他使用玻璃密封材料的玻璃设备的无铅玻璃料公开(公告)号：US07439201B2
公开(公告)日：2008-10-21
申请号：US11511642
申请日：2006-08-29
摘要： The invention is directed to lead-free glass frit compositions that can be used as sealing frits, the compositions being a blend of: (1) at least one of two glass families which are SnO—ZnO—P2O5 and alkali-ZnO—P2O5 glasses; and (2) at least one cerammed filler material having a crystalline phase selected from the group consisting of beta-quartz, beta-eucryptite, cordierite, and beta-spodumene. The blends of the invention have flow characteristics that enable them to be used at sealing temperatures in the range of 450-550° C., and a CTE value in the range of 60-90×10−7/° C.
摘要翻译： 本发明涉及可用作密封玻璃料的无铅玻璃料组合物，该组合物是以下混合物：（1）两种玻璃族中的至少一种，它们是SnO-ZnO-P 2 O 5和碱金属ZnO-P 2 O 5 O 3玻璃; 和（2）至少一种陶瓷填充材料，其具有选自β-石英，β-曙红，堇青石和β-锂辉石的结晶相。 本发明的共混物具有使其能够在450-550℃的密封温度下使用的流动特性，并且在60-90×10 -7 /℃范围内的CTE值 C。
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9.发明申请公开(公告)号：US20080058193A1
公开(公告)日：2008-03-06
申请号：US11511642
申请日：2006-08-29
摘要： The invention is directed to lead-free glass frit compositions that can be used as sealing frits, the compositions being a blend of: (1) at least one of two glass families which are SnO—ZnO—P2O5 and alkali-ZnO—P2O5 glasses; and (2) at least one cerammed filler material having a crystalline phase selected from the group consisting of beta-quartz, beta-eucryptite, cordierite, and beta-spodumene. The blends of the invention have flow characteristics that enable them to be used at sealing temperatures in the range of 450-550° C., and a CTE value in the range of 60-90×10−7/° C.
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10.发明授权Glass package that is hermetically sealed with a frit and method of fabrication 有权用玻璃料和制造方法气密密封的玻璃包装公开(公告)号：US07407423B2
公开(公告)日：2008-08-05
申请号：US10823331
申请日：2004-04-13
申请人： Bruce G. Aitken , Joel P. Carberry , Steven E. DeMartino , Henry E. Hagy , Lisa A. Lamberson , Richard J. Miller, II , Robert Morena , Joseph F. Schroeder, III , Alexander Streltsov , Sujanto Widjaja
发明人： Bruce G. Aitken , Joel P. Carberry , Steven E. DeMartino , Henry E. Hagy , Lisa A. Lamberson , Richard J. Miller, II , Robert Morena , Joseph F. Schroeder, III , Alexander Streltsov , Sujanto Widjaja
IPC分类号： H01J9/00
CPC分类号： C03C27/06 , C03C3/072 , C03C3/17 , C03C3/19 , C03C3/21 , C03C8/24 , C03C8/245 , C03C27/005 , H01L51/5246
摘要： A hermetically sealed glass package and method for manufacturing the hermetically sealed glass package are described herein using an OLED display as an example. Basically, the hermetically sealed OLED display is manufactured by providing a first substrate plate and a second substrate plate and depositing a frit onto the second substrate plate. OLEDs are deposited on the first substrate plate. An irradiation source (e.g., laser, infrared light) is then used to heat the frit which melts and forms a hermetic seal that connects the first substrate plate to the second substrate plate and also protects the OLEDs. The frit is glass that was doped with at least one transition metal and possibly a CTE lowering filler such that when the irradiation source heats the frit, it softens and forms a bond. This enables the frit to melt and form the hermetic seal while avoiding thermal damage to the OLEDs.
摘要翻译： 这里使用OLED显示器作为示例来描述气密密封的玻璃封装和制造密封玻璃封装的方法。 基本上，通过提供第一基板和第二基板并将玻璃料沉积在第二基板上来制造密封的OLED显示器。 OLED沉积在第一基板上。 然后使用照射源（例如，激光，红外光）来加热玻璃料，其熔化并形成将第一衬底板连接到第二衬底板并且还保护OLED的气密密封。 玻璃料是掺杂有至少一种过渡金属和可能的CTE降低填料的玻璃，使得当照射源加热玻璃料时，其软化并形成结合。 这使得玻璃料熔化并形成气密密封，同时避免对OLED的热损伤。
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