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1.发明授权公开(公告)号：US08486302B2
公开(公告)日：2013-07-16
申请号：US13145571
申请日：2010-01-19
IPC分类号： C01B31/04
CPC分类号： C01B32/23
摘要： The present invention relates to a process for preparing a graphite oxide while purging chlorine dioxide. The invention process employs starting materials comprising a sulfuric acid, a nitric acid, a chlorate salt, and a graphite and further employs an inert purge gas.
摘要翻译： 本发明涉及一种吹扫二氧化氯时制备氧化石墨的方法。 本发明方法使用包含硫酸，硝酸，氯酸盐和石墨的原料，并且还使用惰性吹扫气体。
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2.发明申请公开(公告)号：US20110274610A1
公开(公告)日：2011-11-10
申请号：US13145571
申请日：2010-01-19
CPC分类号： C01B32/23
摘要： The present invention relates to a process for preparing a graphite oxide while purging chlorine dioxide. The invention process employs starting materials comprising a sulfuric acid, a nitric acid, a chlorate salt, and a graphite and further employs an inert purge gas.
摘要翻译： 本发明涉及一种吹扫二氧化氯时制备氧化石墨的方法。 本发明方法使用包含硫酸，硝酸，氯酸盐和石墨的原料，并且还使用惰性吹扫气体。
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3.发明申请CONTINUOUS-FEED FURNACE ASSEMBLY AND PROCESSES FOR PREPARING AND CONTINUOUSLY THERMALLY EXFOLIATING GRAPHITE OXIDE 有权连续进料的烧结组件及其制备和连续热膨胀石墨氧化物的方法公开(公告)号：US20100266476A1
公开(公告)日：2010-10-21
申请号：US12754840
申请日：2010-04-06
CPC分类号： C01B31/0423 , C01B32/225 , C01B32/23 , C01P2006/12 , C01P2006/82
摘要： The present invention relates to a continuous-feed furnace assembly and processes for preparing and continuously thermally exfoliating graphite oxide to give a highly exfoliated graphite.
摘要翻译： 本发明涉及一种连续进料炉组件和用于制备和连续热去角质氧化石墨以产生高度剥离的石墨的方法。
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4.发明授权公开(公告)号：US09321652B2
公开(公告)日：2016-04-26
申请号：US12754840
申请日：2010-04-06
CPC分类号： C01B31/0423 , C01B32/225 , C01B32/23 , C01P2006/12 , C01P2006/82
摘要： The present invention relates to a continuous-feed furnace assembly and processes for preparing and continuously thermally exfoliating graphite oxide to give a highly exfoliated graphite.
摘要翻译： 本发明涉及一种连续进料炉组件和用于制备和连续热去角质氧化石墨以产生高度剥离的石墨的方法。
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公开(公告)号：US08574773B2
公开(公告)日：2013-11-05
申请号：US13132374
申请日：2009-11-16
申请人： David R. Wilson , Ravi B. Shankar , Houxiang Tang , Andrew J. Pasztor, Jr. , Peter M. Margl , William J. Kruper, Jr. , Mark D. Newsham , Jing Jin , Matthew M. Yonkey , Deidre A. Strand , Thomas D. Gregory , Jamie L. Cohen , Jeremy R. Stajdl
发明人： David R. Wilson , Ravi B. Shankar , Houxiang Tang , Andrew J. Pasztor, Jr. , Peter M. Margl , William J. Kruper, Jr. , Mark D. Newsham , Jing Jin , Matthew M. Yonkey , Deidre A. Strand , Thomas D. Gregory , Jamie L. Cohen , Jeremy R. Stajdl
IPC分类号： H01M10/0567 , H01M10/052
CPC分类号： H01M10/0567 , H01M6/168 , H01M10/052 , H01M10/4235 , H01M2300/0025 , Y02T10/7011
摘要： A battery electrolyte solution contains from 0.01 to 80% by weight of an aromatic phosphorus compound. The aromatic phosphorus compound provides increased thermal stability for the electrolyte, helping to reduce thermal degradation, thermal runaway reactions and the possibility of burning. The aromatic phosphorus compound has little adverse impact on the electrical properties of the battery, and in some cases actually improves battery performance.
摘要翻译： 电池电解液含有0.01〜80重量％的芳香族磷化合物。 芳族磷化合物为电解质提供了增加的热稳定性，有助于减少热降解，热失控反应和燃烧的可能性。 芳香族磷化合物对电池的电气性能几乎没有不利影响，在某些情况下实际上提高了电池性能。
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6.发明授权Alkaline earth metal compounds and alkali metal substances via electrochemical process 失效碱土金属化合物和碱金属物质通过电化学过程
公开(公告)号：US4808282A
公开(公告)日：1989-02-28
申请号：US482
申请日：1987-01-05
申请人： Thomas D. Gregory
发明人： Thomas D. Gregory
摘要： Included is an invention, which in one aspect, is a process for preparing a product of an alkaline earth metal compound having at least one BVB-heteromoeity and by-product of an alkali metal substance comprising operating an electrochemical cell, said cell having(1) a sacrificial alkaline earth metal anode,(2) a liquid electrolyte, which contains a solvent that is generally inert and a solute that has at least a residual alkali metal moiety and an incorporatable BVB-heteromoiety therein, and(3) an alkali metal substance segregative cathode, under conditions whereby said product and by-product are prepared. Provided, among other products, are alkaline earth metal organoborates. For example, magnesium triethylpyrrolylborate can be prepared by employing a magnesium anode, a solution of lithium triethylpyrrolylborate in tetrahydrofuran and a cupric oxide and carbon containing cathode. Intercalating cathodes can provide electrical current output.
摘要翻译： 包括的发明是一个发明，其一方面是一种制备具有至少一种BVB异质性的碱土金属化合物和包含操作电化学电池的碱金属物质的副产物的产物的方法，所述电池具有（1 ）牺牲性碱土金属阳极，（2）液体电解质，其含有通常为惰性的溶剂和至少具有残留碱金属部分和其中可掺入的BVB异质性的溶质，和（3）碱金属 物质分离阴极，在制备所述产物和副产物的条件下。 除了其他产品之外，还提供碱土金属有机物。 例如，可以通过使用镁阳极，三乙基吡咯烷基硼酸锂在四氢呋喃中的溶液和含氧化铜和含碳阴极来制备三乙基吡咯烷基硼酸镁。 嵌入阴极可提供电流输出。
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公开(公告)号：US4764263A
公开(公告)日：1988-08-16
申请号：US50666
申请日：1987-05-18
IPC分类号： C25B3/04
CPC分类号： C25B3/04
摘要： Substituted amino aromatic compounds such as 3-amino-4-hydroxybenzoic acid are prepared by electrolytically reducing the corresponding nitro aromatic compound in a basic medium at temperatures below 60.degree. C. and current densities greater than 50 milliamps per square centimeter. The aminohydroxybenzoic acids are useful in the preparation of polybenzoxazoles which are used to make fibers and composites having high strength and thermal stability.
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8.发明授权Process for the preparation of asymmetrical alkaline earth metal organoborates, organoaluminates, organoarsenates, and organophosphates 失效制备不对称碱土金属有机物，有机铝酸盐，有机砷酸盐和有机磷酸盐的方法
公开(公告)号：US4900854A
公开(公告)日：1990-02-13
申请号：US281427
申请日：1988-12-08
摘要： Process for the preparation of asymmetrical alkaline earth metal organoborates and organoaluminates represented by the formula I: ##STR1## and asymmetrical alkaline earth metal organoarsenates and organophosphates represented by the formula II: ##STR2## wherein Z is selected from the group consisting of boron and aluminum; X is selected from the group consisting of phosphorus and arsenic; M is an alkaline earth metal; and in which R.sub.1 -R.sub.6 are independently selected from alkyl, aryl, alkaryl, aralkyl, alkenyl, cycloalkyl, and cyano with the proviso that R.sub.1 -R.sub.6 are not all the same.
摘要翻译： 制备由式I表示的不对称碱土金属有机物和有机铝酸盐的方法：由式II表示的不对称碱土金属有机砷酸盐和有机磷酸盐：其中Z选自 由硼和铝组成的组; X选自磷和砷; M是碱土金属; 并且其中R 1 -R 6独立地选自烷基，芳基，烷芳基，芳烷基，烯基，环烷基和氰基，条件是R 1 -R 6不全部相同。
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公开(公告)号：US4705728A
公开(公告)日：1987-11-10
申请号：US922920
申请日：1986-10-27
申请人： Thomas D. Gregory
发明人： Thomas D. Gregory
摘要： An anionically conductive polymer electrolyte, solid at ambient temperature, containing a salt of the formula:(R).sub.3 CMX.sub.n,wherein M is selected from the group consisting of at least one of boron, phosphorus, antimony, and arsenic, wherein X is halogen, n is 4 or 6, and R is aryl of 6-18 carbon atoms, alkyl of 1-8 carbon atoms, or alkaryl of 7-26 carbon atoms. The polymer is derived from at least one monomer having at least one heteroatom in the monomer unit selected from oxygen, nitrogen, sulfur, and phosphorus. The electrolyte can be prepared by mixing the polymer and the salt together in the presence of a diluent or solvent and removing the diluent or solvent or by polymerizing a salt and monomer mixture utilizing a metal or a Lewis acid catalyst.
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公开(公告)号：US4702974A
公开(公告)日：1987-10-27
申请号：US923364
申请日：1986-10-27
摘要： An electric current producing primary electrochemical cell and a process for producing electric current at an ambient temperature of about 20.degree. C. to about 100.degree. C. in a primary electrochemical cell using a polymer electrolyte which is a solid at a temperature of about 20.degree. C. to about 100.degree. C.
摘要翻译： 产生初级电化学电池的电流和在约20℃至约100℃的温度下在一次电化学电池中使用固体的聚合物电解质在约20℃至约100℃的环境温度下产生电流的方法 C.至约100℃
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