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公开(公告)号：US06245475B1
公开(公告)日：2001-06-12
申请号：US09464599
申请日：1999-12-16
申请人： Merlin E. Scharfe , John M. Hammond , Robert F. Dunham , Jian Cai , Kenny Tuan Dinh , Roger T. Janezic
发明人： Merlin E. Scharfe , John M. Hammond , Robert F. Dunham , Jian Cai , Kenny Tuan Dinh , Roger T. Janezic
IPC分类号： G03G500
CPC分类号： G03G5/05 , G03G5/043 , G03G5/0525 , G03G5/0528
摘要： A method of forming one or more polymer containing layers on a substrate using ink jet nozzles. The method is particularly suited to forming one or more polymer containing layers of a photoreceptor. The polymer containing layers may be formed by moving a substrate, in particular a cylindrical substrate, past the ink jet nozzles, by moving the ink jet nozzles over the substrate, or both. The ink jet nozzles are capable of being independently controlled in order to permit precise location of the coating on the substrate.
摘要翻译： 使用喷墨嘴在基板上形成一个或多个含聚合物层的方法。 该方法特别适于形成一种或多种含感光体的聚合物的层。 含聚合物层可以通过使基板，特别是圆柱形基板移动通过喷墨喷嘴，通过将喷墨喷嘴移动到基板上或两者来形成。 喷墨喷嘴能够被独立地控制，以便允许涂层在基板上的精确定位。
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公开(公告)号：US06270850B1
公开(公告)日：2001-08-07
申请号：US09329678
申请日：1999-06-10
申请人： Jian Cai , Huoy-Jen Yuh , Merlin E. Scharfe , Robert F. Dunham
发明人： Jian Cai , Huoy-Jen Yuh , Merlin E. Scharfe , Robert F. Dunham
IPC分类号： B05D118
CPC分类号： B05D1/18
摘要： A method for improving the quality of a dip coated layer that is deposited by flowing a solution along a substrate in a gap between the substrate and a wall, including: (a) determining a yield stress, a viscosity, a density, and a surface tension of the solution, and selecting a wet thickness of the coated layer; (b) determining a coating speed based on the determined viscosity, the determined density, the determined surface tension of the solution, and the selected wet layer thickness; and (c) selecting a distance for the gap and calculating the shear stress of the solution in the gap based on the gap distance, wherein the shear stress is greater than the yield stress.
摘要翻译： 一种改善通过在衬底和壁之间的间隙中沿着衬底流动溶液而沉积的浸涂层的质量的方法，包括：（a）确定屈服应力，粘度，密度和表面 溶液的张力，以及选择涂层的湿厚度; （b）基于所确定的粘度，所确定的密度，所确定的溶液的表面张力和所选择的湿层厚度确定涂布速度; 和（c）选择间隙的距离，并基于间隙距离计算间隙中溶液的剪切应力，其中剪切应力大于屈服应力。
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公开(公告)号：US06195443B1
公开(公告)日：2001-02-27
申请号：US09079791
申请日：1998-05-15
申请人： John M. Hammond , Jian Cai , Kent J. Evans , John G. Matta , Robert F. Dunham , Mario Errico , Julie A. Cady , Mark C. Petropoulos , Stanley J. Pietrzykowski, Jr. , Mark S. Thomas
发明人： John M. Hammond , Jian Cai , Kent J. Evans , John G. Matta , Robert F. Dunham , Mario Errico , Julie A. Cady , Mark C. Petropoulos , Stanley J. Pietrzykowski, Jr. , Mark S. Thomas
IPC分类号： A61B500
CPC分类号： G01N21/85
摘要： A manufacturing system including: (a) a vessel for holding a liquid; (b) a first member and a second member, each having a flat surface, wherein the flat surface of the first member faces and is spaced from the flat surface of the second member, thereby defining a gap region between the two flat surfaces, wherein a section of the first member is transparent through the thickness of the first member; (c) a liquid delivery system connected to the vessel and the gap region which delivers the liquid to the gap region and the liquid flows in the gap region in view of the transparent section of the first member; (d) a camera positioned to view through the transparent section of the first member; (e) image processing means coupled to the camera for determining the homogeneity of the liquid in the gap region; and (f) liquid dispensing equipment connected to the liquid delivery system.
摘要翻译： 一种制造系统，包括：（a）容纳液体的容器; （b）第一构件和第二构件，每个具有平坦表面，其中第一构件的平坦表面面向并与第二构件的平坦表面间隔开，从而在两个平坦表面之间限定间隙区域，其中 所述第一构件的一部分通过所述第一构件的厚度是透明的; （c）连接到容器的液体输送系统和将液体输送到间隙区域的间隙区域，并且液体在第一构件的透明区域中在间隙区域中流动; （d）定位成通过第一构件的透明部分观察的照相机; （e）耦合到相机的图像处理装置，用于确定间隙区域中液体的均匀性; 和（f）连接到液体输送系统的液体分配设备。
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公开(公告)号：US06706315B2
公开(公告)日：2004-03-16
申请号：US09953526
申请日：2001-09-17
IPC分类号： B05D136
CPC分类号： G03G5/0525 , B05C5/0254 , B05C11/1015 , B05D1/26 , Y10S118/04
摘要： A process comprising: providing a moving substrate; applying at least one coating layer wherein the at least one coating Is a photoconductive material, an electrically insulating material, a hole transport material, an anti-curl material, or an adhesive material onto the moving substrate with a slot die coater equipped with at least one position sensor mounted on at least one end of the slot die coater, and for example, applying from one to about five coating layers on the substrate; sensing the position of the slot die coater relative to the moving substrate with at least one position sensor; and, when the position of the slot die coater relative to the moving substrate deviates from a set of predetermined coordinates, iteratively adjusting the position of the die coater relative to the surface of the substrate to return to the set of predetermined coordinates.
摘要翻译： 一种方法，包括：提供移动的衬底; 将至少一个涂层施加至至少一个涂层，其中至少一个涂层是光电导材料，电绝缘材料，空穴传输材料，抗卷曲材料或粘合剂材料到具有至少装有至少 一个位置传感器安装在槽模涂布机的至少一端，并且例如在基底上施加一个到大约五个涂层; 利用至少一个位置传感器感测槽模涂布机相对于移动基板的位置; 并且当槽模涂布机相对于移动基板的位置偏离一组预定坐标时，迭代地调整模涂机相对于基板表面的位置以返回到预定坐标集合。
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公开(公告)号：US06863730B2
公开(公告)日：2005-03-08
申请号：US10369810
申请日：2003-02-19
CPC分类号： G03G5/0525 , B05C5/0254 , B05C11/1015 , B05D1/26 , Y10S118/04
摘要： An apparatus including: a movement device that moves an object to be coated; a slot die coater equipped with a position sensor mounted on at least one end of the slot die coater and which slot die coater controllably dispenses coating material onto the moving object; and at least one servor motor-controller system in electrical contact with the position sensor, wherein the position sensor senses the position of the slot die coater relative to the object and wherein the at least one servor motor-controller system adjusts the position of the slot die coater relative to the object if the position of the slot die coater relative to the moving substrate deviates from a set of predetermined coordinates.
摘要翻译： 一种装置，包括：移动装置，其移动待涂覆的物体; 一个插槽式模涂机，装有一个安装在槽模涂布机的至少一端的位置传感器，并且该槽模涂布机可控制地将涂层材料分配到移动物体上; 以及与所述位置传感器电接触的至少一个伺服电动机控制器系统，其中所述位置传感器感测所述槽模涂布机相对于所述物体的位置，并且其中所述至少一个伺服电动机控制器系统调整所述槽的位置 如果槽模涂布机相对于移动基板的位置偏离一组预定坐标，则相对于物体的模涂机。
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公开(公告)号：US06214513B1
公开(公告)日：2001-04-10
申请号：US09449355
申请日：1999-11-24
IPC分类号： G03G500
摘要： A coating process for the fabrication of organic photoreceptors employs an electrically conductive single slot die biased to allow an electric field between the die and the ground plane on the photoreceptor substrate. The homogenous coating dispersion is fed through the die at a predetermined gap and rate to control coating thickness at the same time that an electric field is applied. The formulation, rheology, particle mobility, coating speed, electric field and the like are controlled so that the photogenerator particles migrate to the substrate in the dwell time defined by the coating die region.
摘要翻译： 用于制造有机光感受器的涂覆方法采用偏置以允许在感光体基底上的管芯和接地平面之间的电场的导电单槽管芯。 均匀的涂料分散体以预定的间隙和速度通过模具进料，以在施加电场的同时控制涂层厚度。 控制制剂，流变性，粒子迁移率，涂布速度，电场等，使得光电发生剂颗粒在由涂覆模具区域限定的停留时间内迁移到基底。
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公开(公告)号：US5273583A
公开(公告)日：1993-12-28
申请号：US877491
申请日：1992-05-01
申请人： Edouard E. Langlois , Kathryn T. Kehoe , Warren R. Smith , Mark Muscato , Barbara D. Ceglinski , Alan C. Kirchoff , Robert F. Dunham , Michael D. Stair
发明人： Edouard E. Langlois , Kathryn T. Kehoe , Warren R. Smith , Mark Muscato , Barbara D. Ceglinski , Alan C. Kirchoff , Robert F. Dunham , Michael D. Stair
CPC分类号： G03G5/047 , G03G5/0525 , Y10T137/0329
摘要： Apparatus for the continuous coating of charge transport solutions onto a substrate to form an electrophotographic imaging member, including a pump to a flow of a first highly doped charge transport solution and a pump to a flow of a second undoped or lowly doped charge transport solution at predetermined rates to a common junction at which the flows intermix into a common flow upon contacting each other; piping connecting the pumping means to the common junction; and mixing device associated with the junction for continuously mixing the common flow during its movement through the mixing device, the mixing device having a short spiral flow path of less than about 200 cm for the solutions sufficient to substantially complete mix the common flow during its movement through the mixing means.
摘要翻译： 用于将电荷输送溶液连续涂覆到基底上以形成电子照相成像构件的装置，其包括泵到第一高掺杂电荷输送溶液的流动和泵到第二未掺杂或低掺杂电荷输送溶液的流动 预定的速率到共同接合点，在共同接合处，当流体在彼此接触时混合成共同的流动; 将泵送装置连接到公共接头的管道; 以及与连接部相关联的混合装置，用于在公共流动通过混合装置期间连续混合公共流动，混合装置具有小于约200cm的短螺旋流动路径，用于足以在其运动期间基本上完全混合公共流动的溶液 通过混合装置。
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公开(公告)号：US5149612A
公开(公告)日：1992-09-22
申请号：US548310
申请日：1990-07-02
申请人： Edouard E. Langlois , Kathryn T. Kehoe , Warren R. Smith , Mark Muscato , Barbara D. Ceglinski , Alan C. Kirchoff , Robert F. Dunham , Michael D. Stair
发明人： Edouard E. Langlois , Kathryn T. Kehoe , Warren R. Smith , Mark Muscato , Barbara D. Ceglinski , Alan C. Kirchoff , Robert F. Dunham , Michael D. Stair
CPC分类号： G03G5/0525 , G03G5/047
摘要： Processes and apparatus for fabricating an electrophotographic imaging member in which a web coated with a charge generation layer is coated with a charge transport layer comprising a dopant, the improvement comprising detecting the change in dopant concentration required, determining the amount of highly doped charge transport composition and amount of undoped or lowly doped charge transport composition required to achieve the change in dopant concentration, feeding the determined amounts of highly doped charge transport composition and undoped or lowly doped charge transport composition into a mixing zone, rapidly mixing the amounts of highly doped charge transport composition and undoped or lowly doped charge transport composition to form a uniformly doped charge transport composition, and applying the uniformly doped charge transport composition to the charge generation layer.
摘要翻译： 用于制造电子照相成像构件的方法和装置，其中涂覆有电荷产生层的幅材涂覆有包含掺杂剂的电荷输送层，该改进包括检测所需的掺杂剂浓度的变化，确定高度掺杂的电荷输送组合物的量 以及实现掺杂剂浓度变化所需的未掺杂或低掺杂电荷转移组合物的量，将确定量的高掺杂电荷输送组合物和未掺杂或低掺杂电荷转移组合物供给到混合区中，将高掺杂电荷的量快速混合 运输组合物和未掺杂的或低掺杂的电荷输送组合物以形成均匀掺杂的电荷输送组合物，并将均匀掺杂的电荷输送组合物施加到电荷产生层。
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公开(公告)号：US6048658A
公开(公告)日：2000-04-11
申请号：US408239
申请日：1999-09-29
CPC分类号： G03G5/047 , G03G5/0525
摘要： A process for fabricating electrophotographic imaging members comprising providing a substrate with an exposed surface, simultaneously applying, from a coating die, two wet coatings to the surface, the wet coatings comprising a first coating in contact with the surface, the first coating comprising photoconductive particles dispersed in a solution of a film forming binder and a predetermined amount of solvent for the binder and a second coating in contact with the first coating, the second coating comprising a solution of a charge transporting small molecule and a film forming binder dissolved in a predetermined amount of solvent for the transport molecule and the binder, drying the two wet coatings to remove substantially all of the solvents to form a dry first coating having a thickness between about 0.1 micrometer and about 10 micrometers and dry second coating having a thickness between about 4 micrometers and 20 micrometers, applying at least a third coating in contact with the second coating, the third coating comprising a solution containing having a charge transporting small molecule, film forming binder and solvent substantially identical to charge transporting small molecule, film forming binder and solvent in the second coating, and drying the third coating to from a dry third coating having a thickness between about 13 micrometers and 20 micrometers.
摘要翻译： 一种用于制造电子照相成像构件的方法，包括提供具有暴露表面的基底，同时从涂层模具将两个湿涂层施加到所述表面，所述湿涂层包括与所述表面接触的第一涂层，所述第一涂层包含光导颗粒 分散在成膜粘合剂和预定量的用于粘合剂的溶剂的溶液中，第二涂层与第一涂层接触，第二涂层包含电荷输送小分子和成膜粘合剂溶液，其溶解在预定的 用于输送分子和粘合剂的溶剂的量，干燥两个湿涂层以除去基本上所有的溶剂，以形成厚度在约0.1微米至约10微米之间的干燥的第一涂层，并且具有约4的厚度的干燥的第二涂层 微米和20微米，施加至少一个第三涂层与本体接触 第三涂层包含含有电荷输送小分子的溶液，成膜粘合剂和与电荷输送小分子基本相同的溶剂，在第二涂层中形成成膜粘合剂和溶剂的溶液，并将第三涂层干燥至干燥的第三涂层 涂层的厚度在约13微米与20微米之间。
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10.发明授权Method and apparatus for a mechanical dryer for drying thick polymer layers on a substrate 失效用于干燥基材上的厚聚合物层的机械干燥器的方法和装置
公开(公告)号：US5394622A
公开(公告)日：1995-03-07
申请号：US76672
申请日：1993-06-15
申请人： Kent J. Evans , Warren R. Smith , Robert F. Dunham , Timothy J. Leenhouts , Barbara D. Ceglinski , Richard A. Cairncross
发明人： Kent J. Evans , Warren R. Smith , Robert F. Dunham , Timothy J. Leenhouts , Barbara D. Ceglinski , Richard A. Cairncross
CPC分类号： F26B13/10
摘要： A dryer with zone temperature controls for drying thick polymer-solvent layers on a substrate. The dryer is formed with several heating elements located in an air duct. The cool air is heated a specific amount as it passes each heating element. The heated air is then applied to the polymer-solvent solution on the substrate in a continuous fashion so that the polymer-solvent solution slowly heats up as it passes through the drying apparatus. The preferred design is to ensure a zone residence time of less than 10 seconds and a web heating rate of 10.degree. F./second or less. Most preferred design is a zone residence time less than 5 seconds and a heating rate less that 5.degree. F./second. The dryer is designed to have a continuous temperature gradient, especially in the critical later stages of drying when the solvent content of the film is less than 20%.
摘要翻译： 具有区域温度控制的干燥器，用于干燥基底上的聚合物 - 溶剂层。 干燥器形成有位于空气管道中的多个加热元件。 冷空气通过每个加热元件时加热一定量。 然后将加热的空气以连续的方式施加到基底上的聚合物 - 溶剂溶液中，使得聚合物 - 溶剂溶液在其通过干燥装置时缓慢加热。 优选的设计是确保区域停留时间小于10秒，网加热速率为10°F /秒以下。 最优选的设计是区域停留时间小于5秒，加热速率小于5°F /秒。 干燥器设计为具有连续的温度梯度，特别是当膜的溶剂含量小于20％时，在干燥的关键后期阶段。
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