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    METHOD FOR PRODUCING LINEAR PENTENENITRILE
    3.
    发明申请
    METHOD FOR PRODUCING LINEAR PENTENENITRILE 有权
    生产线性胆固醇的方法

    公开(公告)号：US20120178958A1

    公开(公告)日：2012-07-12

    申请号：US13361783

    申请日：2012-01-30

    申请人： Tim Jungkamp ,  Robert Baumann ,  Michael Bartsch ,  Gerd Haderlein ,  Hermann Luyken ,  Jens Scheidel ,  Tobias Aechtner ,  Peter Pfab ,  Petra Deckert ,  Wolfgang Siegel ,  Peter Baßler

    发明人： Tim Jungkamp ,  Robert Baumann ,  Michael Bartsch ,  Gerd Haderlein ,  Hermann Luyken ,  Jens Scheidel ,  Tobias Aechtner ,  Peter Pfab ,  Petra Deckert ,  Wolfgang Siegel ,  Peter Baßler

    IPC分类号： C07C253/30

    CPC分类号： C07C253/30 ,  C07C253/10 ,  Y02P20/582 ,  C07C255/07

    摘要： A method for producing 3-pentenenitrile is provided that includes: (a) isomerizing an educt stream containing 2-methyl-3-butenenitrile on at least one dissolved or dispersed isomerisation catalyst to form a stream (1), which contains the isomerisation catalyst(s), 2-methyl-3-butenenitrile, 3-pentenenitrile and (Z)-2-methyl-2-butenenitrile; (b) distilling the stream (1) to obtain a stream (2) as the overhead product, which contains 2-methyl-3-butenenitrile, 3-pentenenitrile and (Z)-2-methyl-2-butenenitrile and a stream (3) as the bottom product, which contains the isomerisation catalyst(s); (c) distilling the stream (2) to obtain a stream (4) as the overhead product, which is enriched with (Z)-2-methyl-2-butenenitrile in comparison to stream (2), and a stream (5) as the bottom product, which is enriched with 3-pentenenitrile and 2-methyl-3-butenenitrile in comparison to stream (2); (d) distilling stream (5) to obtain a stream (6) as the bottom product, which contains 3-pentenenitrile and a stream (7) as the head product containing 2-methyl-3-butenenitrile.

    摘要翻译： 提供了一种制备3-戊烯腈的方法，其包括：（a）在至少一种溶解或分散的异构化催化剂上异构化含有2-甲基-3-丁烯腈的流出物流以形成含有异构化催化剂（ s），2-甲基-3-丁烯腈，3-戊烯腈和（Z）-2-甲基-2-丁烯腈; （b）蒸馏物流（1）以获得作为塔顶产物的物流（2），其含有2-甲基-3-丁烯腈，3-戊烯腈和（Z）-2-甲基-2-丁烯腈和流（ 3）作为含有异构化催化剂的底部产物; （c）与料流（2）相比，蒸馏物流（2）以获得作为塔顶产物的物流（4），其与（2）相比富含（Z）-2-甲基-2-丁烯腈， 作为与料流（2）相比富含3-戊烯腈和2-甲基-3-丁烯腈的底部产物; （d）蒸馏物流（5），得到作为底物的物流（6），其含有3-戊烯腈和作为含有2-甲基-3-丁烯腈的头部产物的物流（7）。

    Method for the recycling of a lewis acid
    9.
    发明申请
    Method for the recycling of a lewis acid 失效
    路易斯酸回收方法

    公开(公告)号：US20050247624A1

    公开(公告)日：2005-11-10

    申请号：US10520007

    申请日：2003-07-04

    申请人： Tim Jungkamp ,  Jens Scheidel ,  Hermann Luyken ,  Michael Bartsch ,  Robert Baumann ,  Gerd Haderlein

    发明人： Tim Jungkamp ,  Jens Scheidel ,  Hermann Luyken ,  Michael Bartsch ,  Robert Baumann ,  Gerd Haderlein

    IPC分类号： B01J31/18 ,  B01J27/32 ,  B01J31/40 ,  B01J38/00 ,  C07B61/00 ,  C07C253/10 ,  C07C255/04 ,  C07C255/07 ,  B01D11/00

    CPC分类号： B01J31/24 ,  B01J27/32 ,  B01J31/1845 ,  B01J31/4015 ,  B01J31/403 ,  B01J2231/343 ,  C07C253/10 ,  Y02P20/584 ,  C07C255/07

    摘要： A process for the recovery of a Lewis acid from a reaction mixture (I) which has been obtained in the hydrocyanation of an olefinically unsaturated compound to a nitrile which has a miscibility gap with water under certain pressure and temperature conditions, in the presence of a catalyst system comprising a Lewis acid and a complex compound. The method comprises a) removing the complex compound from mixture (I) to give a mixture (II), b) adding water to mixture (II) and placing mixture (II) under pressure and temperature conditions to provide a phase (III) and a phase (IV), c) adding a liquid diluent (V) which c1) does not form an azeotrope with water and whose boiling point under certain pressure conditions is higher than that of water, or c2) forms an azeotrope or heteroazeotrope with water under certain pressure conditions,  to phase (III), d) subjecting the mixture of phase (III) and liquid diluent (V) to distillation under the pressure conditions mentioned in step c1) or c2), and e) subjecting mixture (VII) to hydrocyanation of an olefinically unsaturated compound to give the nitrile

    摘要翻译： 从在不饱和化合物的氢氰化中获得的反应混合物（I）中回收路易斯酸的方法，该反应混合物在一定压力和温度条件下，在与 催化剂体系包含路易斯酸和络合物。 该方法包括：a）从混合物（I）中除去配合物，得到混合物（II），b）在混合物（II）中加入水并将混合物（II）置于压力和温度条件下以提供相（III）和 相（Ⅳ），c）加入一种不与水形成共沸物的液体稀释剂（Ⅴ），其某些压力条件下的沸点高于水，或c2）与水形成共沸混合物 （III），d）在步骤c1）或c2）所述的压力条件下使相（III）和液体稀释剂（V）的混合物进行蒸馏，和e）使混合物（VII） 对烯属不饱和化合物进行氢化，得到腈

    Method for producing linear pentenenitrile
    10.
    发明授权
    Method for producing linear pentenenitrile 有权
    线性戊烯腈的制备方法

    公开(公告)号：US08410299B2

    公开(公告)日：2013-04-02

    申请号：US13361783

    申请日：2012-01-30

    申请人： Tim Jungkamp ,  Robert Baumann ,  Michael Bartsch ,  Gerd Haderlein ,  Hermann Luyken ,  Jens Scheidel ,  Tobias Aechtner ,  Peter Pfab ,  Petra Deckert ,  Wolfgang Siegel ,  Peter Baβler

    发明人： Tim Jungkamp ,  Robert Baumann ,  Michael Bartsch ,  Gerd Haderlein ,  Hermann Luyken ,  Jens Scheidel ,  Tobias Aechtner ,  Peter Pfab ,  Petra Deckert ,  Wolfgang Siegel ,  Peter Baβler

    IPC分类号： C07C253/30

    CPC分类号： C07C253/30 ,  C07C253/10 ,  Y02P20/582 ,  C07C255/07

    摘要： A method for producing 3-pentenenitrile is provided that includes: (a) isomerizing an educt stream containing 2-methyl-3-butenenitrile on at least one dissolved or dispersed isomerization catalyst to form a stream (1), which contains the isomerization catalyst(s), 2-methyl-3-butenenitrile, 3-pentenenitrile and (Z)-2-methyl-2-butenenitrile; (b) distilling the stream (1) to obtain a stream (2) as the overhead product, which contains 2-methyl-3-butenenitrile, 3-pentenenitrile and (Z)-2-methyl-2-butenenitrile and a stream (3) as the bottom product, which contains the isomerization catalyst(s); (c) distilling the stream (2) to obtain a stream (4) as the overhead product, which is enriched with (Z)-2-methyl-2-butenenitrile in comparison to stream (2), and a stream (5) as the bottom product, which is enriched with 3-pentenenitrile and 2-methyl-3-butenenitrile in comparison to stream (2); (d) distilling stream (5) to obtain a stream (6) as the bottom product, which contains 3-pentenenitrile and a stream (7) as the head product containing 2-methyl-3-butenenitrile.

    摘要翻译： 提供了一种制备3-戊烯腈的方法，其包括：（a）在至少一种溶解或分散的异构化催化剂上使含有2-甲基-3-丁烯腈的流出物异构化以形成含有异构化催化剂（ s），2-甲基-3-丁烯腈，3-戊烯腈和（Z）-2-甲基-2-丁烯腈; （b）蒸馏物流（1）以获得作为塔顶产物的物流（2），其含有2-甲基-3-丁烯腈，3-戊烯腈和（Z）-2-甲基-2-丁烯腈和流（ 3）作为含有异构化催化剂的底部产物; （c）与料流（2）相比，蒸馏物流（2）以获得作为塔顶产物的物流（4），其与（2）相比富含（Z）-2-甲基-2-丁烯腈， 作为与料流（2）相比富含3-戊烯腈和2-甲基-3-丁烯腈的底部产物; （d）蒸馏物流（5），得到作为底物的物流（6），其含有3-戊烯腈和作为含有2-甲基-3-丁烯腈的头部产物的物流（7）。